Research and Applications of Semi-solid Processing

Since it was pioneered by Flemings and otherresearchers [11, the semi-solid metal processingtechnique has been widely stUdied in the world.Especially in the past decade, SSM as a newproduct forming technique has been rapidly developed and put into commercial applications[2, 31. In recent years, with the development ofthe ado-industry of China, a lot of researchwork on SSM has been done, including the preparation of slumes, reheating and thixoforming[Al6]; moreover, great achievements have …     

高压粉末制样-X射线荧光光谱法测定海洋沉积物中28种组分

常规粉末压片制样是一种简单、高效的绿色环保制样技术,但是应用于某些沉积物样品制备存在样片表面粗糙和粉末容易脱落的问题。实验采用高于常规的压力进行样品制备,建立了X射线荧光光谱法(XRF)分析海洋沉积物样品中包括硫、氧化钠、氧化镁、三氧化二铝、二氧化硅、五氧化二磷、氧化钾、氧化钙、二氧化钛、氧化锰、三氧化二铁、钴、镍、铜、锌、钒、铬、镓、铌、锆、钇、锶、铷、铅、钡、镧、钕和铪在内的28种主、微量组分的方法。探讨了压力为300 kN和1 600 kN时的制样效果,并尝试引入BP神经网络模型利用其非线性拟合能力校正主量组分的基体效应。结果表明,采用1 600 kN压力制备的样片,表面致密、光滑、不龟裂和不掉粉,制样重复性和测试精密度也有较大提高。以55个有证标准物质中17种组分的数据集为训练样本,建立了海洋沉积物样品中主、微量组分的遗传算法-BP神经网络预测模型。按照实验方法对各组分含量相对较低的实际样品连续测试12次,计算得方法的检出限在 0.63～634 μg/g之间;精密度试验结果表明,各组分测定值的相对标准偏差(RSD, n=7)为0.16%～25.1%。方法用于海洋沉积物实际样品分析,其分析结果与国标法的测定结果吻合,能够满足海洋沉积物样品中多种组分准确分析的要求。     

钢铁构件表面上的无机富锌涂层

阐述了无机富锌涂层的研究、发展、特性和应用，指出无机富锌涂层具有杰出的耐环境侵蚀性能、耐化学性、耐溶剂性、耐辐射性、耐热性，在恶劣腐蚀环境下它是钢结构件的最佳底涂层。     

面向网络化定制的产品族复合建模技术

在分析了网络化定制关键技术的基础上，针对性地对信息映射方法和产品族建进行了研究。提出了多层结构信息映射模型，以及综合类元件和参数化特征建模的双层复合产品族模型。结合本方法和以往网络化制造领域中所取得的成果，实现了较完整的基于Web的个性化定制过程。     

Identification of a minor component of the sex pheromone ofLeucoptera malifoliella (Lepidoptera,lyonetiidae)

A new minor component in the female volatile extract ofLeucoptera malifoliella (Costa) (Lepidoptera, Lyonetiidae) has been identified as 5,9-dimethyloctadecane (2). The amount detected of the minor compound2 ranged from 4 to 8% in comparison with the major component 5,9-dimethylheptadecane (1). Neither compound has been found in the male volatile extract. The identification has been based on its spectroscopic properties and Chromatographic behavior in comparison with an authentic synthetic sample. The synthesis has been carried out through a short route from 2,6-dimethylcyclohexanone (3). In field tests, compound2 appears to act as a Synergist of the major component1 when mixed with the latter in a 1000.1– 5 ratio.     

低温共烧陶瓷技术及其应用

低温共烧陶瓷(low temperature co-fired ceramic,LTCC)技术是实现电子元件小型化、片式化的一种理想的封装技术,已成为电子元件集成的主要工艺方式,引起了人们的广泛关注。本文详细叙述了LTCC技术的特点、LTCC材料体系、国内外发展现状以及LTCC技术在电子元件集成中的应用。认为利用LTCC技术来实现电源、有源和无源器件的一体化将是今后信息功能陶瓷发展的一个重要方向。我国应该抓住LTCC技术所面临的前所未有的发展机遇,大力开发具有自主知识产权的LTCC技术,整体提升我国在电子集成领域的技术水平和国际竞争力。     

单组分聚脲材料在寒冷地区某大坝溢流面防护中的应用

水利水电工程泄洪建筑物表面经常遭受高速含沙水流或携带推移质的冲刷,经过一段时间的运行,往往会出现不同程度的磨损及气蚀破坏,采用性能优越的水工混凝土抗冲耐磨材料修复和防护尤为重要。本文通过单组分聚脲材料性能试验揭示了材料的特点,介绍了其在新疆某大坝溢流面防护中的应用情况,其处理技术对类似工程具有良好的借鉴意义。     

Fault identification for process monitoring using kernel principal component analysis

In this research, we develop a new fault identification method for kernel principal component analysis (kernel PCA). Although it has been proved that kernel PCA is superior to linear PCA for fault detection, the fault identification method theoretically derived from the kernel PCA has not been found anywhere. Using the gradient of kernel function, we define two new statistics which represent the contribution of each variable to the monitoring statistics, Hotelling's T²and squared prediction error (SPE) of kernel PCA, respectively. The proposed statistics which have similar concept to contributions in linear PCA are directly derived from the mathematical formulation of kernel PCA and thus they are straightforward to understand. The main contribution of this work is that we firstly suggest a fault identification method especially applicable to process monitoring using kernel PCA. To demonstrate the performance, the proposed method is applied to two simulated processes, one is a simple nonlinear process and the other is a non-isothermal CSTR process. The simulation results show that the proposed method effectively identifies the source of various types of faults.     

蒸汽计量系统的改造及实施方案

通过对一个蒸汽计量系统的实施方案的简单介绍 ,为老企业蒸汽计量系统的改造提供了一种新的经济可行的思路。同时简单介绍了软件开发相关的两个关键控件 :Timer控件和MSComm控件。     

气固相氢氟化催化剂的研究

对于气固相氢氟化反应制备七氟丙烷的催化剂,进行了系统的研究。采用浸渍法制备催化剂,当催化活性组分Ａ为载体的８．５％～１０％,组分Ｃ２为１．０％～２．５％、二者之和为１１％时,达到了较佳的催化性能,将其应用于由六氟丙烯制备七氟丙烷时,在反应温度≥２１０℃时,粗品气中的Ｆ－２２７含量≥９８．５％。