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1.
The tetragonal (t) to monoclinic (m) transformation behaviour and its relationship to microstructural evolution were investigated by means of dilatometry and transmission electron microscopy for ZrO2–9.7 mol% MgO during cyclic heating and cooling between room temperature and 1490 K. In the as-sintered specimens, fine oblate ellipsoidal t-phase precipitates, 20–50 nm in diameter and 100–200 nm long, were distributed in the cubic (c)-phase matrix. They were below a critical size for transformation and exhibited no transformation in the first three cycles. In the fourth and further cycles, transformation occurred in two distinct stages. A low-temperature stage appeared at 850–1000 K on heating and at 400–700 K on cooling, while a high-temperature stage appeared at 1350–1400 K on heating and at 1000–1200 K on cooling. With the increasing number of cycles, at first the size of low-temperature stages increased and then decreased above ten cycles accompanying the development of the high-temperature stage. During cyclic heating and cooling, coarsening of ellipsoidal precipitates and decomposition of c- and t-phases occurred. As a result of the decomposition, MgO particles and a new m-phase containing a very low concentration of MgO were produced. The coarsened ellipsoidal t-phase precipitates were responsible for the low-temperature stage. The new m- or t-phase containing very low MgO produced by the decomposition was responsible for the high-temperature stage. 相似文献
2.
HIRAMITSU SUZUKI SHUN WADA SEIICHI HAYAKAWA SINPATIRO TAMURA 《Journal of food science》1985,50(2):358-360
To prevent loss of w3 polyunsaturated fatty acids over long-term preservation, the effects of temperature and oxygen absorber on the fatty acids of sardine oil stored in air-tight film were studied. The fatty acids of sardine oil and lipids in the diet of experimental animals rapidly decreased over 1 month at 22°C. The amounts in the diet decreased slowly at 2°C; however, no alterations in the oil samples were observed for 6 months. Also, the amounts did not change at -30°C. Significant changes in samples treated with oxygen absorber were not observed under all temperatures during 6 months storage (P > 0.05). These results indicate that treatment with an oxygen absorber and/or freezing can prevent ω3 polyunsaturated fatty acids of fish oil from decreasing during storage. 相似文献
3.
氧浓度对近临界水中纤维素分解的影响 总被引:3,自引:0,他引:3
研究了不同初始氧浓度对纤维素在近临界水中分解的影响,实验结果表明,氧浓度显著地影响产物总碳收支平衡,液相不同组分的收率、气体的产量以及气相产物的组成,微量氧对产物总碳收支平衡影响不大,而对液相不同组分的收率有一定的影响。从实验结果可以看出,离子型反应机理在纤维素水解的第一步中起主导作用。而单糖的进一步分解是一个以自由基反应机理为主的过程。 相似文献
4.
综合介绍了脉冲电流通过细金属丝放电(pulsed wire discharge,PWD)制备纳米粉体的方法.讨论了影响纳米粉体,特别是晶粒尺寸的因素,以防止形成亚微米颗粒.因为达到电压峰值的丝的沉积能相当于丝的汽化能,因此,能夠计算出沉积能.随着所施加的能量增加,气体压力降低,介质气体的热扩散率增大,晶粒尺寸变小.在惰性气氛中,采用PWD工艺,由金属蒸气急冷可制备金属粉体.如果介质气体变为氧气或者氨气,就能制备氧化物、氮化物纳米粒子.要制备双金属合金、双氧化物或氮化物纳米粒子就必需采用双金属丝和不同的介质气体.采用PWD工艺,在有机气体或烟气中,能制备电磁屏蔽和导电浆料和其它用途的钝化纳米粒子.采用丝输送器而实现大量生产纳米粉体的PWD工艺一个实例证明了PWD工艺生产纳米粉体的可行性. 相似文献
5.
