涂料原料和涂层厚度对反射隔热保温性能影响研究

通过研究涂料配方中所用乳液、颜料、常规填料和隔热填料在红外灯下的反射、隔热和保温性能，发现高折射率的二氧化钛和含有微孔的硅藻土具有最佳的反射和隔热保温效果，轻质碳酸钙和重质碳酸钙具有一定的隔热保温作用，而理论上具有隔热保温效果的填料海泡石等并没有预期的效果。涂层厚度对隔热保温效果具有一定影响，但是没有颜料和填料的影响大。隔热涂料使用的填料应含有硅藻土、二氧化钛以及一些常规的填料。     

CAN总线与以太网互联网关的设计

电梯远程监控系统的关键在于电梯CAN总线与以太网的互联,基于此背景提出一种高性能低成本的解决方案。首先,给出系统总体结构和硬件设计,然后详细阐述软件设计,完成基于μC/OS-II操作系统的嵌入式uIP协议栈的移植开发,并提供软件系统的具体优化方法。最终实现以LPC2368为微处理器和DP83848C以太网控制芯片为核心的CAN总线与以太网互联网关,为工业现场总线与以太网的互联提供了一种可行的解决方案。     

基于UIC556标准的列车通信网络UIC初运行算法的研究

鉴于UIC初运行所具有的特性及在动车通信网络中的重要作用,依据UIC556协议规范,详细地分析UIC初运行的算法和工作原理,以此为基础,首先利用CSS(Configuration Service Station)软件配置网关中对应车辆的静态属性、车辆类型,车辆支持的功能等重要信息并生成NSDB数据库,其次利用UIC Train Diagnostic Station软件将数据库下载到半实物仿真平台的网关中,查看CSS中UIC初运行情况。仿真结果表明实现了UIC初运行。     

一种基于悬浮吸收层的双层结构的热电堆红外探测器(英文)

提出一种新颖红外传感器,这种传感器采用悬浮吸收层的双层结构的优势,来实现相对小尺寸下的高探测性能。双层结构采用2种牺牲层材料,分别为聚酰亚胺牺牲层和预埋在热偶条和沉底之间的多晶硅材料。仿真结果证明了该种结构的探测率、响应率和响应时间分别达到2.85×108cm Hz(1/2)/W、1 800 V/W和6 ms。本文给出了该种热电堆红外探测器高度兼容于CMOS工艺的制备流程,使器件的高效量产和低成本生产成为可能。     

基于CMOS工艺钨微测辐射热计阵列集成芯片的设计与制作

采用0.5μm标准CMOS工艺和微机械加工工艺,设计并制作了低成本4×4钨微测辐射热计阵列集成芯片。阵列中每个钨微测辐射热计均由微悬桥结构和钨热敏电阻组成,CMOS读出电路集成在阵列下方。微悬桥结构由表面牺牲层技术实现,不需要任何的光刻工艺。钨微测辐射热计像元尺寸为100μm×100μm,填充因子为20%。测试结果表明,在真空环境下,钨微测辐射热计等效热导为1.31×10-4W/K,等效热容为1.74×10-7J/K,热时间常数为1.33 ms。当红外光源的斩波频率为10 Hz时,钨微测辐射热计的电压响应率为1.91×103V/W,探测率为1.88×107cm·Hz1/2/W。     

基于VB6.0的红外甲烷检测仪串行通信的实现

针对煤矿安全生产中存在的瓦斯爆炸问题,该文以MSP430系列单片机为核心,设计了红外甲烷检测仪.其中着重介绍了检测仪的串行通信,编写了串行通信程序,使检测仪能实现与PC机的数据通信功能,并使用VB6.0编写了人机交互界面,以方便用户及时观察和处理数据,实现对检测仪的校准、复位和阈值设置等操作功能.实验结果表明,编写的串行通信程序能实现检测仪与PC的数据通信功能,检测仪能快速、准确地检测出甲烷气体的浓度,具有较高的实用价值.     

红外线气体分析在合成氨装置中的应用和改造

介绍了红外线气体分析仪的测量原理以及在合成氨装置中的应用情况。对 使用中出现的故障和原因进行了分析,对预处理装置的改造提出了相应的措施。     

TGA analysis of γ‐irradiated linear low‐density polyethylene

Linear low‐density polyethylene (LLDPE), based on butene‐1 or hexene‐1, was irradiated with γ‐rays under vacuum or in the presence of air. The study focused on the influence of the dose rate and the γ‐dose on the thermal properties of LLDPE. Differential scanning calorimetry, thermogravimetric analysis (TGA), and TGA/FTIR techniques were used to address the thermal behavior as a result of γ‐irradiation. During this irradiation, competition between crosslinking and scission reactions, subsequent to oxidation reactions, occurred in the polymeric material, which strongly depends on the experimental conditions. A decrease of the crystallinity for γ‐irradiated samples was observed in particular for samples irradiated under vacuum. This observation may be explained by increased hindrance of segment mobility due to crosslinking reactions that prevent crystal growth. TGA investigations revealed an enhancement of the thermal stability for samples irradiated under vacuum but not for those irradiated in air. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 100: 2790–2795, 2006     

水泥中硫的高频红外分析方法研究

采用高频红外吸收法测定了水泥中硫的含量,并对样品作测定前的预处理(物理处理),在测定中选用复合型助熔剂,解决了高频感应炉中因顶吹氧气流的作用而导致的样品喷溅问题。该法可准确测定水泥中0.001％～5％的硫,回收率为98.6％～102.5％,RSD为0.78％～1.35％。     

Mandibular gland secretions of the male beewolvesPhilanthus crabroniformis,P. barbatus,andP. pulcher (Hymenoptera: Sphecidae)

The composition of the territorial marking pheromones from mandibular glands of males of the beewolvesPhilanthus crabroniformis, P. barbatus, andP. pulcher have been determined. The structures of the components were elucidated by gas chromatography-mass spectrometry and gas chromatography-Fourier transform infrared spectroscopy. The major compound ofP. crabroniformis is isopropyl tetradecanoate, with somewhat lesser amounts of 2-tridecanone, 3-methyl-3-butenyl tetradecanoate, and 928 (Z)(E)-11-eicosen-1-ol. The major compounds ofP. barbatus are ethyl tetradecanoate and hexadecanal, which are present in approximately a 6040 ratio. These two compounds comprise over 95% of the neutral lipids. Also present in lesser amounts are ethyl dodecanoate, tetradecanal, hexadecan-1-ol, a ^x -octadecen-1-ol, and octadecan-1-ol. The major compounds ofP. pulcher are ethyl (Z)-7-hexadecenoate and geranylgeraniol acetate, which comprise nearly 90% of the neutral lipid fraction, with smaller amounts of tetradecanal, pentadecanal, and ethyl hexadecanoate; trace amounts of ^x hexadecenal, hexadecanal, and octadecanal are also present.