A secure and improved multi server authentication protocol using fuzzy commitment

Multimedia Tools and Applications - The advancement in communication and computation technologies has paved a way for connecting large number of heterogeneous devices to offer specified services....     

Static pull-in analysis of microcantilevers based on the modified couple stress theory

This paper investigates the deflection and static pull-in voltage of microcantilevers based on the modified couple stress theory, a non-classic continuum theory capable to predict the size effects for structures in micron and sub-micron scales. It is shown that the couple stress theory can remove the gap between the experimental observations and the classical theory based simulations for the static pull-in voltage.     

Green synthesis of 5-arylidene-2,4-thiazolidinedione, 5-benzylidene rhodanine and dihydrothiophene derivatives catalyzed by hydrated ionic liquid tetrabutylammonium hydroxide in aqueous medium

An efficient synthesis of 5-arylidene-2,4-thiazolidinediones and 5-benzylidene rhodanines by the Knoevenagel condensation of 2,4-thiazolidinedione or rhodanine with aromatic aldehydes was studied. It proceeded smoothly in the presence of tetrabutylammonium hydroxide/H ₂O-EtOH to afford the corresponding products in high yields at 50°C. Also, a series of dihydrothiophene derivatives were synthesized via the four-component reaction of aldehyde, malonitrile, 2,4-thiazolidinedione, and piperidine in the presence of Bu₄NOH as a basic ionic liquid in aqueous medium. This new method offers several advantages, such as excellent yields, short reaction times, and simple procedure.     

Interfacially compatibilized LDPE/POE blends reinforced with nanoclay: investigation of morphology,rheology and dynamic mechanical properties

Morphological, melt rheological and dynamic mechanical properties of low-density polyethylene (LDPE)/ethylene–octene copolymer (POE)/organo-montmorillonite (OMMT) nanocomposites, prepared via melt compounding were studied. The XRD traces indicated different levels of intercalated structures for the nanocomposites. Addition of a compatibilizer (PE-g-MA) improved the intercalation process. TEM results revealed existence of clay layers in both phases but they were mainly localized in the elastomeric POE phase. Addition of 5 wt% OMMT to the LDPE/POE blend led to reduction in the size of the elastomer particles confirmed by AFM. The complex viscosity and storage modulus showed little effect of the presence of the clay when no compatibilizer was added. As the extent of exfoliation increased with addition of compatibilizer, the linear viscoelastic behavior of the composites gradually changed specially at low-frequency regions. The interfacially compatibilized nanocomposites with 5 wt% OMMT had the highest melt viscosity and modulus among all the studied nanocomposites and blends. Also, this particular composition showed the best improvement in dynamic storage modulus. The results indicated that clay dispersion and interfacial adhesion, and consequently different properties of LDPE/POE/clay nanocomposites, are greatly affected by addition of compatibilizer.     

A coupled bending-torsion model for electrostatically actuated torsional nano/micro-actuators with considering influence of van der Waals force

In the current paper, a coupled two degree of freedom model which considers both bending and torsion of the supporting torsion beams is presented for electrostatically actuated torsional nano/micro-actuators under the effect of van der Waals (vdW) force. Newton’s second law is utilized for finding the normalized equations governing the static behavior of the actuator. The implict function theorem is then utilized for finding the equations governing the pull-in state of the actuator. The related results show that torsion model considerably overestimates the pull-in parameters of the nano/micro-actuator. The concept of the instability mode is introduced, and it is shown that when the ratio of the bending stiffness to the torsion stiffness of the supporting torsion beams is relatively low, the dominant instability mode of the actuator would be the bending mode and otherwise the dominant instability mode would be the torsion mode. It is also observed that the presence of the vdW force can significantly reduce the pull-in angle and pull-in deflection of the nano/micro-actuator. The presented results also show that the vdW force can lead to considerable reduction in the pull-in voltage of the actuator. The equilibrium behavior of the actuator is studied, and it is observed that the vdW force and also bending of the supporting torsion beams greatly reduce the maximum allowable voltage which can be applied to the actuator. Results of this paper can be used for successful design of electrostatically actuated torsional nano/micro-actuators where the size of the actuator is sufficiently small, and as a result, the vdW force plays a major role in the system.     

