Fabrication and characterization of Cu2ZnSnS4 thin films deposited by spray pyrolysis technique

We have investigated synthesis conditions and some properties of sprayed Cu₂ZnSnS₄ (CZTS) thin films in order to determine the best preparation conditions for the realization of CZTS based photovoltaic solar cells. The thin films are made by means of spraying of aqueous solutions containing copper chloride, zinc chloride, tin chloride and thiourea on heated glass substrates at various temperatures. In order to optimize the synthesis conditions of the CZTS films, two series of experiments are performed. In the first series the sprayed duration was fixed at 30 min and in the second it is fixed at 60 min. In each series, the substrate temperature was changed from 553°K to 633°K. The X-ray diffraction shows, on one hand, that the best crystallinity was obtained for 613°K as substrate temperature and 60 min as sprayed duration. On the other hand, these CZTS films exhibit the kesterite structure with preferential orientation along the [112] direction. Atomical Force Microscopy was used to determine the grain sizes and the roughness of these CZTS thin film. After the annealing treatment, we estimated the optical band-gap energy of the CZTS thin film exhibiting the best crystallinity as 1.5 eV which is quite close to the optimum value for a solar cell.     

航空放射性遥感技术应用研究

航空放射性遥感系统采用航空γ能谱仪,在空中飞行探测地表放射性,能够快速进行大面积环境放射性调查。结合已经开始进行的首次大面积航空放射性遥感调查工作,简要介绍了航空放射性遥感系统构成、核探测γ能谱测量和数据处理技术。对系统转换因子刻度和剥离系数刻度方法进行了讨论,并对初步应用情况进行了总结。     

特钢长型材轧制技术新进展

在可持续发展原则指导下，强化控轧控冷、高精度轧制和改进表面与外形质量是当前特钢轧制技术发展的重点。     

Modelling diffusion-controlled kinetics in equilibrium and driven alloys

Summary We introduce a very simple model for thermally activated atomic migration on a lattice, and several techniques to handle it. For thermodynamical systems, the model can be used for simulating decomposition paths taking into account relevant metallurgical features. Close to equilibrium, the simplest mean-field approximation of the model can be linearized with respect to the departure from equilibrium; one then gets a microscopic interpretation of classical phenomenological coefficients, such as mobility, interfacial transfer coefficient, rate constants for the coupled relaxation of concentration and order fields. Further away from the equilibrium, the nonlinearities can be taken into account in a consistent way. For driven alloys, i.e. alloys submitted to external forcing, forced atomic migration is added to the model and new features emerge: the model is supported by several experimental results some of which confirmed its predictions a posteriori.     

Influence of the surface conditions on permeation in the deuterium–MANET system

The condition of the surfaces is of crucial importance for the deuterium permeation through materials. In this work a study of the surface constants for the adsorption (σk₁) and release (σk₂) of deuterium under different surface conditions on the martensitic steel DIN 1.4914 (MANET) has been carried out. The growth of an oxide surface layer (Cr₂O₃) of about 25–30 nm in a MANET sample, heat treated in an oxidizing environment, compared to the bare MANET that have a ‘natural' oxide of about 5 nm has provoked a reduction of both the permeation rate and the recombination coefficient (about 3 orders of magnitude). In addition, the permeation governing process has changed from diffusion-limited to surface-limited. The measurements of the permeation rate of deuterium were performed by a gas-phase permeation technique over the temperature range 574–746 K and for deuterium driving pressures in the range from 3 to 10⁵ Pa.     

我国炼油技术开发的若干思考与建议

分析了我国炼油工业面临的挑战，世界炼油工业的发展趋势，提出了我国炼油技术开发要围绕符合国情的清洁燃料生产技术，炼油与化工结合的炼油技术，适合现有炼油装置技术改造、提高技术水平，降低加工成本的技术，渣油转化技术，煤制油，天然气制油技术，炼油厂智能化的技术，减少炼油厂烟尘排放的技术等7个方面开展工作的具体建议。     

DFMC在水利机械产品开发中的应用研究

分析了DFMC(大规模定制设计)关键技术及相关技术,提出了运用该项技术开发产品企业应作好的前期准备,研究了水利机械产品"大型移动启闭机"的定制开发。     

从76届SEG年会看综合物化探技术的发展方向

文中在介绍76届SEG年会的展商、展台及会场专题报告与论文发布情况的基础上，阐述了参加本届SEG年会的体会，指出了重磁电技术发展的四个趋势：向海洋勘探技术方向发展、向复杂区综合勘探技术方向发展、向三维联合处理和三维可视化解释技术发展、向直接圈定和检测油气方向发展。     

新城金矿采场落矿控制爆破技术

新城金矿为蚀变岩型金矿床,由于受地质构造影响,顶板稳定性较差,局部和较大面积的顶板冒落现象时有发生,为了解决采场顶板安全问题和提高落矿主要技术经济指标而进行了“上向水平分层尾砂胶结充填法采场控制爆破技术”的试验研究工作,试验达到了预期效果。     

Development and implementation of a NURBS curve motion interpolator

This paper deals with the issues of development and implementation of a real-time NURBS interpolator for a six-axis robot. Using an open-architecture controller system as a testbed, a real-time NURBS curve interpolator was developed, implemented and tested. Sample runs were conducted with the resulting trajectories measured in real-time during robot motion. The resulting trajectories are analyzed, discussed and compared with those from a commonly used point-to-point approximation technique. The real-time NURBS curve interpolator's feasibility, advantages and related issues are also discussed.