CLAM钢TIG焊后的热处理工艺研究

为了解决利用钨极氩弧(TIG)焊方法焊接的CLAM钢在焊缝区存在的强度、硬度增加而韧性减弱的问题,从回火温度、回火时间以及重复回火等方面研究了回火对焊缝区硬度的影响,得到了回火温度选择为760℃、回火时间选择为2 h和在760℃保温1 h回火,重复进行两次的两种最佳热处理工艺.     

标准金属布氏硬度块测量不确定度评定

基于JJG147—2005《标准金属布氏硬度块》国家计量检定规程,给出测量不确定度评定的一种方法,指出测量不确定度主要由其均匀度、工作基准布氏硬度机的重复性(短期稳定性)、(副)基准布氏硬度机的测量不确定度、标准比对硬度块的均匀度和长期稳定性引起。以(125～225)HBW10/3 000/30标尺标准块为例,按规程的测量条件和方法,对其测量不确定度进行系统的间接评定。     

DHP铜板爆炸硬化实验研究

DHP铜板是制造连铸结晶器的主要材料,表面硬化技术研究对于提高结晶器使用寿命,具有十分重要的应用价值。采用高应变速率下爆炸硬化方法,对厚度为14 mm的DHP铜板进行表面硬化研究。本研究方法打破传统塑性加工硬化和表面化学硬化等方法,是一种高能率硬化方式。通过检测爆炸硬化后DHP铜板表面的硬度、耐磨性及硬化层组织等指标,表现出突出的表面硬化效应,为这一研究成果的工业应用奠定了良好的研究基础。     

Microstructure Variation and Hardness Diminution During Low Cycle Fatigue of 55NiCrMoV7 Steel

 The influence of temperature and hardness level on the cyclic behavior of 55NiCrMoV7 steel, and the microstructure variation and hardness diminution during low cycle fatigue behavior were investigated. By means of SEM and XRD, the modality of carbides and the full width half maximum (FWHM) of martensite (211) [M(211)] of X ray diffraction spectrum in fatigue specimen were studied. The results showed that the cyclic stress response behavior generally showed an initial exponential softening for the first few cycles, followed by a gradual softening without cyclic softening saturation. The fatigue behavior of the steel is closely related to the hardness level. The hardness diminution and the variation of half width M(211) are remarkably influenced by the interaction between the cyclic plastic deformation and the thermal loading when the fatigue temperature exceeds the tempering temperature of the steel.     

自然崩落法采区地压活动控制技术研究

某铜矿自然崩落法矿山自生产以来底部结构反复受压,造成巷道破坏,为生产带来极大困扰。矿山针对不同的来压情况及破坏形式进行支护试验,并利用沉降观测、微震监测和应力监测等手段对底部结构围岩、支护结构进行监测。经过现场支护试验研究与现场监测,发现断层带最有效的支护方式是刚柔并济,并从超前支护、控制拉底推进线、控制出矿等方面总结出了采场地压活动控制技术。该方法对底部结构地压活动控制具有指导性意义,可为自然崩落法矿山或地压较大的矿山提供参考。     

注氮、注氟SIMOX/NMOS器件辐射加固性能

本文对注N、注F的SIMOX/NMOSFET器件的抗辐射特性进行了研究,发现两者都能减少埋氧层及其界面的空穴陷阱,对辐射加固有所改善,特别是对大剂量辐射的加固更为明显.总体来说,在此能量下,离子注入剂量越大,加固越好.由于注入的剂量对片子本身的阈值电压有很大影响,所以选择对于器件初始特性影响较小的剂量及能量非常重要.     

Resinification Behavior of Regenerated Feather Keratin Powder

A preliminary study was performed on the resinification behavior of regenerated feather keratin powder by changing the sintering conditions, and the thermal and mechanical properties for the obtained resin were investigated. It was confirmed that the molding at 140°C was enough to complete the resinification. The resin obtained was amorphous and its glass transition temperature could be raised to 93°C. In addition, the hardness of the resin could be increased from 20–25 HV to 90 HV by leaving the as-sintered compact resin in ambient air at room temperature for 133 days. Crosslinking agents that work even at room temperature seem to be synthesized during the molding.     

Effect of Kollidon VA®64 particle size and morphology as directly compressible excipient on tablet compression properties

The study evaluates use of Kollidon VA^®64 and a combination of Kollidon VA^®64 with Kollidon VA^®64 Fine as excipient in direct compression process of tablets. The combination of the two grades of material is evaluated for capping, lamination and excessive friability. Inter particulate void space is higher for such excipient due to the hollow structure of the Kollidon VA^®64 particles. During tablet compression air remains trapped in the blend exhibiting poor compression with compromised physical properties of the tablets. Composition of Kollidon VA^®64 and Kollidon VA^®64 Fine is evaluated by design of experiment (DoE). A scanning electron microscopy (SEM) of two grades of Kollidon VA^®64 exhibits morphological differences between coarse and fine grade. The tablet compression process is evaluated with a mix consisting of entirely Kollidon VA^®64 and two mixes containing Kollidon VA^®64 and Kollidon VA^®64 Fine in ratio of 77:23 and 65:35. A statistical modeling on the results from the DoE trials resulted in the optimum composition for direct tablet compression as combination of Kollidon VA^®64 and Kollidon VA^®64 Fine in ratio of 77:23. This combination compressed with the predicted parameters based on the statistical modeling and applying main compression force between 5 and 15?kN, pre-compression force between 2 and 3?kN, feeder speed fixed at 25?rpm and compression range of 45–49?rpm produced tablets with hardness ranging between 19 and 21?kp, with no friability, capping, or lamination issue.     

Comparison of mechanical properties of ground corn stover,switchgrass, and willow and their pellet qualities

Mechanical and physical properties of ground corn stover, switchgrass, and willow were measured and compared in addition to the quality of pellets. Biomass was size-reduced with two different screen sizes (3.175 and 6.35?mm) and conditioned to obtain samples at two different moisture contents (17.5 and 20% on wet basis). Ground switchgrass had the smallest and willow had the highest D₅₀ when size-reduced with the same screen size. Hydrostatic triaxial compression tests were performed using the cubical triaxial tester to determine the bulk modulus, compression index, and spring-back index at specific unloading pressures (20, 45, 70, and 95?kPa). The trends of pressure vs. volumetric strain and void ratio vs. natural log of pressure were similar for all three materials; however, the magnitudes were different. Willow, size-reduced with 3.175?mm screen size at 17.5% wet basis, had the highest bulk modulus among different conditions of all the three biomass. Pellet durability values for all the three materials were higher than 80%. Corn stover pellets formed with 3.175?mm screen size at 20% wet basis had the highest diametral tensile and axial compressive strengths among different conditions for all the three biomass, however the values were not significantly different (p?>?0.05).     

A first-principles investigation on mechanical and metallic properties of titanium carbides under pressure

The titanium carbides are potential candidates to achieve both high hardness and refractory property. We carried out a structural search for titanium carbides at three pressures of 0 GPa, 30 GPa and 50 GPa. A phase diagram of the Ti-C system at 0 K was obtained by elucidating formation enthalpies as a function of compositions, and their mechanical and metallic properties of titanium carbides were investigated systematically. We also discussed the relation of titanium concentration to the both mechanical and metallic properties of titanium carbides. It has been found that the average valence electron density and tractility improved at higher concentrations of titanium, while the degree of covalent bonding directionality decreased. To this effect, the hardness of titanium carbide decreases as the content of titanium increases. Our results indicated that the titanium content significantly affected the metallic properties of the Ti-C system.