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51.
动态光散射法研究海藻酸钠凝胶松弛行为 总被引:5,自引:0,他引:5
在前文的基础上,用相关函数轮廓分析的方法剖析了运动模型模式的复杂性。通过海藻酸钠水溶液在0.1mol/LCaCl2水溶液透析凝胶化过程中交联网络的松弛时间谱表明它不是单一的峰,有两上特征运动模式,并随透析向更慢的运动模式发展,这很慢的运动模式估计与区域的结构的生成有关。 相似文献
52.
热释电系数的测量方法 总被引:2,自引:0,他引:2
描述热释电系数的两种测量方法。其一为电荷积分法,测试系统简单,测量数据准确,且能满足零电场条件下的测量。其二为动态电流法,采用调制热源技术,研究在特定温度条件下热释电材料的动态热释电响应。 相似文献
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Aggregates of carbon black (CB) in a polymer matrix have a tendency to form a CB network. The dynamic mechanical properties of binary systems of chlorinated polyethylene (CPE) and CB or 3,9‐bis{1,1‐dimethyl‐2[β‐(3‐tert‐butyl‐4‐hydroxy‐5‐methylphenyl)propionyloxy]ethyl}‐2,4,8,10‐tetraoxaspiro[5,5]‐undecane (AO‐80) and their ternary systems were investigated. It was found that the dynamic mechanical properties of those systems depend on the colloidal properties, surface oxides, and surface modification of CB. For binary systems of CPE and CB, oxidized CB gives a high modulus at low strain amplitude and a large Payne effect compared with untreated CB. In contrast, the reverse effect was observed for their ternary systems. Consequently, a good micro‐dispersion is obtainable by surface modification due to physical adsorption of AO‐80 on oxidized CB particles via hydrogen bonds. © 2003 Society of Chemical Industry 相似文献
56.
Ioannis Arvanitoyannis John M. V. Blanshard Ioannis Kolokuris 《Polymer International》1992,27(1):7-15
Mastication of gutta percha (trans-polyisoprene) resulted in the selective scission of molecules, producing a narrower distribution of lower molecular weights. The mechanical properties of the samples also underwent a significant change due to mastication. The greater the content of incompatible substances (salts and oxides) in commercial gutta percha. the more substantial were these effects. The atmosphere (air, N2, O2) in which the experiments were conducted yielded significantly different results. The decrease in molecular weight was far greater in an O2 atmosphere than under a current of nitrogen or air, owing to the combination of double bonds with O2. 相似文献
57.
本文为了克服精馏塔静态仿真不易收敛和初值难以给定等难题,巧妙地利用隐含数值积分方法的特点,将稳态与动态数学模型耦合起来,用以求解高难度的非理想精馏塔静态仿真问题。所得静动态混俣模型大大提高了精馏塔静态仿真的鲁棒性,对于高度非理想精馏塔的仿真尤为有效。通过对某丙烯腈萃取精馏塔的静态仿真,充分证明了这种混合模型化方法的可行性。 相似文献
58.
预测控制算法的统一格式及其在电加热炉的应用 总被引:4,自引:0,他引:4
本文根据常用的两类预测控制算法推出一种新型预测控制算法。并将其应用于一双输入/双输出的力学持久机电加热炉的温度控制系统上,获得了满意的结果:控温精度为±1.5℃/300℃,且适用于非最小相位系统。 相似文献
59.
J. Clausen L. Damkilde L. Andersen 《International journal for numerical methods in engineering》2006,66(6):1036-1059
A new return method for implicit integration of linear isotropic yield criteria is presented. The basic idea is to perform all the manipulations in the principal stress space and thereby achieve very simple formulae for calculating the plastic corrector stresses, based on the constant gradient of such criteria. The return formulae are in closed form and no iteration is required. The method accounts for three types of stress return: return to a single yield plane, to a discontinuity line at the intersection of two yield planes and to a discontinuity point at the intersection between three or more yield planes. The infinitesimal and the consistent elastoplastic constitutive matrix are calculated for each type of stress return, as are the conditions to ascertain which type of return is required. The method is exemplified with the Mohr–Coulomb yield criterion. Copyright © 2005 John Wiley & Sons, Ltd. 相似文献
60.
Plastisols, which are a blend of poly(vinyl chloride) resin and a plasticizer (DEHP), were used as a toughening agent of a resol resin in order to improve the mechanical properties. It was not possible to formulate resol blends by adding more than 10 % of plastisol owing to a lack of apparent homogeneity in the systems, which also showed many air bubbles. The relationship between dynamic mechanical, mechanical and thermal properties and the amount of plastisol added was studied. It was determined from the infrared spectroscopy and dynamic mechanical results that the resol–plastisol blends seem to be formed by a reaction between the phenol and PVC giving a higher crosslinked structure. An improvement in the thermal resistance of the blends at lower temperatures was observed with an increase in the percentage of plastisol. Flexural analysis showed the elastic behaviour of the systems. However, it was not possible to observe the effect of the plasticizer (DEHP) owing to the low quantity of plastisol that was added to the resol. Copyright © 2004 Society of Chemical Industry 相似文献