预控法与均值极差图在磷铵生产中的应用

以磷铵生产工艺指标中和料浆中N与P物质的量比为例,对比分析了预控法与均值极差图应用效果差异,发现在标准偏差较小的数据分析时,应用预控法效果更佳。     

电子陶瓷材料元素分析的前处理方法研究

陶瓷材料,由于其耐高温、耐腐蚀、耐磨等性能优异,在各行各业应用相当广泛。但也正是因为它的这些特性,在使用化学方法进行元素分析时,会遇到样品难以消解的问题,导致测试无法进行。文章重点研究电子元件中常用的三氧化二铝、氧化锆类陶瓷材料的消解方法,并介绍使用ICP-OES对消解完全的样品溶液进行元素分析的注意事项。     

钠基膨润土胶质价测试方法的改进

以两种人工钠化膨润土为研究对象,探讨了文献胶质价测试方法的不合理性、取土量和MgO量这两个关键因素。实验结果表明:用常规100 mL量筒测胶质价时,取土量和MgO量影响较大,有必要针对具体试样做条件试验,最佳条件是1#钠土为取3.00 g土、0.2 g MgO,2#钠土为取5.00 g土、0.33 g MgO。     

松辽盆地北部致密油体积压裂裂缝形成机理及控制方法

松辽盆地北部中央坳陷区,致密油资源丰富。这种致密储层一般孔吼比大、吼道窄、启动压力高,储层孔隙度小于12%,渗透率小于0.1×10~(-3)μm~2,储层基质向裂缝供油能力较差,常规技术难以有效开发。为致密油储层的有效动用,研究应用了体积压裂技术。通过对大庆油田外围致密储层形成体积缝的延伸机理及特征研究,研发了有效的工艺控制及设计方法,并建立了致密油体积压裂压后产能分析图版。现场试验16口井,增产效果显著,有效指导了设计优化,降低了致密油工业动用孔隙度下限,为大庆油田致密油储层有效开发奠定了基础。     

Quality dependence study on dimensions for plano-concave molded glass lenses

A comprehensive study was conducted to analyze the quality dependence of a plano-concave molded glass lens on its own dimensions, i.e. the effective diameter, sag ratio, and center thickness ratio. To achieve this goal, a thermal-displacement coupled finite element analysis was carried out on the whole molding process, in order to get the results of curve deviation, temperature gradient, and residual stress with sets of variations in these dimensions. Then Taguchi method, one approach for design of experiments, was incorporated to conduct sensitivity analysis on the simulation results to figure out the dominating sequence of these dimensions. The results show that the effective diameter is the most influential factor among these three dimensions. In addition, curve deviation is sensitively proportional to diameter and sag ratio, but decreases insignificantly with greater center thickness ratio. However, residual stress is distinctly proportional to diameter and center thickness ratio, but increases very slightly with greater sag ratio. Results also confirmed the consequential relationship between temperature gradient and residual stress. These discoveries are fundamentally meaningful in getting an overall understanding of the dimensions’ influence on the molded lens quality, thus will help make decision in choosing proper dimensions for optical design.     

Evaluation of membrane filtration for cleanup in multi-residue pesticide analysis of spinach

This study reports a new membrane filtration-based cleanup method for the analysis of pesticides. Recovery and cleanup by membrane filtration using 11 different membranes, classified by their molecular weight cut-off, pore size, and material, were examined. Three different eluent mixtures were also examined. The results indicated that membranes with a 0.1-μm pore size were the most effective among those tested. In particular, hydrophobic polyvinylidene difluoride and hydrophobic polytetrafluoroethylene gave better recoveries and cleanup than other membranes. Results from GC chromatograms and matrix effects showed that membrane filtration afforded better cleanup than the modified QuEChERS method. Furthermore, over 90% of the 89 pesticides tested had acceptable recoveries using these two membranes, according to an acceptable recovery range of 70–120%. Therefore, this technique has potential as an effective cleanup method.     

Optimization of the stream finishing process for mechanical surface treatment by numerical and experimental process analysis

The stream finishing process represents an efficient mass finishing process capable in mechanical surface modification. In order to generate a deeper understanding of the cause-effect relationships, normal forces, material removal and surface topography were analyzed and correlated for varied process parameters of disc-shaped AISI 4140 specimens. Local resolution of tangential velocities of the particles and normal forces on the workpiece’s surface were simulated using the discrete element method for defined process parameter configurations and were correlated with experimental results. A deep process understanding is accomplished enabling the process design for efficient surface smoothing and improved residual stress depth distribution.     

桁架结构中节点板失效模式分析及设计方法研究--以实验测试为例

本文通过实验测试的方法,研究了节点板在腹杆承受轴向压力作用下的破坏过程。     

高填方路基稳定性的几点思考

本文结合实际情况,在分析工程概况及工程地质条件的基础上,分析了填方路基失稳类型,通过反演方法进行了高填方路基填料的抗剪强度参数计算,并进行了高填方路基监测,说明了路基稳定控制的可行性。