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191.
柴胡皂苷的提取与鉴定 总被引:2,自引:1,他引:1
报道了大孔吸附层析分离提取柴胡皂苷的实验研究。结果表明。提取分离柴胡皂苷的最佳工艺是:30%乙醇洗杂质、70%的乙醇洗脱2个糖基或3个糖基的柴胡皂苷。柴胡总皂苷的提取率为1.96%。TLC、HPLC检测2个糖基的皂苷是柴胡皂苷b2,属于结构类型Ⅱ。 相似文献
192.
193.
活性炭单柱提取肌苷新技术研究 总被引:1,自引:0,他引:1
活性炭单柱提取肌苷新技术研究李永泉,张进,姚恕,郑莲英,俞峰(杭州大学生物系杭州310028)(浙江大学化工系杭州310027)关键词:肌苷,提取技术,活性炭单柱1前言目前,国内肌苷发酵后处理工艺落后,在分离提取工序中肌苷损失严重,收率一般只有50%... 相似文献
194.
David A. Carlson 《The Journal of supercomputing》1992,6(2):107-116
In this paper a set of techniques for improving the performance of the fast Fourier transform (FFT) algorithm on modern vector-oriented supercomputers is presented. Single-processor FFT implementations based on these techniques are developed for the CRAY-2 and the CRAY Y-MP, and it is shown that they achieve higher performance than previously measured on these machines. The techniques include (1) using gather/scatter operations to maintain optimum length vectors throughout all stages of small-to medium-sized FFTs, (2) using efficient radix-8 and radix-16 inner loops, which allow a large number of vector loads/stores to be overlapped, and (3) prefetching twiddle factors as vectors so that on the CRAY-2 they can later be fetched from local memory in parallel with common memory accesses. Performance results for Fortran implementations using these techniques demonstrate that they are faster than Cray's library FFT routine CFFT2. The actual speedups obtained, which depend on the size of the FFT being computed and the supercomputer being used, range from about 5 to over 300%. 相似文献
195.
196.
Z.M. Zhong J. Chen P. Zhong J.B. Wu 《The International Journal of Advanced Manufacturing Technology》2006,28(9):855-862
As the result of vibration emission in air, a machine sound signal carries important information about the working condition
of machinery. But in practice, the sound signal is typically received with a very low signal-to-noise ratio. To obtain features
of the original sound signal, uncorrelated sound signals must be removed and the wavelet coefficients related to fault condition
must be retrieved. In this paper, the blind source separation technique is used to recover the wavelet coefficients of a monitored
source from complex observed signals. Since in the proposed blind source separation (BSS) algorithms it is generally assumed
that the number of sources is known, the Gerschgorin disk estimator method is introduced to determine the number of sound
sources before applying the BSS method. This method can estimate the number of sound sources under non-Gaussian and non-white
noise conditions. Then, the partial singular value analysis method is used to select these significant observations for BSS
analysis. This method ensures that signals are separated with the smallest distortion. Afterwards, the time-frequency separation
algorithm, converted to a suitable BSS algorithm for the separation of a non-stationary signal, is introduced. The transfer
channel between observations and sources and the wavelet coefficients of the source signals can be blindly identified via
this algorithm. The reconstructed wavelet coefficients can be used for diagnosis. Finally, the separation results obtained
from the observed signals recorded in a semi-anechoic chamber demonstrate the effectiveness of the presented methods . 相似文献
197.
冀中坳陷东北部石炭—二叠系储层特征及勘探方向 总被引:3,自引:0,他引:3
渤海湾盆地冀中坳陷石炭—二叠系残留分布区即坳陷东北部的文安斜坡、杨村斜坡、大城凸起等地区,受印支—燕山和喜马拉雅期强烈的后期构造运动改造,历经差异升降和拉张断陷两大构造发育阶段,致使东、西部剥蚀带的埋藏史表现为沉降—抬升—沉降、沉降—抬升两种类型。区内沉积体系发育较为齐全,自下而上可以识别出滨海潮坪—沼泽、三角洲和河流等三大沉积体系;其中,三角洲和河流体系发育的分流河道、辫状河道砂岩分布范围广、厚度大,形成了该区最主要的砂体类型。区内砂岩储层在其间断埋藏成岩过程中,受表生淋滤作用和深部淋滤作用的影响,形成了较为发育的次生孔隙,孔隙度一般为15%~25%,大气水的深部淋滤作用又进一步改善了断层发育区的储集性能,并由此形成了该区优质的储层。综合评价认为,西部剥蚀带附近是最有利的勘探区带。 相似文献
198.
Ronak A. Kapadia Simant R. Upreti Ali Lohi Ioannis Chatzis 《Journal of Petroleum Science and Engineering》2006,51(3-4):214-222
In this work, a mathematical model is developed and simulated to determine gas dispersion along with solubility during the vapor extraction (Vapex) of live oil from a laboratory scale physical model. The physical model is a rectangular block of homogenous porous medium saturated with heavy oil and bitumen. At a given temperature and pressure, the block is initially exposed on its side to a solvent gas, which diffuses into the medium and gets absorbed. The absorption of gas reduces the viscosity of heavy oil and bitumen causing it to drain under gravity. The low-viscosity “live oil” is produced at the bottom of the porous block. The production of live oil with time is accompanied by the shrinkage of oil in the block as well as its increased exposure to gas from top. These phenomena of Vapex are described by the mathematical model, which is used to calculate live oil production with various values of gas solubility and dispersion. Their optimal values are determined for the vapor extraction of Cold Lake bitumen with butane by matching calculated live oil production with its experimental values published earlier. 相似文献
199.
We studied the surface deformations affecting the southeastern sector of the Po Plain sedimentary basin, in particular the area of Bologna. To this aim an advanced DInSAR technique, referred to as DInSAR-SBAS (Small BAseline Subset), has been applied. This technique allows monitoring the temporal evolution of a deformation phenomenon, via the generation of mean deformation velocity maps and displacement time series from a data set of acquired SAR images. In particular, we have processed a set of SAR data acquired by the European Remote Sensing Satellite (ERS) sensors and compared the achieved results with optical levelling measurements, assumed as reference. The surface displacements detected by DInSAR SBAS from 1992 to 2000 are between 10 mm/year in the historical part of Bologna town, and up to 59 mm/year in the NE industrial and agricultural areas. Former measurements from optical levelling referred to 1897 show 2-3 mm/year vertical movements. This trend of displacement increased in the second half of the 20th century and the subsidence rate reached 60 mm/year. We compared the more recent levelling campaigns (in 1992 and late 1999) and DInSAR results from 1992 to 1999. The standard deviation of the difference between levelling data, projected onto the satellite Line Of Sight, and DInSAR results is 2 mm/year. This highlights a good agreement between the measurements provided by two different techniques. The explanation of soil movements based on interferometric results, ground data and geological observations, allowed confirming the anthropogenic cause (surface effect due to the overexploitation of the aquifers) and highlights a natural, tectonic, subsidence. 相似文献
200.
正交实验优选盐生藻多糖的提取工艺 总被引:1,自引:0,他引:1
以盐生藻为原料,盐生藻多糖得率为指标,运用稀酸、稀碱和蒸馏水为提取剂提取盐生藻多糖,得出合适的提取剂为稀酸.进一步的正交实验表明,盐生藻多糖的最适提取工艺为:提取75min,pH=4,固液比为1∶70,温度为95℃. 相似文献