Influence of initial textures on dynamic recrystallization and textures in AZ31 magnesium alloys

1　INTRODUCTIONMagnesiumisthelightestmetallicstructurema terialwithhighspecificstrengthandthereforeiswidelyusedinautomotive ,electronicsandaerospaceindustries[1,2 ] .However ,magnesiumoftenshowsinsufficientplasticityatroomtemperatureduetoitsHCPstructurewithlessindependentsystemsofbasalslip .Toenhanceformabilityofmagnesium ,ahigherdeformingtemperatureisusuallyusedwithtwopur poses .Thefirstistoactivatenewslipsystemsbesidesbasalslip ,sothatmorethanfiveindependentslipsystemscanbeprovided ,be…     

The Effects of Aging Precipitation on the Recrystallization of CuNiSiCr Alloy

The interaction between precipitation and recrystallization and its effect on the properties of the Cu-Ni-Si-Cr alloy during aging were discussed. The results show that the deformation results in much more dispersed precipitation of the phases. The precipitations have accelerating or retarding effects on the recrys allization. On the formation and growth of recrystallization, the precipitated phases are coarsed or dissolved in front of grain boundaries following a re-precipitation in the recrystallization area.     

Effect of Hot Band Annealing on Magnetic Properties in 3% Si Grain‐oriented Electrical Steels

Hot band annealing is known to be a prerequisite for good magnetic properties irrespective of manufacturing methods in grain‐oriented Fe‐3 wt.% Si electrical steels. In this study, the effects of hot band annealing on magnetic properties were investigated in 3% grain‐oriented electrical steels of low soluble AI contents and one‐stage cold rolling. Microstructure and precipitate distribution were compared with hot band annealing conditions. Secondary recrystallization behaviour with hot band annealing condition was also discussed.     

Formation of structure of the CdTe film, recrystallized on Mo/glass substrate under high temperature and mechanical pressure

Large-grained and 7 μm thick CdTe film has been fabricated on top of Mo coated soda-lime glass substrate. As a new approach the dynamic recrystallization process (DRC) was used to form the structure of films. For the characterization of the structure and composition of the films a scanning electron microscopy (SEM), energy dispersive X-ray microanalysis (EDS) and X-ray diffraction (XRD) methods were used. The changes in the structure of films were studied in accordance with the process temperature, pressure and as-deposited film thickness. Significant changes in the CdTe film were observed after DRC of deposited films at the process temperatures between 450 °C and 550 °C. EDS quantitative analysis showed that during the recrystallization the Mo and CdTe films composition remained stable for all studied samples. The XRD results showed that the increase in the process temperature caused improvement in orientation of the films along direction of (111). The DRC temperature above 550 °C reduced the orientation again. The limits of the temperature and pressure in application of soda-lime glass in DRC were found and discussed.     

Recrystallization Behavior of Deformed Austenite in High Strength Microalloyed Pipeline Steel

 Using methods of single hit hot compression and stress relaxation after deformation on a Gleeble 1500D thermomechanical simulator, the curves of flow stress and stress relaxation, the microstructure and the recrystallization behavior of Nb V Ti high strength microalloyed low carbon pipeline steel were studied, and the influence of the thermomechanical treatment parameters on dynamic and static recrystallization of the steel was investigated. It was found that microalloying elements improved the deformation activation energy and produced a retardation of the recrystallization due to the solid solution and precipitation pinning. The deformation conditions such as deformation temperature, strain, and strain rate influenced the recrystallization kinetics and the microstructure respectively. Equations obtained can be used to valuate and predict the dynamic and static recrystallizations.     

