变频器数字语音设计

随着电子元器件以及控制技术的发展．变频器的性能越来越高．人性化的设计要求变得越来越突出。美国信息存贮器件公司的ISD1420单片语音录放芯片．以其优良的性能正被广泛应用。本文即是针对变频器人性化设计的要求．采用ATmega16L单片机控制．利用ID1420语音芯片，实现了变频器高性能语音提示的功能。     

Determination of Myricetin in Medicinal Plants by High-Performance Liquid Chromatography

The concentrations of myricetin in medicinal plants such as Rosa canina L. (rosa hip), Terebinthina chica L. (terebinth), Urtica dioica L. (nettle), and Portuca oleracea L. (purslane) were determined by high-performance liquid chromatography-mass spectrometry (HPLC-MS). The aglycones of myricetin were extracted using methanol–ascorbic acid– hydrochloric acid, methanol–hydrochloric acid, and methanol, separated within 5 min, and individually quantitated in the positive ionization mode using optimized conditions for HPLC-MS. Methanol–ascorbic acid–hydrochloric acid was the optimum extraction solvent. The myricetin concentration in the plants were between 3 and 58 mg kg^?1, with a limit of quantification equal to 0.1 mg L^?1.     

Tribological behaviour of AISI 316L stainless steel for biomedical applications

Abstract

The aim of this research is to study the tribological behaviour of AISI 316L stainless steel for surgical implants (total hip prosthesis). The tribological behaviour is evaluated by wear tests, using tribometers ball on disc and sphere on plane. These tests consisted of measuring the weight loss and the friction coefficient of stainless steel (SS) AISI 316L. The oscillating friction and wear tests have been carried out in ambient air with an oscillating tribotester in accord with standards ISO 7148, ASTM G99-95a and ASTM G133-95 under different conditions of normal applied load (3, 6 and 10 N) and sliding speed (1, 15 and 25 mm s^?1). A ball of 100Cr 6, 10 mm in diameter, is used as counter pairs. These tribological results are compared with those carried out with a tribometer type pin on disc under different conditions of normal load applied P (19·43, 28 and 44 N) and sliding speed (600 and 1020 rev min^?1). The behaviour observed for both samples suggests that the wear and friction mechanism during the tests is the same, and to increase the resistance to wear and friction of biomedical SS AISI 316L alloy used in total hip prosthesis (femoral stems), surface coating and treatment are necessary.     

Influence of the countermaterial on the dry sliding friction and wear behaviour of low temperature carburized AISI316L steel

Low temperature carburising (LTC) allows a significant hardness increase, with a consequent increase in wear resistance, without deteriorating corrosion behaviour. However, wear resistance strongly depends on contact conditions, therefore this work focuses on the dry sliding behaviour of LTC-treated AISI316L austenitic stainless steel against several countermaterials (AISI316L, LTC-treated AISI316L, hard chromium or plasma-sprayed Al₂O₃–TiO₂). LTC produced a hardened surface layer (C-supersaturated expanded austenite), which improved corrosion resistance in NaCl 3.5% and increased wear resistance, to an extent which depends on both normal load and countermaterial. The best results were obtained when at least one of the contacting bodies was LTC-treated, because this condition led to mild tribo-oxidative wear. However, LTC did not improve the behaviour in terms of friction.     

杨凌地区田间小菜蛾种群对新型杀虫剂的敏感性

用浸叶法测定了陕西杨凌地区小菜蛾田间种群对阿维菌素等几种新型杀虫剂的敏感性。结果表明．田间种群小菜蛾对阿维菌素、氟虫腈、啶虫咪、溴虫腈、茚虫威、多杀霉素、甲胺基阿维菌素等的抗性倍数分别为2．75、1.65、1．10、1.27、1．16、1．14和1．32倍,结果表明,田间种群对大多数新型杀虫剂还没有产生明显的抗药性。     