通过一个足尺的2层木结构房屋振动台试验,对Hilbert-Huang变换(HHT)在结构损伤诊断中的应用进行了研究与分析。在简要介绍了Hilbert-Huang变换的基本原理与方法后,根据在振动台试验中获取的结构反应数据,利用Hilbert-Huang变换对结构的动力特性及损伤状况进行了诊断。分析结果表明,Hilbert-Huang变换能有效地将隐含在实测结构反应信号中的结构动力特性与损伤信息进行提取,从而能对结构的健康状况进行诊断。 相似文献
6.
SEIICHI NAKAMORI 《International journal of systems science》2013,44(12):2573-2584
The optimal fixed-point smoother is designed based on an innovations theory for the white gaussian plus coloured observation noise in linear continuous systems. The signals to be estimated are non-stationary or stationary stochastic processes. The proposed fixed-point smoothing algorithm calculates estimates sequentially by using the observed value, the autocovariance function of the signal plus the coloured observation noise process and the cross-covariance function of the signal with the observed value. 相似文献
7.
The preparation for an experimental soft x-ray tomography study on the Heliotron J (H-J) machine is carried out, with the objectives of evaluating the capability of the current soft x-ray tomographic system in terms of the identification of different mode structures and their poloidal rotation, and the axis shift with different plasma and machine parameters, and fixing the physics goals for the experimental study. These preparations were carried out via a simulated soft x-ray data set arising from different plasma conditions, such as magnetic islands, low beta and high beta. Soft x-ray tomography (SXT) is performed by the discrete pixel method including singular value decomposition and Phillips–Tikhonov regularization, to obtain clear and smooth images. The H-J soft x-ray tomography results from simulated soft x-rays for the equilibrium H-J plasma sensed the magnetic axis shift clearly and an estimate was also achieved. Successful reconstruction for mode structure m=1/n=1 was obtained along with the realization of the poloidal rotation of the structure. The reconstruction for the m=2/n=1 mode was not very clear for the current soft x-ray diagnostic design. Effective mode identification was not possible due to the lack of measurements. The SXT from the current soft x-ray diagnostic on H-J, the magnetic axis shift can be estimated and the m=1/n=1 mode can be studied. Study of higher poloidal modes is difficult with the current design. 相似文献
8.
各种引气剂以及抑泡剂对混凝土经时变化状态等的影响 总被引:1,自引:0,他引:1
众所周知,采用粉煤灰制备混凝土,因粉煤灰成分中含有未燃炭等微粒子,容易造成阴离子型引气剂吸附在这些微粒子上,导致含气量经时损失.同时在混凝土的制备、运输过程中,因受采用的材料、拌和状态等物理因素影响,还会发生含气量经时增加的现象.所以在制备、管理混凝土时,如何保证出机初期一定的含气量、缓解含气量的经时损失或经时增加,是一项极其关键的技术.本文将就采用能改善上述状态的引气剂、抑泡剂拌和混凝土,对混凝土的经时变化以及抗冻融性等特征产生的影响进行论述. 相似文献
9.
Acid Urease: Reduction of Ethyl Carbamate Formation in Sherry under Simulated Baking Conditions 总被引:1,自引:0,他引:1
Acid urease derived from Lactobacillus fermentum was applied to reduce ethyl cthe target level (90 μg/L). However, complete prearbamate (EC) formation in California sherry production. Commercial sherry and sherry base were treated with urease under different conditions. Amounts of urea were determined and EC amounts were monitored by gas chromatography. Urea removal by acid urease reduced EC formation during the baking process and effectively maintained EC concentrations below vention of EC was not achieved because of precursors other than urea. 相似文献
10.
STUDIES ON THE GELATINIZATION RATE OF RICE AND POTATO STARCHES 总被引:1,自引:0,他引:1
KIYOSHI KUBOTA YOSHIHIKO HOSOKAWA KANICHI SUZUKI HIDEAKI HOSAKA 《Journal of food science》1979,44(5):1394-1397