奎宁印迹聚合物的吸附与识别特性的研究

以奎宁为模板分子 ,利用分子印迹技术合成了一种新型的类似于人工受体的印迹聚合物 ,研究了它对奎宁和其它底物的吸附特性和选择性识别能力 ,并对其固相萃取性能做了初步的研究。     

Original Finger Image Extraction by Morphological Technique and Finger Image Comparisons for Persons' Identification

This research uses the object extracting technique to extract the index, middle and ring fingers from the hand images. The algorithm developed in this research can find the precise locations of the different fingers' fingertips and the finger-to-finger-valleys. After finding the positions of the fingertips and finger-valleys, the index, middle and ring fingers can be extracted from the hand images by using morphological technique. The extracted index, middle and ring fingers contain many useful geometry features. One can use these features to do the person's identification. The orientations of the index, middle and ring fingers are found in this research. Image rotating, image shifting, and image interpolating techniques are used to align different persons' index, middle and ring fingers. Image subtraction is used to exam the difference of two index, middle and ring finger images. In this research so far only use the index, middle and the ring fingers as the features to identify different persons. ^★This work was supported by National Science Council under grant NSC 93-2213-E-212-011.     

马尾松木材中性脱脂工艺的研究

采用全因素试验法，对马尾松木材进行过热乙醇溶液脱脂处理，以获取马尾松木材高效脱脂工艺技术。试验结果显示：（1）脱脂温度对马尾松松脂溶出量的影响极显著，且溶出量随着脱脂温度的升高而增大；（2）脱脂时间对马尾松松脂溶出量的影响极显著，且溶出量随着脱脂时间的延长呈先增大后减小的趋势；（3）脱脂浴比对马尾松松脂溶出量的影响极显著，且溶出量随着脱脂浴比的延长呈先增大后减小的趋势；（4）利用过热乙醇溶液对马尾松木材进行脱脂，其最佳工艺是脱脂时间为130℃、脱脂时间为8h、浴比1：8。     

In situ formation of multi scale reinforcing phases to improve performance of Al2O3-SiC C castables

In order to improve the physical properties and slag corrosion resistance of refractory materials for hot metal pretreatment, different contents of composite metal powders (CMP) were introduced into Al2O3-SiC-C refractory castables. The effect of CMP on the microstructure, physical properties and slag corrosion resistance of Al2O3-SiC-C refractory castables were studied. The results show that the multi scale reinforcing phases including flake crystals, rod shaped fibers, filamentous fibers and whiskers are in situ formed in the samples with addition of CMP, which result to the improvement of the cold modulus of rupture and cold crushing strength. When the addition of CMP is 6 wt.%, the high temperature modulus of rupture increases by 231%, the thermal shock resistance increases by 77% after thermal shock by water cooling 5 times and the percentage of the slag resistant area reduces by 37.2%.     

超临界萃取装置高压快开密封结构改进设计

对普遍采用的以橡胶O形环作为自紧密封件的高压快开密封装置密封部位的结构进行了改进,彻底解决了橡胶O形环在卸压后发生膨胀,将筒体端部法兰与密封盖卡死的问题。开发出了1种新的组合密封环,该密封环可广泛用于超临界萃取装置上。     

Protein Extraction from Heat-stabilized Defatted Rice Bran: II. The Role of Amylase, Celluclast, and Viscozyme

ABSTRACT: The effectiveness of 3 carbohydrases for protein extraction from heat-stabilized defatted rice bran (HDRB) was evaluated. Amylase, viscozyme and celluclast extracted a maximum of 45.4, 12.1, and 28.5% protein, respectively. Further study showed that extracted protein ranged from 9.5 to 58.4% under conditions of water to bran ratio (5:1 to 20:1), α-amylase (0 to 110000 units/10 g rice bran), temperature (35 to 55 °C), and time (1 to 8 h). The maximum protein extracted was 58.4% with a water to bran ratio of 17:1, 87637 units amylase, and 50.9 °C. These results suggest that impure food-grade amylase containing protease is more effective than celluclast and viscozyme in protein extraction from HDRB.     

Minimal forbidden subwords

Motivated by a study of similar problems stated for factors of words, we study forbidden subwords of a language or a word. A procedure for obtaining the set of all words avoiding a given set of subwords is presented. On the other hand, an algorithm for computing the set of minimal forbidden subwords for a word is given. The case of a two-letter alphabet appears to be particularly interesting and it is considered separately.     

芳烃抽提装置技术改造

由于中国石化锦西石化分公司600kt／a连续重整装置的建设，芳烃抽提装置的原料由原来的脱戊烷油变为Ce组分。为此，对抽余油水洗塔和芳烃分离部分的苯塔塔盘，以及苯塔塔顶和塔底抽出部分进行了改造，更换部分机泵和增加变频泵，并将常规仪表改为DCS控制。改造后装置实现一次开车成功，生产出合格产品。抽余油中总芳烃含量小于0．1％，苯回收率达到99%以上。     

石油渣油制备针状焦研究--中间馏分热反应研究

石油渣油的组成复杂,分子量分布宽,直接焦化不能生产针状焦。采用一定的预处理技术将渣油中适宜制备针状焦的组分保留,可获得理想的焦化原料。通过以辽河减压渣油为原料,经溶剂萃取对渣油进行"掐头去尾"处理,获得了分子量分布窄、杂质含量少的中间馏分A及馏分B。对馏分A、B分别进行热反应研究,结果表明:渣油的预处理效果明显,中间馏分热反应产物具有光学各向异性物含量高、取向性好等特点,是制备针状焦的理想原料。     

金的分离富集

综述了金的分离和富集方法，主要包括各种吸附和萃取方法。采用活性炭和泡沫塑料(简称泡塑)吸附分离金是传统的分离富集法，有负载活性炭和有负载泡塑可以提高富集金的能力。近些年，离子交换树脂和离子交换纤维素在分离富集金的应用中，占有相当大的比例。萃取法除了使用传统的MIBK作为萃取剂，又见报道硫醚、亚砜、醇类等作为萃取剂的各种萃取体系。中引用参考献107篇。