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61.
介绍了激光在材料打孔、切割、成形中应用的原理、特点,并阐述了激光快速成形制造的概念、方法及激光在模具制造中的应用情况. 相似文献
62.
Yusuke Yamada Atsushi Ueda Zhen Zhao Toru Maekawa Kengo Suzuki Tadashi Takada Tetsuhiko Kobayashi 《Catalysis Today》2001,67(4):325-387
The rapid evaluation of catalysis is an indispensable technology for the success of combinatorial chemistry. A small-sized, less expensive, easily operating screening is desirable for parallel settings which dramatically shortens the evaluation time. Recent advances in gas sensors have enabled us to use them for the rapid evaluation of oxidation catalysis. Three typical catalytic oxidations over metal oxide catalysts were evaluated by gas sensor systems optimized for each catalytic system. The first one is the total oxidation of carbon monoxide in air. Five catalytic combustion-type gas sensors were used in a parallel reactor system to shorten the evaluation time. The second one is the oxidative dehydrogenation (ODH) of ethane over the mixed oxide of nickel and iron. The evaluation of the ODH catalysis was performed by a selective olefin sensor which determines the concentration of C2H4 in C2H6. The third one is the selective oxidation catalysis of propane over alkali modified Fe/SiO2. The effluents including CO, CO2, aldehydes and ketones in propane were analyzed by the CO, CO2 and semiconductor-type gas sensors selective toward aldehydes and ketones. These evaluation results indicated that gas sensors have a good potential for the rapid evaluation of oxidation catalysts. 相似文献
63.
《Ceramics International》2020,46(12):20163-20172
A double-layer coating composed of MoSi2–SiO2–SiC/ZrB2–MoSi2–SiC was designed and successfully constructed by a novel combination of precursor pyrolysis assisted sintering and rapid sintering to improve the ablation resistance of SiOC ceramic modified carbon fiber needled felt preform composites (CSs). The ZrB2–MoSi2–SiC inner layer coating was in relatively uniform distribution in the zone of 0–3 mm from the surface of CSs through the slurry/precursor infiltration in vacuum and SiOC precursor pyrolysis assisted sintering, which played a predominant role in improving oxidation and ablation resistance and maintaining the morphology of CSs. The MoSi2–SiO2–SiC outer layer coating was prepared by the spray and rapid sintering to further protect CSs from high-temperature oxidation. The ablation resistance of CSs coated with double-layer coating was evaluated by an oxygen-acetylene ablation test under the temperature of 1600–1800 °C with different ablation time of 1000 and 1500 s. The results revealed that the mass recession rates increased with the rise of ablation temperature and extension of ablation time, ranging from 0.47 g/(m2·s) to 0.98 g/(m2·s) at 1600–1800 °C for 1000 s and from 0.72 g/(m2·s) to 0.86 g/(m2·s) for 1000–1500 s at 1700 °C, while the linear recession rates showed negative values at 1700 °C due to the formation of oxides, such as SiO2 and ZrO2. The ablation mechanism of the double-layer coating was analyzed and found that a SiO2–ZrO2–Mo4.8Si3C0.6 oxidation protection barrier would be formed during the ablation process to prevent the oxygen diffusion into the interior CSs, and this study provided a novel and effective way to fabricate high-temperature oxidation protective and ablation resistant coating. 相似文献
64.
65.
Myung-Geun?Song Jong-Yun?Kim Sung-Ho?Cho Jong-Duk?KimEmail author 《Korean Journal of Chemical Engineering》2004,21(6):1224-1230
Microwave-hydrothermal processes for the synthesis of mesoporous silica were investigated with different pathways and mixture
conditions at 373 K, and the corresponding structures to the hydrothermal method were synthesized within a very short crystallization
time. 2-D hexagonally ordered arrays of MCM-41 materials via the direct electrostatic assembly pathway of ST and mediated
templating pathways of S+X-I+ with CTAB were synthesized, and cubic mesophase of MCM-48 was also prepared within 2 hrs of microwave heating without adding
alcohol. Nonionic surfactants with ethylene oxide (EO) moiety as structure-directing agents were used for the preparation
of ordered array of hexagonal or cubic mesostructured silica via the charge matching principle of (S0H+)(X-I+). Although the detailed roles of microwaves may differ for each process, microwaves accelerate the formation of multiply
charged silicate oligomers, initiating mesophase assembly. Therefore, the use of microwave radiation can transfer energy uniformly
and quickly, and complete the syntheses of mesostructured materials within a short time 相似文献
66.
Jared A. StoegerCharitomeni M. Veziri Miguel PalominoAvelino Corma Nick K. KanellopoulosMichael Tsapatsis Georgios N. Karanikolos 《Microporous and mesoporous materials》2012,147(1):286-294
Continuous films comprised of highly c-oriented aluminophosphate AlPO4-5 or cobalt-substituted AlPO4-5 (CoAPO-5) were grown on porous supports and subjected to heat treatment in order to investigate the potential for membrane applications. A study in the early stages of in-plane crystalline intergrowth revealed a potential mechanism for flake-like crystal formation between the original oriented columnar crystals. Variations in metal substitution (AlPO4-5, CoAPO-5), support (glass, silicon, porous alumina), and calcination method (conventional, rapid thermal processing) were chosen to examine the conditions by which structural integrity was compromised following secondary (or tertiary) growth, resulting in reduced membrane functionality. Through the use of rapid thermal processing, the structure debilitation could be partially avoided. The membrane quality was inspected through pervaporation measurements consisting of a liquid hydrocarbon feed of n-heptane and 1,3,5-triisopropylbenzene. By investigating the effect of template removal on the oriented, columnar crystalline structure, useful insight is provided into the potential for the membranes to participate in applications such as molecular separations, catalysis, or host-guest assemblies. 相似文献
67.
以电动按摩棒产品的外观造型设计为例,按照现代设计方法开发工作流程,综合运用逆向工程技术、三维激光测量技术,完成产品外观造型设计。与传统设计方法相比,现代设计方法提高了产品设计的效率,缩短了塑料制品设计和研发周期,提高了企业在市场上的竞争力。 相似文献
68.
Rabia NazirNida Iqbal Abdul S. KhanAftab Akram Anila AsifAqif A. Chaudhry Ihtesham ur. RehmanRafaqat Hussain 《Ceramics International》2012,38(1):457-462
We have optimized the wet precipitation synthesis of hydroxyapaptite to obtain thermally stable powder in the short time span of 3 min. Exposure of the reaction mixture to 1000 W microwave for 3 min furnished hydroxyapatite, which was thermally stable at temperatures up to 1200 °C. Powders were analyzed for phase purity using X-ray crystallography; chemical composition was studied using Fourier transform infrared spectroscopy while particle morphology was analyzed using scanning electron microscopy. 相似文献
69.
The master-alloy ingots for casting bulk metallic glasses are routinely prepared by arc melting a mixture of pure elements. This paper addresses the difficulty in achieving complete and homogeneous melting of refractory component additions in Zr-based BMGs using the above procedure, and its influences on the microstructure and thermal behavior of alloys. 相似文献
70.