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1.
J. Gegner 《Materialwissenschaft und Werkstofftechnik》2003,34(3):290-297
Chemical Composition and Microstructure of Polymer‐Derived Glasses and Ceramics in the Si–C–O System. Part 2: Characterization of microstructure formation by means of high‐resolution transmission electron microscopy and selected area diffraction Liquid or solid silicone resins represent the economically most interesting class of organic precursors for the pyrolytic production of glass and ceramics materials on silicon basis. As dense, dimensionally stable components can be cost‐effectively achieved by admixing reactive filler powders, chemical composition and microstructure development of the polymer‐derived residues must be exactly known during thermal decomposition. Thus, in the present work, glasses and ceramics produced by pyrolysis of the model precursor polymethylsiloxane at temperatures from 525 to 1550 °C are investigated. In part 1, by means of analytical electron microscopy, the bonding state of silicon was determined on a nanometre scale and the phase separation of the metastable Si–C–O matrix into SiO2, C and SiC was proved. The in‐situ crystallization could be considerably accelerated by adding fine‐grained powder of inert fillers, such as Al2O3 or SiC, which permits effective process control. In part 2, the microstructure is characterized by high‐resolution transmission electron microscopy and selected area diffraction. Turbostratic carbon and cubic β‐SiC precipitate as crystallization products. Theses phases are embedded in an amorphous matrix. Inert fillers reduce the crystallization temperature by several hundred °C. In this case, the polymer‐derived Si–C–O material acts as a binding agent between the powder particles. Reaction layer formation does not occur. On the investigated pyrolysis conditions, no crystallization of SiO2 was observed. 相似文献
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This article is the second of two papers that review the field of spatially sensitive social scientific research into the links between social status and transport disadvantage. The first paper undertook a comprehensive review of the social scientific and transport planning literature to mark the level of development in the field and identify conceptual and methodological issues and constraints in this field of inquiry. The present article supports the advancement of socially and geographically sensitive transport research by opportunities for the development of more sophisticated spatial analytical methodologies. The approach we present is able to account for factors not previously addressed in either social or transport planning research, in particular the temporal dimensions of transport service accessibility. The article articulates the methodology through an empirical case study of socio-spatial transport disadvantage within the Gold Coast City. The article demonstrates that there are important theoretical and practical lessons to be gained for researchers and policy makers in addressing the social dimensions of transport and infrastructure provision. Further, the article argues that an attentiveness to new ways of combining and representing social and transport data-sets can promote policy relevant empirical social inquiry. The article also contributes in a productive way to the empirical knowledge of Australia's sixth-largest metropolitan area, which is often overlooked by urban scholars. 相似文献
4.
Tatsuro Kijima Kouji Ohshima Hideo Kise 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》1994,59(1):61-65
Racemic amino acid esters were optically resolved via hydrolysis in organic solvents by the catalysis of an industrial alkaline protease, “Alcalase”. The products which were composed mainly of L-amino acids were insoluble and easily separated by filtration. The activity of the enzyme and enantiomeric excess of the products were significantly dependent on the nature of solvent and the water content in the reaction media. Generally, high values of enantiomeric excess were obtained at low water contents. Many natural and unnatural amino acids were resolved by this method. 相似文献
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Using the photonic band gap in photonic crystals, the fundamental waveguide structures for the light wavelength range have been developed. Based on the fine structure of these many functional devices have been proposed by analytical or numerical simulation methods and the experiments of trial manufacture. In this paper, the treatment of chiral dielectric in the Condensed Node Spatial Network for the vector potential is explained, and we show the polarization plane rotation property in air‐hole and pillar type photonic crystal waveguide structures with the chiral medium substrate. Then, we show the fundamental advantage of the air‐hole type photonic crystal waveguide structure in application to a mode converter. © 2005 Wiley Periodicals, Inc. Electr Eng Jpn, 152(1): 7–14, 2005; Published online in Wiley InterScience ( www.interscience. wiley.com ). DOI 10.1002/eej.20098 相似文献
7.
改进粒子群算法的动态空间调度方法 总被引:1,自引:0,他引:1
针对船体分段生产调度的多目标性和动态性,提出了一种改进粒子群算法的动态空间调度方法,确定船体分段在工作平台上的加工顺序和空间布局位置.算法以加工完成时间最短和空间利用率最高为目标,采用自适应惯性权重策略保证算法的收敛性,并引入遗传算法中的选择算子和变异算子增强算法的收敛速度和多样性,利用启发式定位策略确定分段的位置.最后,以船厂实际生产数据进行仿真验证.仿真结果表明,所提方法可以大大降低以手工方式制定调度计划的复杂度,并能有效地提高空间利用率达到70%,说明该方法是解决动态空间调度问题的一种有效方案. 相似文献
8.
基于MRIO与SNA的中国水资源空间转移网络分析 总被引:2,自引:0,他引:2
基于2002年、2007年和2012年的多区域投入产出表的相关数据,利用多区域投入产出(MRIO)模型和社会网络分析法(SNA)分析了中国水资源流动网络的空间关联性和结构特征。结果表明:网络中的链接数量没有随水足迹贸易值的增加而增加,链接路径上的流量不断增加,网络的韧性不够,空间关联渠道有待拓展,存在一定的等级差异,稳定性需要加强;网络中一些省份链接的增加,会削弱其他省份的链接数目,这种可塑性特征有利于在全国范围内合理配置水资源;将网络划分为4个板块,板块间的溢出关系主要是以板块内部为主,且少数板块之间没有任何的溢出关系。 相似文献
9.
通过产业集聚的EG指数对中国各省份信息服务业的空间集聚程度进行研究,得出集聚程度比较显著.在此基础上,找到这一服务业的两个相关指标,利用产业集中度CRn判断出信息服务业主要集中于北京、广东等六个地区,然后对两指标数据进行无量纲化处理,加权求和得到新的综合指标,最后对这一新指标进行了系统聚类分析,得知这一产业主要集中在北京和广东两个地区. 相似文献
10.
空间网络是空地一体化组网中地面网络延伸的重要组成部分。针对空间网络为移动星座的场景,传统的空地一体化组网模型将空间网络视为独立自治域,利用边界网关协议将空间网络与地面自治域互联起来,最大化同地面网络保持兼容。然而,传统组网模型存在边界网关面临频繁会话中断或大量路由更新等问题。通过重新审视空间网络的角色定位和边界划定问题,提出一种面向空地一体化组网的体系架构Slink。Slink的核心思想是空间网络为地面网络提供互联通道,利用星地网关隔离空地两网间的路由更新。实验仿真表明,Slink体系架构能够有效减小对空间路由器的路由存储空间需求,降低星地网络间的带宽消耗。 相似文献