Fabrication of nano-porous silicon oxide layers by plasma polymerisation methods

We report on the synthesis of nano-porous silicon oxide (SiO₂) layers by gas phase polymerisation reactions of hexamethy disiloxane and oxygen. The SiO₂ layers are deposited onto one or more layers of poly(methylmethacrylate) (PMMA) particles spin coated onto the substrate surface. Subsequent annealing of the films to high temperature (500 °C) leads to the pyrolysis of the polymeric particles resulting in a 3D nanoporosity in the film. X-ray Photoelectron (XPS) and Fourier Transform Infra Red Spectroscopy (FTIR) show an SiO₂-like surface chemistry and virtually complete removal of the organic components. These materials offer a very high surface area-to-volume ratio suitable for sensing applications.     

A critical transition state in liquid metals

Temperature dependence of viscosities of liquid Sn, Cu, Pb_38.1Sn_61.9, Pb_44.8Bi_55.2, and Cu_0.7Sn_99.3 has been studied by a torsional oscillation viscometer. During the measurement process, a deviation from the Arrhenius behavior is found when the temperature is lowered to about 60 K higher than the melting point. The abnormal increasing of the viscosity and the activation energy indicates the changes of the elementary melt structure during cooling towards the melting point. The deviation region from Arrhenius viscosity is defined as the transition state. The differential scanning calorimeter experiments also show the existence of the critical transition state in liquid metals near the melting point. The drastic increase of the viscosity in the transition state can be regarded as continuum transition and be presented well by the amended Arrhenius equation which is based on the critical phenomenon.     

α-Fe_2O_3(SO_4~(2-),Sn)气敏电阻的温度响应特性

在气敏温度区域内研究了α-Fe_2O_3(SO_4~(2-),Sn)材料的电阻-温度特性,认为表面结构的变化导致温度特性出现峰值并呈现气敏性。可利用空气中电阻温度特性提供的信息改性或发现新的气敏材料。     

Synthesis and two-photon absorption property of new π-conjugated dendritic fluorophores containing styrylpyridyl moieties

Four new multi-branched two-photon absorption chromophores, namely 1-(4-bromobenzal)-3,5-bis(4-((E)-2-(pyridin-4-yl)vinyl)phenyl)benzene (4), tris(4-((E)-2-(pyridin-4-yl)vinyl)phenyl)-benzene (5), 6-chloro-N²,N⁴-bis(4-((E)-2-(pyridin-4-yl)vinyl)phenyl)-1,3,5-triazine-2,4-diamine (6), tris-[4-(2-pyridin-4-yl-vinyl)-phenyl]-amine (7), have been synthesized and characterized. One-photon fluorescence, fluorescent quantum yields and two-photon fluorescence have been investigated. The experimental two-photon absorption cross-sections of 4–7 in DMF are 6, 11, 13 GM (pumped by 740 nm laser) and 19 GM (pumped by 800 nm laser), respectively. The calculated two-photon absorption cross-sections of 4–7 are 5.41, 7.67, 9.57 and 76.14 GM, respectively. The two-photon induced fluorescent peak wavelengths of 4–7 in DMF are 421, 425, 474 and 534 nm pumped by 680, 680, 740 and 800 nm laser, respectively. The results show that molecule 7 is a good two-photon absorption fluorophore possessing long two-photon fluorescent lifetime, good fluorescent quantum yield and large two-photon absorption cross-section. The two-photon absorption peak wavelength of molecule 7 is at 800 nm, which is favourable for initiating two-photon photopolymerization.     

Verification of humans using the electrocardiogram

A feasibility study on the potential of the electrocardiogram (ECG) for biometrical applications is presented. A test set of 234 ECG recordings from 74 subjects was compiled emulating a realistic scenario for ECG biometrics by using short measurements of 10 s length in combination with a practicable choice of ECG leads. The long-term stability of the individual ECG was investigated during time periods up to several years. Verification and identification was done by utilizing the heart vector and a simple distance measure. As a result, encouraging error rates were obtained; for verification, for instance, the achieved equal error rate was smaller than 3%.     

论新时期油田企业医院思想政治工作

随着医院内部管理体制改革的不断推进,医务人员的主人翁思想有所动摇,价值观发生了变化,服务理念跟不上现实的要求。针对这些问题,应该处理好"疏"与"堵"的关系、"实"与"虚"的关系。努力做好以下三点工作:1、把握人的行为规律,体现科学性;2、抓住职工结构新特点,体现针对性;3、解决实际问题,体现实效性。同时抓好四个结合:即思想政治工作与医疗业务工作的结合;思想政治工作与解决职工实际问题的结合;思想政治工作与职业道德建设的结合;思想政治工作与文化建设的结合。     

基于虚拟技术的单闭环直流调速系统的研究

本文建立了他励直流电动机虚拟模型,通过模型进行仿真算法分析,并利用虚拟技术,在仿真平台上实现仿真,在上位机上显示数据,对单闭环直流调速系统进行可行性研究与优化。仿真做的主要前期工作为模型建立,通过电枢回路方程和动力方程进而推导出电动机的数学模型方程,并对模型进行分析计算。后期工作对所建立的模型进行仿真,并调试出模型数据,进而得到仿真结果。设计的虚拟模型建立在虚拟仿真平台上,利用平台的模拟和数字输入输出端口进行信号的采集和传递,并利用仿真平台强大的内部资源进行运算分析,从而达到期望的研究效果。     

高校门户网站Banner的“图说＂功能研究

在高校门户网站中,“图说”功能是Banner自身具有的网络广告属性的直观体现,使Banner具有页面装饰和信息传递的双重效果,极大地提升网站的视觉吸引力,是网站主页重要位置的典型设计应用。进行高校门户网站Banner设计,可选用学校各类主题图片,配合简洁文案,形成图文专题,发挥“图说”功能。还要注重Banner信息的采集和更新,建立专业维护团队,建设完善运行机制,来确保Banner“图说”功能的精彩呈现。     

风机冷风保安控制系统优化

介绍菜钢型钢AV80风机冷风保安控制系统的优化改造,以增加其控制安全性及可靠性.