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1.
From chloromethylated polyimide, a useful starting material for modification of aromatic polyimides, a thermocurable transparent polyimide having acrylate side groups was prepared. In the presence of 1,8‐diazabicyclo[5,4,0]undec‐7‐ene, chloromethylated polyimide was esterified with acrylic acid to synthesize poly(imide methylene acrylate). The polymer was soluble in organic solvent, which makes it possible to prepare a planar film by spin coating. The polymer film became insoluble after thermal treatment at 230 °C for 30 min. Optical transparency of the film at 400 nm (for 1 µm thickness) was higher than 98 % and not affected by further heating at 230 °C for 250 min. Adhesion properties measured by the ASTM D3359‐B method ranged from 4B to 5B. Preliminary results of planarization testing showed a high degree of planarization (DOP) value (>0.53). These properties demonstrate that poly(imide methylene acrylate) could be utilized as a thermocurable transparent material in fabricating display devices such as TFT‐LCD. Copyright © 2004 Society of Chemical Industry  相似文献   
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We analyze specific features of the design of equipment used for mechanical testing of sheet structural materials under the conditions of biaxial static, cyclic, or dynamic loading. We propose original solutions of the problems related to the fatigue testing of crosslike specimens performed without using complex hydraulic systems and their dynamic testing carried out by using very simple testing machines for uniaxial tension–compression.  相似文献   
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A one–dimensional, transient thermal degradation heat transfer model for the response of composite materials when exposed to fire is presented. The model can handle layers of different materials. Material properties are functions of temperature. The reaction can be specified using Arrhenius‐type parameters or by inputting a density–temperature relationship determined by any experimental technique such as thermogravimetric analysis. The model is validated against the experimental data presented in Boyer's 1984 dissertation. Overall, the model provides excellent agreement with the experimental data. It is shown that very little difference is found between results arrived at by Arrhenius kinetics and results obtained by specifying the easier to measure density–temperature relationship. From this it is concluded that this technique is a viable alternative to Arrhenius‐type models. Copyright © 2006 John Wiley & Sons, Ltd.  相似文献   
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This paper describes the synthesis of photoisomerizable derivatives of isosorbide. These derivatives contain a stilbene or cinnamate moiety and can therefore be used as photoisomerizable chiral compounds in cholesteric liquid‐crystalline mixtures. The reflection wavelength of cholesteric layers made from these mixtures is increased by UV irradiation due to the fact that the Z‐isomers of these derivatives exhibit a lower helical twisting power than the corresponding E‐isomers. The cinnamate derivatives are very suitable for use in cholesteric color filters that find application in liquid‐crystal displays.  相似文献   
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部分种子成分的特征X射线在等效生物材料中衰减的测定   总被引:6,自引:5,他引:1  
韩光武  卫增泉 《核技术》1995,18(10):615-620
用Si(Li)探测器实现了Na、Mg、S、Cl的特征X射线在有机膜中的相对衰减以及与O、K元素的特征X射线能量相当的X射线或轫致辐射在有机膜中的相对衰减,分别得出了它们减的数学描述,并把实验得到不同能量的X射线在有机膜中的质量吸收系数与Berkeley的OCG软件计算出的结果相比,相关都小于30%。  相似文献   
9.
This two-part paper presents a closed-form procedure for evaluation of estimates of local thermomechanical stress fields in two-phase fibrous composites and laminates. The first part is concerned with a unidirectional elastic laminate subjected to uniform mechanical loads and to uniform changes in temperature. Both phases are assumed to be elastic, with temperature-dependent moduli and expansion coefficients; the solution reflects the influence of thermomechanical interactions. Exact solutions are not possible for any real system, because the local geometry is not known in detail. Instead, estimates of the fields are found from a modified Mori-Tanaka approximation. Examples are presented for two SiC/Ti---Al---Nb composites. Local stresses of interest are found after cooling from fabrication to room temperature. The presence of local yielding, and the influence of coupling terms on the local stress magnitudes are examined. Extension of the results to laminated plates is presented in Part II (Dvorak, G.J., Chen, T. & Teply, J., Composites Science and Technology, 43 (1992) 359–368, this issue).  相似文献   
10.
Intensional negative adjectives alleged , artificial , fake , false , former , and toy are unusual adjectives that depending on context may or may not be restricting functions. A formal theory of their semantics, pragmatics, and context that uniformly accounts for their complex mathematical and computational characteristics and captures some peculiarities of individual adjectives is presented.
Such adjectives are formalized as new concept builders, negation‐like functions that operate on the values of intensional properties of the concepts denoted by their arguments and yield new concepts whose intensional properties have values consistent with the negation of the old values. Understanding these new concepts involves semantics, pragmatics and context‐dependency of natural language. It is argued that intensional negative adjectives can be viewed as a special‐purpose, weaker, conntext‐dependent negationin natural language. The theory explains and predicts many inferences licensed by expressions involving such adjectives. Implementation of sample examples demonstrates its computational feasibility. Computation of context‐dependent interpretation is discussed.
The theory allows one to enhance a knowledge representation system with similar concept building, negation‐like, context‐dependent functions, the availability of which appears to be a distinct characteristic of natural languages.  相似文献   
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