Preparation of submicrometer-sized titania hollow spheres by templating sulfonated polystyrene latex particles

Submicrometer-sized titania hollow spheres with tunable shell thickness and smooth surfaces have been successfully synthesized by employing sulfonated polystyrene (PS) latex particles as a template in sol-gel method. The structure of the particles was characterized by scanning electron microscopy and transmission electron microscopy. The shell thickness was readily tuned by altering the concentration of titanium tetrabutoxide (TBOT) in ethanol solutions. The surface roughness as well as the shell thickness has the tendency to increase with the increase in the concentration of TBOT. The diameter of the hollow spheres was on the average of 20-26% smaller than the diameter of template PS latex particles. Some titania fragments were also observed for the sample with the highest TBOT concentration.     

可编程序控制器PLC的抗干扰措施

对可编程序控制器系统常见的一些干扰现象进行分析，对不同的干扰采用了相应的防护措施。     

Influence of the Preheat Treatment on the Microstructure and Properties of X37CrMoV5-1 Steel

The technological properties of the hot-work tool steels depend on their microstructural quality induced by the production process and the heat treatment. One of the frequently applied methods to improve microstructure is preheat treatment. The treatment of carbonitriding X37CrMoV5-1 steel has been investigated in fluidized bed furnaces. Thickness and phase composition have been conducted using optical microscopy Neophot 32 and scanning microscopy, JEOL 5400, after etching in nital.     

Stages of surface erosion under ion irradiation

Initial stages of surface erosion have been studied for NaCl and LiF single crystals bombarded by Ar⁺ ions with 20 keV. For irradiation with doses D=10¹⁰-10¹¹ ions/cm², exoelectron emission has been used, whereas for higher doses, we have used electron microscopy. Two stages of initial surface erosion have been identified; for small doses, there is slow development of atomic-scale roughening, which reaches its peak when areas damaged by closest incident ions start to overlap, and then, beginning with D=10¹⁶ ions/cm², there is rapid etching, deep into the crystal, followed by the emergence of secondary microscopic structure, i.e. caverns, concentric closed steps and terraces. Ion-induced surface structure of alkali halide crystals has been shown to depend strongly on the presence of foreign particles on the surface, as well as on segregation. Topography of thin carbon films and some metals have been discussed.     

Investigation of structural properties of ITO thin films deposited on different substrates

The influence of the substrate nature on the structure and morphology of ITO thin films grown by thermal evaporation in vacuum is investigated. The as-prepared metal films with Sn/In molar ratio of 0.1 were subsequently annealed for 2 h at 723 K in air (to obtain tin doped indium oxide), then annealed in vacuum at 523 K, followed by UV irradiation (to reduce the electrical resistivity). Irrespective of substrate nature, XRD data evidence a (222) preferential orientation in films. Substrate nature, annealing in vacuum and UV irradiation influence the structure, morphology, optical, electrical and surface wetting properties of the films' surface.     

阳泉市煤矿采空区地质因素对公路的破坏

介绍了阳泉市煤矿采空区对公路建设所造成的危害，对其上覆岩层变形破坏的地质因素及其破坏机理作了分析，指出应该采取各种措施减少对公路的破坏。     

65 Mn热轧带钢表面裂纹分析

分析了热轧带钢表面裂纹产生的原因，介绍了采取的工艺措施及其效果。     

鄂尔多斯盆地姬塬-堡子湾地区长4+5油层成岩作用与储层评价

利用岩石铸体薄片鉴定、X射线衍射分析、扫描电镜分析等测试手段，对鄂尔多斯盆地姬塬一堡子湾地区延长组长4＋5油层储集岩的岩石学特征、成岩作用和物性特征进行了分析。结果表明，该储集岩为细粒的长石砂岩和岩屑长石砂岩，颗粒呈次棱角状，成分成熟度普遍较低，结构成熟度中等一较好；经历了压实、胶结、压溶和溶解等一系列成岩作用；储集岩具有低孔、低渗的特点。在以上研究基础上，结合压汞分析、孔隙组合分析，对储层进行综合评价认为，长4＋5储层可分为4类，研究区以Ⅱ、Ⅲ类（中等一差）储层为主。     

用环氧厚浆涂料防混凝土碳化

介绍了针对早期建筑的混凝土桥梁碳化情况采用H52-S4环氧厚浆涂料进行封闭保护、防腐处理的施工方法及施工工艺，并提出施工中应注意的有关事项，对温度影响、表面气泡处理进行了讨论，提出合理化建议。