热塑性弹性体SBS的工程开发Ⅴ．万吨级聚合装置SBS产品的性能剖析

对用国内技术建设的万吨级聚合装置生产的５种牌号产品：线型ＳＢＳ１３０１，ＳＢＳ１４０１和星形ＳＢＳ４３０３，ＳＢＳ４４０２及充油３３％的星形ＳＢＳ４４５２２进行了性能剖析。结果表明，国产ＳＢＳ的物理性质、热氧稳定、玻璃化转变温度、微观结构和相态结构与国外同类产品相当，Ｍ＿ｎ可以达到预期要求，说明该开发技术是成功的。     

基于电力GIS的电网故障监控系统的研究与设计

电网故障监控系统利用故障采集器回传的电参数信息和地理标志信息,通过监控中心对这些信息读取处理后,导入GIS中,在显示器上通过GIS地图显示相关信息。从而帮助调度人员快速准确地发现和了解故障信息,及时制定抢修方案或启动抢修预案,并调度维修人员快速到达现场,可有效提高供电抢修效率,提升客户满意度,具有良好的应用价值。     

网络在线文化信息监控平台建设与服务机制研究

针对高速网络环境下网络文化信息传输内容监控的需要,提出了实现拥有自主版权的能够在边界路由器上监测运行的网络文化信息监控系统的3种设计方法、3个层面的设计思想,以及数据采集结构、模块功能实现、服务机制创新的方法和理念,试图有效监测特征敏感性在线文化信息的来源与去向,创新监控应对策略,提高监控安全事件处理的效能。     

基于网络中控技术的多媒体教室管理与监控系统的应用

设计基于网络中控技术的多媒体教室管理与监控系统,该系统能够将高校各个独立的多媒体教室管理与监控系统关联到一起进行管理,实现集远程管理、监控、维护于一体的应用系统,提高高校多媒体应用水平。     

基于RFID技术的监所巡更系统

介绍一种基于射频卡及读卡器进行软件开发而成的方便实用的监所巡更系统。由PC微机、射频卡及其读卡器等部分组成,完成巡更资料的采集、传输、管理等功能。该统既可以加强对监所的管理,又可以省去管理人员检查的麻烦,同时也适应各监所逐步普及计算机管理、提高管理水平的要求,具有很好的实用和推广意义。     

室温固相合成掺杂ZnO纳米粉体制备ZnO压敏电阻

以金属离子盐和草酸为原料,采用室温固相化学反应合成掺杂ZnO前驱物,根据DSC-TG分析结果,将其在450℃热分解2 h,得到掺杂ZnO粉体,并用此粉体制备了片式ZnO压敏电阻。借助XRD、TEM、BET等检测手段对粉体产物的物相、形貌、粒度等进行了表征。研究了烧结温度对ZnO压敏电阻电性能的影响。结果表明,所制备的粉体为平均粒径24 nm左右、颗粒呈球状、分散性好的纤锌矿结构掺杂ZnO。在1 080℃烧结时,ZnO压敏电阻的综合电性能达到最佳,电位梯度为791.64 V/mm,非线性系数为24.36,漏电流为43μA。     

Synthesis,characterization, and thermal behavior study of methyl methacrylate polymers containing 4‐carbazole substitutes

A new polymerizable monomer, [4‐(9‐ethyl)carbazolyl]methyl methacrylate ( 2 ), was synthesized by reacting of methacrylic acid and 4‐hydroxymethyl‐9‐ethyl carbazole ( 1 ) by esterification procedure in the presence of N,N′‐dicyclohexylcarbodiimide. The resulting monomer was then polymerized free‐radically to form the poly(methyl methacrylate) containing 4‐(9‐ethyl)carbazolyl pend ent groups. Also, copolymerization of monomer 2 with various acrylic monomers such as methyl methacrylate, ethyl methacrylate, methyl acrylate, ethyl acrylate, and n‐butyl acrylate by azobisisobutyronitrile as a free radical polymerization initiator gave the related copolymers in high yields. The structure of all the resulted compounds was characterized and confirmed by FTIR and ¹H NMR spectroscopic techniques. The average molecular weight of the obtained polymers was determined by gel permeation chromatography using tetrahydrofurane as the solvent. The thermal gravimetric analysis and differential scanning calorimeter instruments were used for studying of thermal properties of polymers. It was found that, with the incorporation of bulky 4‐(9‐ethyl)carbazolyl substitutes in side chains of methyl methacrylate polymers, thermal stability and glass transition temperature of polymers are increased. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 4989–4995, 2006     

A novel synthesis method for the preparation of aromatic poly(imide benzoxazole) from trimellitic anhydride chloride and bis(o‐aminophenol)

A poly(imide benzoxazole) was prepared directly from trimellitic anhydride chloride and 2,2‐bis(3‐amino‐4‐hydroxyphenyl)hexafluoropropane (BisAPAF) monomers in a two‐step method. In the first step, a poly(hydroxyamide amic acid) precursor was synthesized by the low‐temperature solution polymerization in an organic solvent. Subsequently, thermal cyclodehydration of the poly(hydroxyamide amic acid) precursor at 350°C produced the corresponding poly(imide benzoxazole). The inherent viscosity of the precursor polymer was 0.22 dL/g. The cyclized poly(imide benzoxazole) showed a glass transition temperature (T_g) at 329°C and a 5% weight loss temperature at 530°C in nitrogen and at 525°C in air. The poly(imide benzoxazole) is amorphous as evidenced by the wide‐angle X‐ray diffraction measurement. The structures of the precursor polymer and the fully cyclized polymer were characterized by Fourier transform infrared (FTIR) and proton nuclear magnetic resonance spectroscopy (¹H NMR). © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 88: 2388–2391, 2003     

个人剂量无线监测装置的研制

本文提出了一种基于无线功能的个人剂量核辐射监测.旨在对辐射工作区域的工作人员提供辐射剂量的实时监测.该系统采用射频通信传输技术,将工二人所受的辐射剂量、剂量率和受照时间等数据发送至监控中心,以方便自动数据存储和分析.同时及时有效的预警,可避免工作人员超剂量受照的风险,对辐射环境卫生领域的深入研究也有重要的参考价值.     

连续退火炉板温控制策略讨论

结合退火炉内带钢辐射率的变化,通过对几种板温控制方案的研究比较,分析各种控制方案的优缺点,对以后更好实现板温的精确控制起一定指导作用.