剖析F型、GK型密炼机结构特征

目前，以美国F型和德国GK型为代表的密炼机已在我国基本上实现了国产化。对这两类密炼机的结构特点和安装、使用上的利与弊，本文从密炼装置、转子密封装置、卸料装置、锁紧装置到主传动5个方面作了详细的剖析，并在此基础上，提出一个取长补短的新的密炼机设计方案。     

静态混合器气液两相流压降的数值模拟及实验研究

气泡流经过静态混合器的压降问题涉及到舰船动力系统性能的好坏。在分析了气泡平均驰豫时间的基础上,结合k ε湍流模型,利用平衡流模型模拟静态混合器内形成的稀疏湍流气泡流,得到了混合器内两相流流场。空气—水系统的压力降实验表明,计算流体力学模拟能够很好地预测SMV型静态混合器内气泡流的压降,是静态混合器设计的有效手段。     

Flow patterns in granulating systems

Particle flow patterns were investigated for wet granulation and dry powder mixing in ploughshare mixers using Positron Emission Particle Tracking (PEPT). In a 4-l mixer, calcium carbonate with mean size 45 μm was granulated using a 50 wt.% solution of glycerol and water as binding fluid, and particle movement was followed using a 600-μm calcium hydroxy-phosphate tracer particle. In a 20-l mixer, dry powder flow was studied using a 600-μm resin bead tracer particle to simulate the bulk polypropylene powder with mean size 600 μm. Important differences were seen between particle flow patterns for wet and dry systems. Particle speed relative to blade speed was lower in the wet system than in the dry system, with the ratios of average particle speed to blade tip speed for all experiments in the range 0.01–0.25. In the axial plane, the same particle motion was observed around each blade; this provides a significant advance for modelling flow in ploughshare mixers. For the future, a detailed understanding of the local velocity, acceleration and density variations around a plough blade will reveal the effects of flow patterns in granulating systems on the resultant distribution of granular product attributes such as size, density and strength.     

化工搅拌器的参数优选

本文提出了确定化工用搅拌器搅拌时间的一种简单试验方法,并用正交表安排寻找最佳搅拌参数的试验和整理试验数据,得到了有实用价值的结果。     

Gas/liquid dispersions with a SMX static mixer in the laminar regime

A Sulzer SMX mixer was used to disperse gas into viscous, Newtonian and non-Newtonian fluids. The investigation covered the effect of the dispersed phase volume fraction, the viscosity of the continuous phase, the mixer length and the power draw. The flow regime was kept laminar in all the experiments. The dispersion of gas was carried out with gas concentrations between 1% and 7% in volume. Using the “process viscosity” concept, it was possible to collapse all the measured sizes on a single master curve by using the energy consumption in the mixer as the common variable between the experiments. Comparison was made with a Kenics mixer. The SMX mixer was found to be better adapted to the dispersion task due to its internal structure.     

球窝型动态混合器结构和机理的研究

介绍研制的题示混合器结构及其混合机理。在分析球窝流场各节点速度分布的基础上,用加权平均总应变和分流混合度作为评定指标,对球窝型混合器的混合行为进行分析。通过对比实验证明球窝型混合器对于高粘流体具有良好的混合功效。     

氯醇化管道反应新工艺的压降和传质的研究

氯醇化管道反应新工艺是环氧丙烷生产过程中关键步骤，该反应属气液非均相系统，但装有Ｋｅｎｉｃｓ型静态混合构件的管道反应器用于气液系统还缺乏大量的基础数据。研究以Ｎ２－Ｈ２Ｏ２作为实验系统，测定了不同工况下压降和氧含量，并应用一心均相模型救是了相应的摩擦系数和传质系数。     

强化两相混合的超临界技术制备聚乳酸微粒

针对商品化聚乳酸微球粒径分布较宽难于适用气溶胶给药要求的不足,采用水力空化混合强化超临界流体辅助雾化技术(SAA-HCM)制备聚乳酸(PLA)超细微粒.该技术主要特点是通过在超临界流体和液相进料处引入水力空化混合器,强化两相间的混合.考察SAA-HCM过程混合器压力、温度、沉淀器温度、进料中CO2与液体溶液质量流量比和溶液质量浓度等操作参数对微粒形态和粒径分布的影响,成功制备出球形度较好,粒径分布较窄(1～3μm)的PLA微球.经X射线衍射(XRD)分析和差示扫描量热(DSC)分析显示,与原料PLA相比,微球晶型及热曲线变化不大,但结晶度下降.同时把操作参数与相行为进行关联,探讨了影响颗粒形貌的机理.对比超临界流体辅助雾化法(SAA)的实验结果表明:水力空化的引入能有效强化混合器内的两相传质,混合更好,能制备出适用于气溶胶给药要求的超细微粒.     

混炼胶门尼粘度的预测与控制

使用ＭＧＫＪ型密炼机混炼微机监控系统，在ＢＢ２７０型密炼机上预测混炼胶的门尼粘度值，实现了胎面胶门尼粘度值的预测。预测值与实测值的差平均为０８（相对误差１％）。借助预测门尼粘度的数学模型，对排胶点进行控制，使混炼胶门尼粘度的波动范围为－３～＋３。     

潜水搅拌器安装角度对搅拌效果的影响

研究潜水搅拌器水平安装角度对搅拌池内流场的影响,建立不同的水平安装角度,通过Fluent对潜水搅拌机的搅拌槽内流场进行三维数值模拟,得出不同方案的速度分布情况.利用UDF模块,分别计算流场中流速达到搅拌效果的有效搅拌流体体积及其占整个流场体积的百分比,通过比较,选出最优的潜水搅拌器安装方案,提出了评价潜水搅拌器效能及其安装布置优劣的新方法——有效搅拌域法,利用此方法,使潜水搅拌器的搅拌效果分析更加准确.