导电聚苯胺在微波场中的升温特性

本文研究了微波辐照下导电聚苯胺的升温特性。研究表明 ,导电聚苯胺在微波场中具有快速升温的特点 ,升温速度与掺杂剂的种类、掺杂酸的浓度、聚苯胺的导电率、合成聚苯胺的温度等因素有关。盐酸掺杂聚苯胺热稳定性较差 ,在微波场中不能反复升温 ,而热稳定性较好的DBSA掺杂的聚苯胺具有一定的反复升温能力     

Micro-RBS characterisation of the chemical composition and particulate deposition on pulsed laser deposited Si1−xGex thin films

The formation and deposition of particulates by pulsed laser deposition of Si_1−xGe_x semiconductor alloy thin films are discussed. Using Rutherford backscattering spectrometry with micrometer lateral resolution (micro-RBS) the film composition was measured with high accuracy, even in the presence of particulates with a high areal density of 20,000–30,000 particulates per mm². We show that on impact of a particulate, the part of the thin film which is already deposited probably melts and its Ge content segregates to the surface.     

Effect of the Treatment Temperature on the Surface Drying Set of Sugi Boxed-Heart Square Timber

High-temperature and controlled humidity treatment before drying has proven to be highly effective in preventing surface checks by forming drying sets in the surface layer of boxed-heart square timber in Japan. In this study, we examined the differences of the surface drying sets on sugi timber under different treatment temperatures. As a result, the width of a surface check after drying was much smaller at a treatment temperature of 120°C than at 80°C, and this indicates that the drying set with 120°C treatment would be larger than that with 80°C treatment. Also we observed that treatment temperature had a greater effect on the drying set as the drying advanced.     

借鉴英国经验完善中国土地产权流转

本文在简要介绍中、英两国土地产权制度和土地产权流转的基础上，分析了我国土地产权流转过程中出现的问题，如征地过程中的赔偿过低且不完善、国有土地拆迁补偿不公以及补偿的分配方式不公平等问题。由于英国在土地制度方面与中国的相似性，文章借鉴英国土地补偿中的补偿金与改善金相结合原则、土地使用权的租赁行为以及开发收益回馈社会的方法，为完善和健全我国的土地产权流转机制提出措施和建议。     

Preparation of submicrometer-sized titania hollow spheres by templating sulfonated polystyrene latex particles

Submicrometer-sized titania hollow spheres with tunable shell thickness and smooth surfaces have been successfully synthesized by employing sulfonated polystyrene (PS) latex particles as a template in sol-gel method. The structure of the particles was characterized by scanning electron microscopy and transmission electron microscopy. The shell thickness was readily tuned by altering the concentration of titanium tetrabutoxide (TBOT) in ethanol solutions. The surface roughness as well as the shell thickness has the tendency to increase with the increase in the concentration of TBOT. The diameter of the hollow spheres was on the average of 20-26% smaller than the diameter of template PS latex particles. Some titania fragments were also observed for the sample with the highest TBOT concentration.     

Influence of the Preheat Treatment on the Microstructure and Properties of X37CrMoV5-1 Steel

The technological properties of the hot-work tool steels depend on their microstructural quality induced by the production process and the heat treatment. One of the frequently applied methods to improve microstructure is preheat treatment. The treatment of carbonitriding X37CrMoV5-1 steel has been investigated in fluidized bed furnaces. Thickness and phase composition have been conducted using optical microscopy Neophot 32 and scanning microscopy, JEOL 5400, after etching in nital.     

Stages of surface erosion under ion irradiation

Initial stages of surface erosion have been studied for NaCl and LiF single crystals bombarded by Ar⁺ ions with 20 keV. For irradiation with doses D=10¹⁰-10¹¹ ions/cm², exoelectron emission has been used, whereas for higher doses, we have used electron microscopy. Two stages of initial surface erosion have been identified; for small doses, there is slow development of atomic-scale roughening, which reaches its peak when areas damaged by closest incident ions start to overlap, and then, beginning with D=10¹⁶ ions/cm², there is rapid etching, deep into the crystal, followed by the emergence of secondary microscopic structure, i.e. caverns, concentric closed steps and terraces. Ion-induced surface structure of alkali halide crystals has been shown to depend strongly on the presence of foreign particles on the surface, as well as on segregation. Topography of thin carbon films and some metals have been discussed.     

Investigation of structural properties of ITO thin films deposited on different substrates

The influence of the substrate nature on the structure and morphology of ITO thin films grown by thermal evaporation in vacuum is investigated. The as-prepared metal films with Sn/In molar ratio of 0.1 were subsequently annealed for 2 h at 723 K in air (to obtain tin doped indium oxide), then annealed in vacuum at 523 K, followed by UV irradiation (to reduce the electrical resistivity). Irrespective of substrate nature, XRD data evidence a (222) preferential orientation in films. Substrate nature, annealing in vacuum and UV irradiation influence the structure, morphology, optical, electrical and surface wetting properties of the films' surface.     

Field Verification of Two-Dimensional Surface Irrigation Model

A two-dimensional (2D) model of unsteady shallow-water flow in surface irrigation was developed to evaluate the influence of field-grading precision on surface irrigation performance. This paper presents field data for verification of this 2D model. No attempt was made here to evaluate irrigation performance. Verification of such models relies on independent estimates of parameters for infiltration and roughness. To accomplish this, water surface elevations were measured at 26 points within a 3 ha level basin. A double-bubbler system was used to obtain relative water depths. Field surveys were used to convert these to water surface elevations and field water depths, from which surface water volumes over time were computed. The infiltration function was determined by matching inflow minus surface volume over time with computed subsurface volume. A value of Manning n (0.05) was found for which advance and water depth hydrographs were both well predicted with the 2D model. Differences in advance for a plane versus undulating field surface were minor, except near the end of advance.