前卸料混凝土搅拌运输车车架结构模态分析

有限元模态分析和试验模态分析方法是辨识车辆结构动态性能的一种有效手段。为分析前卸料混凝土搅拌运输车车架的动态特性,建立了以板壳单元为基本单元的车架有限元模态分析模型及模态试验系统。应用NASTRAN有限元分析软件计算了该车架在自由状态下的模态参数,并进行了模态试验,提取模态参数。计算结果与试验结果对比分析表明,所建立的有限元模型和分析方法是可行的,可为分析车架在工作状态下的动态特性及车架结构的进一步改进提供依据。     

双工质塑料冷混机设计研讨

介绍了可提高塑料混合时冷却效率的双工质塑料冷混机，并简要叙述了立式，卧式和立式搅龙双工质冷混机却装置冷却物料的工序。     

Laminar mixing of shear thinning fluids in a SMX static mixer

Flow and mixing of power-law fluids in a standard SMX static mixer were simulated using computational fluid dynamics (CFD). Results showed that shear thinning reduces the ratio of pressure drop in the static mixer to pressure drop in empty tube as compared to Newtonian fluids. The correlations for pressure drop and friction factor were obtained at Re_MR?100. The friction factor is a function of both Reynolds number and power-law index. A proper apparent strain rate, area-weighted average strain rate on the solid surface in mixing section, was proposed to calculate pressure drop for a non-Newtonian fluid. Particle tracking showed that shear thinning fluids exhibit better mixing quality, lower pressure drop and higher mixing efficiency as compared to a Newtonian fluid in the SMX static mixer.     

具有高可调增益范围的CMOS宽带中频调制器

利用TSMC 0 .2 5 μmCMOS混合工艺 ,针对超外差结构的无线宽带收发器 ,实现了一个能够工作在 5 0～6 0 0MHz的中频调制器 ,并对该调制器进行了仿真和测试。由于该调制器在输出端采用了一个具有高可调增益范围而且鲁棒性能好的可变增益放大器 (VGA) ,从而使得该调制器具有超过 70dB的增益可调范围。测试结果表明 ,该调制器能够工作在 5 0～ 6 0 0MHz的频率上 ,输出功率为 - 81～ - 10dBm ,最小增益的输出噪声为 - 130dBm/ Hz,最大增益的输出P1dB点为 - 4 .3dBm ,在 3V的电源电压下 ,电流功耗为 32mA。     

模块化微反应系统内溴化间甲基苯甲醚连续合成

根据微化工技术发展的主要趋势,针对4-溴-3-甲基苯甲醚间歇非均相合成技术存在的问题,以微筛孔反应器与玻璃微珠填充床为核心功能微设备单元构建了模块化微反应系统,并在此模块化微反应系统内对液-液非均相连续溴化合成4-溴-3-甲基苯甲醚开展研究。通过优化操作条件,在溴浓度(x_Br2)为17.5%(质量分数)、溴与间甲基苯甲醚摩尔比(n_Br2/n_M)为1.01、反应起始温度(T)为0℃、停留时间为0.78 min条件下,4-溴-3-甲基苯甲醚的收率大于98%,多溴代副产物的含量仅为1%。与传统间歇溴化反应相比,模块化微反应系统内连续溴化反应具有十分明显的优势:可将间歇过程连续化,在保证安全的基础上极大地提升了反应的效率(时空收率为6.5×10⁴kg/(m³·h));另外,该过程是由传质控制的,微反应器的传质性能优异,可极大地改善产品的选择性(多溴代副产物的量减少50%)。该研究为4-溴-3-甲基苯甲醚的连续高效安全合成提供了技术和设备依据。     

Foam granulation: Liquid penetration or mechanical dispersion?

There have been significant advances in the understanding of wet granulation processes. Foam granulation is the latest development and an emerging area of interest for pharmaceutical manufacturing.Single foam penetration experiments were carried out on static powder beds, followed by short-nucleation experiments (where nuclei are formed by a nucleation-only mechanism) and full foam granulation experiments (where nucleation, growth and breakage are occurring simultaneously). All experiments were performed with lactose monohydrate powder using a 5 L high shear mixer–granulator. The foam penetration/dispersion behaviour was examined and the granule size distributions were investigated as a function of foam quality (83–97% FQ), impeller speed (105–515 rpm) and wet massing period (0–4 min).Nucleation in foam granulation is postulated to undergo either “foam drainage” or “mechanical dispersion” controlled mechanisms. For “foam drainage” mechanism, the foam penetrates the powder bed to form coarse and broad granule size distributions. For “mechanical dispersion” mechanism, the wetting and nucleation conditions are governed by the powder mixing conditions and similar granule size distributions are produced. Regardless of the mechanism, the initial wetting and nucleation behaviour controls the initial nuclei size distribution, and this initial distribution is retained in the final granule size distribution. This work demonstrated the critical importance of the nucleation and binder distribution in determining the granule size distributions for foam granulation process.     

高速混合机的应用及研究进展

高速混合机是高分子材料成型加工等行业的必备设备之一。介绍调整混合机的基本工作原理、在各行业的应用及及研究情况和应用展望。     

含氟聚合物聚合反应釜传质能力改善

介绍了含氟聚合物聚合反应釜传质能力改善的方法：将聚合反应釜的推进式和锚式的组合体搅拌更换为涡轮式和锚式的组合体;延长挡板,缩短与反应釜釜盖的距离。改善前后生产的聚合物的分子量及其分布的变化也证实反应釜传质能力的提高。     

焦炉新型煤气掺混器的开发与应用

针对以往煤气混合器的优缺点,设计开发了新型煤气混合器。新型煤气混合器具有掺混均匀、不易堵塞、操作方便安全等优点,对降低能源消耗和生产成本有积极的作用。该掺混装置应用于多个焦炉项目中,运行状态良好。     

脉冲式气流混合机的设计与应用

设计了新型脉冲式气流混合机。该混合机具有混合效率高、快速混合、大型化、单位能耗低等特点。