Osmotic and activity coefficients in the solutions of 1- and 2-naphthol in methanol and ethanol at 298.15 K

The osmotic coefficient of the solution, activity of the solvent and activity coefficient of the solute in solutions of 1- and 2-naphthol in methanol and ethanol have been measured by the isopiestic method. The experimental osmotic coefficient data were correlated using the Non-Random Two Liquid model (NRTL), the Non-Random Factor model (NRF), the two suffix Margules equation and a polynomial in terms of the molality of the solute. The models give reliable results for the correlation of the osmotic coefficient data. The activity coefficients of 1- and 2-naphthol were evaluated according to the considered methods using the parameters obtained by the correlation of osmotic coefficients.     

Synthesis,Characterization, and Bioactivity Evaluation of Amorphous and Crystallized 58S Bioglass Nanopowders

The aim of this work was synthesis and characterization of amorphous and crystallized 58S nanopowders produced via sol‐gel method. According to the thermal analysis, the nanopowders were heat‐treated at 600°C and 1100°C. X‐ray diffraction results revealed that the phases of Wollastonite and tricalcium phosphate were formed at 1100°C. The in vitro tests showed that hydroxyl carbonate apatite was precipitated on both crystallized and amorphous nanopowders, while amorphous nanopowder showed a higher bioactivity than that of crystallized nanopowder. In contrast, mechanical properties of crystallized specimen were higher than those of amorphous specimen.     

Supercritical carbon dioxide (SC-CO2) dyeing of cellulose acetate: An opportunity for a “greener” circular textile economy

This article compares the dyeing of cellulose diacetate (cellulose-based) and polyester fabrics using supercritical carbon dioxide (SC-CO₂) and aqueous media. The benefits of dyeing in SC-CO₂ were clearly demonstrated in laboratory-based and pilot-scale studies in terms of increased colour strength, uniformity, fastness and the absence of auxiliaries such as dispersing agents or surfactants. In addition, the “super-levelling” nature of the SC-CO₂ medium was demonstrated in the reprocessing of polyester “waste textile” and the re-use of the “locked-in waste” colourant. The SC-CO₂ processing medium can be utilised to accurately colour “multiple life” polyester and cellulose acetate uniformly and to creatively tie-dye polyester and cellulose acetate fabrics. Through SC-CO₂ fluid technology, we can envisage a viable waterless circular manufacturing and recycling/remanufacturing framework for the predominantly polyester global fibre market coupled to the sustainably sourced, biodegradable cellulose diacetate as a replacement for cotton. The key technical and commercial advantages being the use of a single solvent dye class for both polyester and the cellulose diacetate, saving on energy costs, integrated simpler processing, reduced water usage and associated efficient recycling. Further, repositioning the cellulosic fibre industry towards using sustainable forests is attractive in terms of improved land, water and environmental management.     

Tool point dynamics prediction by a three-component model utilizing distributed joint interfaces

In machine dynamics the tool point frequency response functions (FRFs) are employed to predict the stable machining conditions. In this paper, a combined analytical–experimental substructuring procedure is proposed to determine the tool point FRFs for different holder–tool configurations. The method employs the measured spindle-machine FRFs and analytical models of the tool and the holder to predict the tool tip FRFs for different sets of tools and holders mounted on the machine spindle without the need for repeated experimental measurements. Distributed joint interfaces are used to couple the three-component model of the machine. The machine tool tip FRFs with different tool–holder combinations are obtained assuming the clamping conditions at joint interfaces remain unchanged. An experimental case study is provided to demonstrate the applicability of the proposed method in dynamic modeling of machine tool.