Structure of Atomic and Molecular Adsorbates on Low-Miller-Index ZnO Surfaces Using X-ray Absorption Spectroscopy

We review our X-ray absorption spectroscopy studies of adsorbate geometries on the O-terminated (000 ) and Zn-terminated (0001) basel faces, as well as the non-polar (10 0) prism face of ZnO. Studies employing near-edge X-ray absorption fine-structure (NEXAFS) and surface X-ray absorption fine-structure (SEXAFS) are included.     

结合误差变换的Bouc-Wen迟滞非线性系统反步控制器设计

针对智能材料执行器中非平滑、多映射的迟滞非线性,采用Bouc-Wen模型描述迟滞,并提出了一种基于误差变换的反步控制器设计方案.首先利用Bouc-Wen模型中的变量特性,通过预设性能函数,将误差约束在预设范围内.然后通过误差变换,将一个对输出误差存在约束的跟踪问题转化为一个无约束的镇定问题.最后利用反步控制法设计迟滞系统的控制器,该控制方法保证期望的跟踪精度,并能将误差限定在设定范围内且满足预设性能,提高了系统的暂态和稳态性能.仿真结果表明设计方法的有效性.     

一种检测单晶炉热场温度的新方法

为去除单晶炉热场温度测量信号中的低频干扰、提高温度信号的估计精度,本文提出了一种基于跨维模拟退火(trans dimensional simulated annealing,TDSA)的单晶炉热场温度检测方法.该方法首先将AIC(Akaike information criterion)信号个数判断准则纳入采样机制中以便对干扰个数采样估计,进而利用所设计的基于信号频谱和轮盘赌思想的Metropolis Hastings机制对相应个数的干扰频率进行采样,最后设计了混合均匀和高斯采样机制对单晶炉热场温度进行采样估计.仿真和单晶炉工程实验结果表明,该方法在干扰个数未知的情况下,能够有效地抑制低频干扰、准确检测单晶炉热场的温度.     

Effects of an organic phosphorus nucleating agent on crystallization behaviors and mechanical properties of poly(propylene)

The effects of an organic phosphorus nucleating agent on the crystallization behavior and mechanical properties of poly(propylene) were investigated. As the concentration of nucleating agent increased from 0 to 0.8%, the tensile and flexural strengths of the nucleated poly(propylene) resin increased by 15%, the flexural modulus increased by 35%, the crystallization peak temperature increased by 10°C, and the nucleation density (calculated with the nonlinear Voltrra integral equation) increased by 10⁶ times. Mechanical properties increased with nucleation density. Linear equations between the mechanical properties and the logarithmic nucleation density were revealed. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 88: 297–301, 2003     

重钙装置改产DAP的工程实践

介绍瓮福重钙装置采用混合工艺改产 DAP的技术改造及试车概况、试车中出现的问题及解决措施。     

TiB2的SHS合成过程理论分析

在ＴｉＢ２陶瓷材料的自蔓延高温合成（简称ＳＨＳ）过程中，通过改变原料的起始温度，稀释剂的含量和原始颗粒的尺寸等都可以调节合成过程的绝热温度，产物中熔融相的含量，以及燃烧波蔓延的速度，人而最终影响合成产物的结构和性质。本文对上述各种关系进行了理论计算和分析，其结果对实际合成与制备过程将有着重要的指导作用。     

时间Petri网与CAGA算法相结合的并行测试研究

在并行测试的研究中对于任务的测试次序一直是个研究重点及难题。用时间Petri网建立关于并行测试系统的模型,并首次用元胞遗传算法(CAGA)对模型中的变迁序列进行搜索,快速得到最好的测试序列。通过仿真结果表明,该算法展示了很好的收敛效果,并且与已有的研究成果相比更具优势。     

Removal of chromium (VI) from dilute aqueous solutions by activated carbon developed from Terminalia arjuna nuts activated with zinc chloride

Different structured activated carbons were prepared from Terminalia arjuna nuts, an agricultural waste, by chemical activation with zinc chloride for the adsorption of Cr(VI) from dilute aqueous solutions. The most important parameter in chemical activation was found to be the chemical ratio (activating agent/precursor, g/g). Carbonization temperature and time are the other two important variables, which had significant effect on the pore structure of carbon. A high surface area of was obtained at a chemical ratio of 300%, carbonization time and temperature of 1 h and 500 °C, respectively. The activated carbon developed shows substantial capability to adsorb Cr(VI) from dilute aqueous solutions. The parameters studied include pH, adsorbent dosage, contact time, and initial concentrations. The kinetic data were best fitted to the Lagergren pseudo-first-order model. The isotherm equilibrium data were well fitted by the Langmuir and Freundlich models. The maximum removal of chromium was obtained at pH 1.0 (about 99% for adsorbent dose of 2 g/l and 10 mg/l initial concentration).     

HDPE耐环境应力开裂性能的研究及改进

对HDPE的耐环境应力开裂性能进行了研究。试验表明:采用共混及化学改性的方法,HDPE的耐环境应力开裂性能有了很大提高,为解决HDPE树脂在制作管材时出现的短时间内应力开裂问题提供了依据。     

印刷哈萨克斯拉夫粘连字符的切分方法

哈萨克斯拉夫图像文本经过行切分和列切分后,存在水平方向接触和垂直方向重叠的粘连字符。为提高字符识别率,依据字符连通域的最小外接矩形切分开垂直方向重叠的粘连字符图像块;利用判决条件:字符宽度概率密度分布图、字符图像块垂直投影的波峰数目和字符图像块垂直投影波峰的对称性,分离初始粘连字符图像块中正确的单个字符图像块和实际接触的粘连字符图像块;在允许的字符宽度范围内,寻找粘连字符图像垂直投影图的极小值点,以切分实际接触的粘连字符。实验结果表明,该方法泛化能力较好且识别率有明显提高。