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1.
A. J. Slifka T. Hall E. S. Boltz 《Journal of research of the National Institute of Standards and Technology》2003,108(2):151-156
A simple measurement system is described for evaluating damage to graphite-epoxy panels, such as those used in high-performance aircraft. The system uses a heating laser and infrared imaging system to measure thermal performance. Thermal conductivity or diffusivity is a sensitive indicator of damage in materials, allowing this thermal measurement to show various degrees of damage in graphite-epoxy composites. Our measurements track well with heat-flux damage to graphite epoxy panels. This measurement system, including analysis software, could easily be used in the field, such as on the deck of an aircraft carrier or at remote air strips. 相似文献
2.
M.A.R. Alves 《Microelectronics Journal》2005,36(1):51-54
We developed a process to obtain sharper silicon tips by employing anisotropic etching in a KOH solution followed by SF6 plasma etch. The tips were further sharpened using the established thermal oxidation technique to decrease the cone angle and, therefore, obtain smaller curvature radii. We have analyzed the impact of such changes in geometry on a figure of merit associated with the field emission characteristics. An increase in the figure of merit by a factor of three was found in relation to the tips before sharpening. 相似文献
3.
Using the photonic band gap in photonic crystals, the fundamental waveguide structures for the light wavelength range have been developed. Based on the fine structure of these many functional devices have been proposed by analytical or numerical simulation methods and the experiments of trial manufacture. In this paper, the treatment of chiral dielectric in the Condensed Node Spatial Network for the vector potential is explained, and we show the polarization plane rotation property in air‐hole and pillar type photonic crystal waveguide structures with the chiral medium substrate. Then, we show the fundamental advantage of the air‐hole type photonic crystal waveguide structure in application to a mode converter. © 2005 Wiley Periodicals, Inc. Electr Eng Jpn, 152(1): 7–14, 2005; Published online in Wiley InterScience ( www.interscience. wiley.com ). DOI 10.1002/eej.20098 相似文献
4.
5.
A. Domingue K. Piyakis E. Sacher M. Di Renzo S. D nomm e T. H. Ellis 《The Journal of Adhesion》1993,40(2):151-162
The irreversibly bound interfacial layer deposited by the γ-aminopropysilanetriol adhesion promoter onto a crystalline silicon substrate, which remains even after profuse washing, was found by XPS to have resulted from the fragmentation and rearrangement of the original γ-aminopropylsilanetriol molecule. A mechanism is proposed, involving the homolytic scission of the terminal N-C bond. One of the subsequent reactions is believed to involve hydrogen loss by abstraction and the formation of a terminal vinyl group, which bonds to the substrate. Support for this mechanism is found in IR spectroscopy of this layer. 相似文献
6.
Zinc Coated Steel/Epoxy Adhesive Systems: Investigation of the Interfacial Zone by FTIR Spectroscopy
The present study takes advantage of the ability of Fourier Transform Infrared Spectroscopy (FTIR) for the analysis of ultrathin organic films on metals. FTIR in the reflection mode (IRRAS) is used in order to study the interaction of ultrathin films of dicyandiamide (hardener of most one-pack epoxy resins) with various substrates, model ones such as gold or zinc and industrial ones such as steel and zinc-coated steels.
Pure zinc surfaces and, to a lesser extent, zinc-coated steels are shown to react with dicyandiamide after heating at 180°C, as evidenced by the frequency shift of the absorption band (at about 2200 cm-1) characteristic for nitrile groups. As real systems consist of thick layers of a fully formulated adhesive cured onto a metallic substrate, the direct investigation of such a buried interphase is no longer possible by FTIR and by most of the known spectroscopies. Some mechanically tested specimens are then analysed, after failure, by FTIR microspectrometry. The spectra obtained, corresponding to the fracture initiation zone which is about 100 μm in diameter, advocate for the presence of an ultrathin layer of modified polymer still covering the substrate. 相似文献
Pure zinc surfaces and, to a lesser extent, zinc-coated steels are shown to react with dicyandiamide after heating at 180°C, as evidenced by the frequency shift of the absorption band (at about 2200 cm-1) characteristic for nitrile groups. As real systems consist of thick layers of a fully formulated adhesive cured onto a metallic substrate, the direct investigation of such a buried interphase is no longer possible by FTIR and by most of the known spectroscopies. Some mechanically tested specimens are then analysed, after failure, by FTIR microspectrometry. The spectra obtained, corresponding to the fracture initiation zone which is about 100 μm in diameter, advocate for the presence of an ultrathin layer of modified polymer still covering the substrate. 相似文献
7.
Mine overburden dumps have posed significant safety issues in the operations of various unit operations of open pit min-ing especially the external dumps. The external dumps are composed of a mixture of fragmented rocks and loose soil. Their charac-teristic is comparable to heavily discontinuous solid mass. The conventional approach of limit equilibrium methods provide safety factors for the slope but nothing about the stress-strain characteristics of the large dump mass. The designs of dump location and their respective geometry are integrated for the know-how of the stability characteristics of these dumps. The discrete element method uses a circular disk to represent the granular solid mass and their interactions are described by the Newton's third law of motion. The displacement is described by the sliding of the circular disk. This work is focused on the modeling efficiency of the discrete element methods to represent the behaviour of mine dump masses with the specified joint plane for the limit equilibrium method. The advantage of the work lies on the ease of information retrieval at any point at the dump mass concerning the stress and strain histories, displacement, failures etc. which when integrated produces a better understanding of the stability of the dump masses. 相似文献
8.