Deformation band and texture of a cast Mg-RE alloy under uniaxial hot compression

Microstructural evolution and texture of a cast Mg-9Gd-4Y-0.6Zr ingot under hot compression were studied in this paper. Post-deforming microstructures were characterized by optical microscopy, scanning electron microscopy and transmission electron microscopy, while crystallographic orientation information was obtained from X-Ray macro-texture measurement and EBSD micro-texture analysis. Dynamic recrystallization (DRX) initiated from the deformation bands (DB) forming on original grain boundaries; the DB became widen with continuously conversion of low-angle-boundary grains into high-angle-boundary grains. The tendency of strain localization increased with Z parameter. The macro-texture analysis indicates that uniaxial compression yielded out the randomized basal texture component. This texture component was found to be strengthened with increasing Z parameter. The micro-texture analysis shows that the deviation from the ideal basal texture arose from orientated growth within DBs. Moreover, the localization deformation promoted dynamic precipitation within DBs, which inhibited the development of DRX.     

Modeling of Mechanical Characteristics in Hot Deformation of 4130 Steel

In this investigation, hot compression tests were performed at 900 °C ? 1100 °C and strain rate of 0.001 ? 0.1 s^?1 to study hot deformation behavior and flow stress model of 4130 steel. Based on the classical stress–dislocation relations and the kinematics of the dynamic recrystallization, the flow stress constitutive equations of the work hardening‐dynamical recovery period and dynamical recrystallization period were established for 4130 steel, respectively. The validity of the model was demonstrated by comparing the experimental data with the numerical results. The agreement of this comparison is quite reasonable.     

激光快速成形Inconel 718超合金拉伸力学性能研究

研究了激光快速成形Inconel 718超合金试样3个相互垂直方向的拉伸力学性能,以及热处理对激光快速成形凝固组织与3个相互垂直方向拉伸力学性能的影响。结果表明,激光快速成形Inconel 718超合金试样3个相互垂直方向的拉伸力学性能均明显低于其锻件拉伸力学性能,且表现出明显的各向异性。经过热处理的Inconel 718超合金试样,其沿沉积高度方向定向外延生长的柱状枝晶组织转变为晶粒粗大且不均匀的等轴状再结晶组织,随Laves相固溶消失及强化相γ″和γ′大量析出,3个相互垂直方向上的拉伸力学性能均大幅度提高,其中,与基板平行的两个相互垂直方向上的拉伸力学性能均达到Inconel 718超合金锻件拉伸力学性能标准,但沿成形件高度方向,出现拉伸力学性低于Inconel 718超合金锻件拉伸力学性能标准的试样。     

低碳冲压钢板静态再结晶行为的研究

利用背散射电子衍射(EBSD)技术和X射线衍射(XRD)对SPCD冷轧钢板缓慢升温退火工艺下的再结晶取向特征、织构的形成规律及与形变织构的关系进行研究,并与快速加热退火工艺下的IF钢再结晶取向特点进行对比。结果表明:宏观织构显示冷轧态下{111}〈112〉形变织构稳定存在,随后的再结晶过程中γ线上存在{111}〈112〉与{111}〈110〉织构的竞争,其中再结晶初期{111}〈112〉织构占主导,后期{111}〈110〉吞食{112}〈110〉和{001}〈110〉织构进而取代{111}〈112〉作为γ线织构的主导取向;不同取向新晶粒具有不同的再结晶形核地点:{111}〈110〉新晶粒主要在{112}〈110〉和{111}〈112〉形变晶粒的晶界处形核;{111}〈112〉新晶粒主要在相同取向的形变晶粒内形核;而{110}〈001〉新晶粒主要在{111}〈112〉形变晶粒的形变带内形核。     

温度对非晶硅薄膜二次晶化的影响

为研究温度对固相晶化的影响,用玻璃作衬底,在不同温度下用PECVD法直接沉积非晶硅(a-Si:H)薄膜,把在室温、350℃和450℃下沉积的样品,在600℃和850℃下退火3h,把前后样品用拉曼光谱和扫描电镜分析,发现二次晶化后的晶化效果比直接沉积的薄膜好,850℃下退火的薄膜比600℃好。在450℃下沉积、850℃退火3h,SEM观察,表面最大晶粒尺寸为900nm左右。