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51.
Aditya Arun Lakshaman Kumar Anirban Chowdhury 《Journal of the American Ceramic Society》2021,104(7):3497-3507
Dense (~97%) CaO-stabilized ZrO2 ceramic was stabilized with minimum (3 mol%) doping (reported to date) and processed via conventional sintering at a low temperature (~1200°C); compositional analysis via X-ray florescence confirmed the CaO doping accuracy. Phase-pure tetragonal structure (characterized via both X-ray diffraction and Raman spectroscopy) along with uniform nanograins (90 nm) of the ceramic ensured the evolution of no monoclinic phase even after vigorous low-temperature degradation experiments (both thermal and hydrothermal aging for 80-100 h). The sintered ceramic recorded a high hardness (~15 GPa); the indentation toughness value was also comparable to a 3 mol% yttria-stabilized zirconia system. The remarkable structure–property correlations in the 3 mol% CaO-stabilized ZrO2 ceramic suggests that the same may be worth examining for suitable future applications (e.g., in dental ceramics). 相似文献
52.
Leonardo Resende Naira M. Balzaretti Altair S. Pereira Marcos A. Z. Vasconcellos Silvio Buchner 《Journal of the American Ceramic Society》2021,104(6):2552-2559
In this work, high-density lithium disilicate (LS2) vitreous systems were produced by melting and quenching under high pressure (7.7 GPa) following two distinct experimental routes. In the first case, LS2 glass was remelted at 7.7 GPa and 1600°C and, then, quenched. In the second case, a stoichiometric mixture of precursor oxides (Li2O and SiO2) was melted at 1600°C and 7.7 GPa before quenching. A reference LS2 glass sample was produced at atmospheric pressure using conventional melting and quenching procedure. The samples were characterized by X-ray diffraction, differential thermal analysis, and instrumented ultramicro hardness measurements. X-ray diffraction confirmed that all samples were amorphous and thermal analysis suggests that different glassy structures were produced depending on the route of synthesis. Hardness and elastic modulus of the glasses produced under high pressure were higher than those of the reference glass, reflecting the irreversible densification effect induced by the high-pressure processing. 相似文献
53.
Erosion-corrosion investigation of high chromium cast irons using newly designed jet type tester 总被引:1,自引:0,他引:1
A jet type erosion-corrosion tester was developed for the erosion-corrosion investigation of high-chromium cast irons. During tests the size and the shape of particles in the slurry can be maintained stable. The jet velocity and attack angle can be accurately controlled. The repeatability and ranking consistency of the test results are satisfactory. The test parameters can be adjusted in a wide range, so that the tester can simulate various practical working conditions. Electrochemical test data can be automatically collected and processed. Dynamic polarization curves can be obtained during erosion-corrosion test, which can be used to study the dynamic corrosion characteristics.Two high chromium cast irons were studied in hot concentrated alkaline slurry. The results show that the erosioncorrosion mass loss rate and dynamic corrosion rate of 295Cr26 iron is lower than that of 185Cr13 under the conditions similar to alumyte processing. The mechanism of erosion-corrosion of 295Cr26 and 185Cr13 was studied by using the tester. The interaction between erosion and corrosion was also quantitatively evaluated. 相似文献
54.
55.
研究了20Cr11MoVNbNB钢550—650℃的蠕变性能及组织的变化,发现在550℃,蠕变应力>180MPa时,过渡蠕变应变和蠕变时间的ε_β-ι~(1/3)关系中,呈现前期斜率β_1大于后期β_2的两段线性关系;550℃稳态蠕变速率可用■=Aσ~nexp(-Q_c/RT)来表示,其中n=4.7,Aexp(-Q_c/RT)=5.37×10_(-16);550—650℃的表观蠕变激活能Q_c=430kJ/mol,其值远大于基体Fe原子的自扩散激活能;发现在蠕变过程中,随蠕变应力和蠕变时间增加,沉淀相的总量和其中的Cr,Mo,V含量增加,Fe和Nb含量则下降。 相似文献
56.
57.
Manish Roy 《Journal of Thermal Spray Technology》2002,11(3):393-399
The objective of the present work was to determine the dynamic hardness of WC-Co coatings from the dynamic hardness of the
coating substrate system. It was also the purpose of this work to evaluate the influence of coating composition, coating thickness,
and substrate materials on the dynamic hardness of the coating. To achieve the above-mentioned objectives, WC-12%Co and WC-17%Co
coatings were deposited by detonation spraying on three different substrate materials: mild steel, commercially pure (CP)
aluminum, and CP titanium. The dynamic hardness of the coating/substrate composite was evaluated by a drop weight system.
The dynamic hardness of the coating independent of the substrate was determined from the dynamic hardness of the coating/substrate
composite. 相似文献
58.
Thermally sprayed WC-Co is widely used as a wear-resistant coating for a variety of applications. Although it is well established
that thermal spray processes significantly affect chemistry, microstructure, and the phase distribution of WC-Co coatings,
little is known about how these changes influence wear resistance. In this study, the microstructure and wear behavior of
sintered and thermally sprayed WC-Co materials are examined. Powders of WC-12 wt% Co and WC-17 wt% Co were pressed and sintered,
as well as thermally sprayed by high-velocity oxy-fuel (HVOF), air plasma spray (APS), and vacuum plasma spray (VPS) techniques.
Results indicated considerable differences in the resulting microstructures, mechanical properties, and wear resistance. The
thermally sprayed coatings showed anisotropic fracture toughness, whereas the sintered materials did not. It was also shown
that a combined mechanical property/microstructure parameter, based on considerations of indentation fracture mechanisms,
can be used in most cases to describe abrasive and erosive wear resistance of thermally sprayed WC-Co materials as follows:
Wear resistance a
whereK
ic
is the indentation fracture toughness,H is hardness, andV
Co
f
is the volume fraction of cobalt. This relationship provides a means for assessing wear resistance of WC-Co coatings intended
for industrial applications requiring abrasion and/or erosion resistance. 相似文献
59.
Recent progress of CERN RD50 Collaboration 总被引:1,自引:0,他引:1
P. LUUKKA 《中国有色金属学会会刊》2006,16(B01):133-136
The objective of the CERN RD50 Collaboration is to develop radiation hard semiconductor detectors for very high luminosity colliders, in particular, for the upgrade of the large hadron collider (LHC) which itself is scheduled to be operational in 2007. The approach of the RD50 has two major research lines, material engineering and device engineering. These are further subdivided into projects covering defect characterization and engineering, new detector materials, detector characterization, new detector structures and full detector systems. Presently, 264 members from 53 institutes are actively participating in the RD50 Collaboration. Detectors made of defect engineered substrates, e.g. high resistivity magnetic Czochralski (MCz-Si), epitaxial silicon (Epi-Si) on Czochralski silicon (Cz-Si) substrate, intentionally thermal donor (TD) compensated p-type MCz-Si and oxygen enriched (DOFZ) silicon, have been demonstrated by the RD50 Collaboration. An overview and highlights of the results of these defect engineering techniques were given in this report. 相似文献
60.