二硫代磷酸硫化氧钼与硫,磷添加剂的复配特性研究

研究了二烷基二硫代磷酸硫化氧钼（ＭｏＤＴＰ）摩擦改进剂及其与硫、磷、硫－磷型添加剂复合的抗磨减摩性能。试验表明，经过适当复配后，这类合活性元素的添加剂对ＭｏＤＴＰ的抗磨减摩性能均有增效作用，同一类型添加剂的活性愈高，增效作用愈显著。同时利用扫描电镜和Ｘ－射线能谱仪进行摩擦副表面膜的形貌照相及元素分析，对复合作用的机理进行了初步探讨。     

瓦斯尾巷在高档普采工作面的应用

介绍了高档普采工作面利用掘送瓦斯尾巷等措施形成回风空间 ,从根本上解决高档普采工作面的瓦斯超限问题 ,其工艺有利于在其它采煤工作面内应用     

带有块间串扰MC-CDMA的时域信道估计和多用户检测

本文把带有IBI的MC-CDMA系统等效解释为特殊的直接序列码分多址（DS-CDMA）系统，并给出了相应的时域信道估计方法和时域线性最小均方误差（MMSE）多用户检测方法。仿真实验表明了本文方法的性能。     

孔隙度校正缺乏理论依据

储油岩石一般为致密介质。致密介质在应力作用下，以本体变形（弹性变形）为主，孔隙度不发生变化。油气储量计算时，地面实测孔隙度不发生变化。油汽储量计算时，地面实测孔隙度不需要进行校正。传统的孔隙度校正无形中损失了一部分地质储量，同时为确定校正值大小也浪费了大量人力和物力。致密岩石弹性变形过程中的孔隙度不变性原则将给储量计算带来很大的方便。     

克拉2气田储层岩石的应力敏感性及其对生产动态的影响

克拉2气田是一个异常高压气藏，压力系数在2．0以上。在衰竭式开采条件下，其地层压力降幅可为普通气藏地层压力降幅的3倍以上，因此研究储层岩石应力敏感性及其对生产动态的影响意义重大。研究得出，岩石的应力敏感性特征主要有：岩石物性对应力的敏感性总体上不大，其中以孔隙度最小，渗透率次之，压缩系数最大；岩石物性随地层压力的下降而下降；在同一地层压降下．岩石物性下降幅度不是渗透率的连续函数，而是与渗透率分布范围有关，高渗透率范围，岩石物性下降幅度小，低渗透率范围，岩石物性下降幅度大。研究得出，克拉2气田岩石的应力敏感性对其生产动态的影响较小。     

Thermal Radiative Properties of Xonotlite Insulation Material

Introduction Xonotlite-type calcium silicate (6CaO?6SiO2?H2O) is synthesized porous insulation material by hydrothermal processing with quartz powder and limestone as the raw material (with CaO/ SiO2≈1:1). Compared with fire- retardant fibre, xonotlite has more excellent insulating performance, such as low thermal conductivity, environment friendly, high intension, and wide applying temperature range, which has been emphasized in recent years by many scholars and widely used in many indu…     

Inference for pth‐order random coefficient integer‐valued autoregressive processes

Abstract. A pth‐order random coefficient integer‐valued autoregressive [RCINAR(p)] model is proposed for count data. Stationarity and ergodicity properties are established. Maximum likelihood, conditional least squares, modified quasi‐likelihood and generalized method of moments are used to estimate the model parameters. Asymptotic properties of the estimators are derived. Simulation results on the comparison of the estimators are reported. The models are applied to two real data sets.     

2，6-萘二甲酸二甲酯在有机溶剂中溶解度的测定与关联

Solubility of dimethyl-2,6-naphthalene dicarboxylate in acetic acid, N,N-dimethylfonnamide, N,N-dimethyl acetamide, dimethyl sulphoxide, and N-methyl-2-ketopyrrolidine were determined using a dynamic method. The measured systems were correlated by UNIFAC group contribution method. A new main group （aromatic ester, ACCOO） was defined to express the activity coefficients of the aromatic ester. New interaction parameters of the ACCOO group were expressed as the first-order function of temperature and were determined from the experimental data. The calculated results for the new interaction parameters were satisfactory. The measured systems were also correlated with the Wilson and 2-h models, and the results were compared with those of the UNIFAC model.     

Complex system reliability modelling with Dynamic Object Oriented Bayesian Networks (DOOBN)

Nowadays, the complex manufacturing processes have to be dynamically modelled and controlled to optimise the diagnosis and the maintenance policies. This article presents a methodology that will help developing Dynamic Object Oriented Bayesian Networks (DOOBNs) to formalise such complex dynamic models. The goal is to have a general reliability evaluation of a manufacturing process, from its implementation to its operating phase. The added value of this formalisation methodology consists in using the a priori knowledge of both the system's functioning and malfunctioning. Networks are built on principles of adaptability and integrate uncertainties on the relationships between causes and effects. Thus, the purpose is to evaluate, in terms of reliability, the impact of several decisions on the maintenance of the system. This methodology has been tested, in an industrial context, to model the reliability of a water (immersion) heater system.     

Simultaneous HPLC quantification of total cholesterol,tocopherols and β-carotene in Barrosã-PDO veal

A simple, rapid and sensitive procedure for the simultaneous determination of total cholesterol, tocopherols and β-carotene in meat is described. The method involves a direct saponification of the meat, a single n-hexane extraction and the analysis of the extracted compounds by normal-phase HPLC, using fluorescence (tocopherols) and UV–Vis photodiode array (cholesterol and β-carotene) detections in tandem. Rates of recovery of spiked meat samples were 93% for cholesterol, 83–86% for (α-, β- and -γ) tocopherols and 89% for β-carotene. Repeatabilities were high (CV < 6%) for all determined compounds, except for δ-tocopherol. This tocopherol, which is not usually present in meat, showed a much lower recovery percentage (73%) and repeatability (12.8%). This methodology was applied for the quantification of total cholesterol, tocopherols and β-carotene in three muscles (longissimus thoracis, longissimus lumborum and semitendinosus) of the Portuguese traditional Barrosã-PDO veal, obtained from autochthonous calves fed extensively during summer (with the least abundant green pastures) and slaughtered in early autumn (October). Barrosã-PDO veal showed median contents of total cholesterol (0.50–0.56 mg/g) and, depending on the analysed muscle, moderate to high contents of α-tocopherol (3.3–3.9 μg/g) and β-carotene (0.07–0.09 μg/g), suggesting an high sensorial and hygienic quality.