J. H. Li P. Deshpande R. Y. Lin 《Journal of Materials Engineering and Performance》2004,13(4):445-450
The objective of this study is to investigate an innovative infrared (IR) technique to enhance adhesion of electroplated copper
(Cu) on Ti-6Al-4V without dichromate dipping. The ultimate goal is to develop a Cu coating process on Ti-6Al-4V without hazardous
hexavalent chromium (Cr) solution treatments. Cu coatings of around 50 μm were electroplated on Ti-6Al-4V specimens at a current
density of 0.03 A/cm2 in an acidic Cu solution. To improve adhesion of coatings, IR heat treatments were performed on the Cu-coated samples at
different temperatures and durations: 860 °C for 600 s and 875 °C for 20–120 s. This process was accomplished in an attempt
to replace the use of dichromate dipping before electroplating. For samples heat treated at 860 °C, no bonding existed, even
after 600 s. It is believed that solid-state diffusion prevailed at 860 °C and that 600 s was not enough for sufficient diffusion
to occur. Adhesion was poor when samples were heat treated at 875 °C for 20 s. Excellent adhesion was observed when the heat
treatment holding time was increased to 40 s. For 90 s, the surface appearance of coatings partially changed from Cu-colored
to a grayish color. There was no Cu left on the surface after a 120 s heat treatment. From optical microscopic observations
on sample cross sections, an interlayer between the Cu and Ti-6Al-4V formed when heat treated at 875 °C for 40 s and longer.
The interlayer thickness increased as the holding time increased, until depletion of Cu. The sheet resistivity of coated specimens
was on the order of pure Cu for samples heat treated at 875 °C and less than 90 s. During the 875 °C heat treatment, the following
occurred: solid-state diffusion of Cu in Ti-6Al-4V, formation of eutectic solutions, dissolution of Cu and Ti-6Al-4V into
the liquid phase, and the formation of intermetallic compounds. The lowest eutectic temperature of 875 °C played a key role
in this innovative process of Cu coating on Ti-6Al-4V.
This paper was presented at the 2nd International Surface Engineering Congress sponsored by ASM International, on September
15–17, 2003, in Indianapolis, Indiana and appears on pp. 403–10 of the Proceedings. 相似文献
9.
INFORMATIONDESIGNOFUNIVERSALADJUSTMENTPROGRAMOFPLANECONTROLNETWORKSINFORMATIONDESIGNOFUNIVERSALADJUSTMENTPROGRAMOFPLANECONTRO... 相似文献
10.
Radiometric normalization and image mosaic generation of ASTER thermal infrared data: An application to extensive sand sheets and dune fields 总被引:1,自引:0,他引:1
Data from the Advanced Spaceborne Thermal Emission and Reflection Radiometer (ASTER) have a significant advantage over previous datasets because of the combination of high spatial resolution (15-90 m) and enhanced multispectral capabilities, particularly in the thermal infrared (TIR) atmospheric window (8-12 μm) of the Earth where common silicate minerals are more easily identified. However, the 60 km swath width of ASTER can limit the effectiveness of accurately tracing large-scale features, such as eolian sediment transport pathways, over long distances. The primary goal of this paper is to describe a method for generating a seamless and radiometrically accurate ASTER TIR mosaic of atmospherically corrected radiance and from that, extract surface emissivity for arid lands, specifically, sand seas. The Gran Desierto in northern Sonora, Mexico was used as a test location for the radiometric normalization technique because of past remote sensing studies of the region, its compositional diversity, and its size. A linear approach was taken to transform adjacent image swaths into a direct linear relationship between image acquisition dates. Pseudo-invariant features (PIFs) were selected using a threshold of correlation between radiance values, and change-pixels were excluded from the linear regression used to determine correction factors. The degree of spectral correlation between overlapping pixels is directly related to the amount of surface change over time; therefore, the gain and offsets between scenes were based only on regions of high spectral correlation. The result was a series of radiometrically normalized radiance-at-surface images that were combined with a minimum of image edge seams present. These edges were subsequently blended to create the final mosaic. The advantages of this approach for TIR radiance (as opposed to emissivity) data include the ability to: (1) analyze data acquired on different dates (with potentially very different surface temperatures) as one seamless compositional dataset; (2) perform decorrelation stretches (DCS) on the entire dataset in order to identify and discriminate compositional units; and (3) separate brightness temperature from surface emissivity for quantitative compositional analysis of the surface, reducing seam-line error in the emissivity mosaic. The approach presented here is valid for any ASTER-related study of large geographic regions where numerous images spanning different temporal and atmospheric conditions are encountered. 相似文献