6种杀虫剂对小菜蛾的室内毒力测定及田间药效研究

室内毒力测定结果表明,处理24h后,秀田蛾克的室内毒力最强,LC50为0.64μg/mL,美满次之,LC50为1.86μg/mL。田间药效结果表明,秀田蛾克和美满防治小菜蛾的效果明显优于其他杀虫剂,两者的防效在药后3d达到81%以上,在药后6d达到90%以上。因此,可以作为推广药剂在生产上推广使用。     

人乳头瘤病毒16型晚期蛋白L1基因重组MVA病毒的构建及鉴定

目的研制预防人乳头瘤病毒(HPV)感染的重组修饰的Ankara痘病毒(MVA)活载体疫苗。方法将HPV16L1基因插入MVA病毒转移载体psc11M2的P7·5启动子的下游,构建转移质粒psc11M2-L1,与MVA共转染鸡胚成纤维细胞(CEF),进行同源重组。通过9轮蓝斑筛选,以PCR和Westernblot鉴定重组病毒。结果获得的含目的片段的重组MVA病毒,表达产物与鼠抗人HPV16L1抗体发生阳性反应,目的蛋白相对分子质量约为55000。结论已成功地构建了可正确表达HPV16L1基因的重组MVA病毒株。     

选区激光熔化MnSi2增强316L不锈钢复合材料的表面质量及耐蚀性能

为改善316L不锈钢在海洋环境下的耐腐蚀性能,通过MnSi₂增强316L不锈钢基体,采用选区激光熔化(SLM)制备MnSi₂/316L不锈钢复合材料。利用Image-Pro Plus软件、光学显微镜、扫描电镜(SEM)及电化学工作站研究了激光功率对316L不锈钢金属基复合材料致密度及耐腐蚀性能的影响,通过Tafel极化曲线和阻抗谱表征其耐腐蚀性能的强弱,并通过点蚀形貌揭示了其腐蚀机理。结果表明:添加MnSi₂是提高316L不锈钢耐腐蚀性能的有效途径。随着激光功率的增大,耐腐蚀性能呈现先提高后降低的趋势,当激光功率达到190 W时,2%MnSi₂/316L不锈钢复合材料的致密度为99.80%,其腐蚀电位为－0.053 V (vs SCE)。同时,2%MnSi₂可以显著改善316L不锈钢的成形质量,提高其耐腐蚀性能,其腐蚀形式为氯离子诱导氯化物生成的点蚀,且点蚀产生位置主要集中在孔隙边界处。     

振动时效处理和消应力热处理对304L不锈钢焊接残余应力的影响

奥氏体不锈钢在腐蚀性介质中工作时,若焊接接头存在残余应力易产生应力腐蚀裂纹,需进行消应力处理.文中对不同的消应力方法及其组合对304L不锈钢焊接接头残余应力的影响进行了试验研究.结果表明,单纯的消应力热处理方式和进行机械振动时效处理均可有效去除焊缝及焊趾的峰值应力,应力峰值下降相当,采用消应力热处理方式消应力相对比较均...     

尾矿库埋入式传感器不锈钢外壳腐蚀研究

针对尾矿库埋入式监测仪器或传感器在不同的地下环境中腐蚀严重、经济损失大等问题,采用挂片浸泡、扫描电镜(SEM)、失重法和电化学测试相结合的方法研究了传感器外壳材料(以316L不锈钢为研究对象)在酸性环境和盐卤环境中的腐蚀规律。结果表明,在pH1.5的酸性腐蚀环境中,不锈钢试样短期内钝化膜处于逐渐形成状态,耐蚀性越来越好;经过长期1 a浸泡腐蚀后,耐蚀性略微有所降低;在pH3的硫酸与卤水混合液和pH7.5盐卤水的腐蚀环境中,不锈钢试样短期内耐蚀性越来越好;经过长期浸泡腐蚀后,由于盐卤水中侵蚀性Cl-的存在加速了钝化膜的溶解和破坏,耐蚀性下降幅度明显增大。