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1.
研究了重金属工业废水缓蚀阻垢-净化回用的工艺,通过加入缓蚀阻垢剂ZY605,缓蚀阻垢效果明显。该工艺操作简单、科学合理、国内首创,经济效益显著。  相似文献   
2.
通过荧光光谱法研究槲皮素镧配合物(La L3·6H2O,L=槲皮素)与牛血清白蛋白(BSA)之间的相互作用。荧光光谱结果表明:槲皮素镧配合物与BSA形成基态复合物并引起荧光的静态猝灭,主要通过作用于BSA酪氨酸残基处引起BSA构象发生的变化。  相似文献   
3.
文章介绍了湘南学院化学与生命科学系无机实验室近年来从教学内容、教学模式及考核方式等方面进行教学改革的措施。实践证明:经改革后,无机化学实验课程内容体系得到充分优化,教学资源得到整合,充分调动了教师和学生的积极性,锻炼和培养了学生的实践动手和创新能力,取得了明显的教学效果。  相似文献   
4.
在碱性条件下,氯甲基化聚苯乙烯与丁二酰亚胺反应合成了聚(对乙烯基苄基丁二酰亚胺)树脂(简称为丁二酰亚胺树脂),采用元素分析、红外光谱对合成树脂的组成进行了表征。并考察了该树脂在酯水解反应中的催化活性。结果表明,在合成反应12h后,树脂增重最多,其中氮含量为4.08%,残余氯含量为2.51%,IR谱图中1640cm-1处出现较强酰胺羰基峰。在催化酯水解反应中,酸收率均大于85%,且催化稳定性好。  相似文献   
5.
The similarities of the non-linear chemical (NLC) fingerprints of Radix Glycyrrhizaes from four producing areas and eight other traditional Chinese medicines (TCMs) were calculated, using a systemic similarity calculation method proposed and three other main calculation ones (Euclidean distance, correlation coefficient and included angle cosine). All of the correlation coefficient similarities of different TCMs are higher than 0.952, and the included angle cosines are all higher than 0.962. So, both the correlation coefficient and included angle cosine similarities are unable to be used as the criteria for quantitatively evaluating the similarities of NLC fingerprints of TCMs. Although all of the Euclidean distance similarities of Berry Liquorices from four producing areas are less than 73, those of the other eight TCMs are all more than 180. The Euclidean distance cannot reflect the relative magnitudes of the feature differences in the NLC fingerprints very correctly. The systemic similarity method is the best among the four ones. All of the systemic similarities of Berry Liquorices from the four producing areas are higher than 0.962, while those of the other eight TCMs are all lower than 0.805, and the systemic similarity can reflect the differences between samples most faithfully, and can be used as a quantitative one evaluating the similarities of NLC fingerprints of TCMs, by which TCM could be distinguished and evaluated quickly, simply and exactly.  相似文献   
6.
The chemical components of the essential oils in the barks and leaves of Eucommia ulmoides Oliver were analyzed and compared by chromatograms and mass spectra technique, heuristic evolving latent projections (HELP), alternative moving window factor analysis (AMWFA) algorithms and normalization method based on the peak areas; the flavones in the barks and leaves of Eucommia ulmoides Oliver were separated on an ODS column by gradient elution carried out with the flow phase consisting of water, methanol and phosphoric acid (0.1%), and their contents were quantitatively determined by standard curve method and diode array detection (DAD) at 362 nm. The results show that 68 and 73 compounds respectively from essential oils of the barks and leaves of Eucommia ulmoides Oliver are identified, and there are 33 mutual compounds among 108 compounds determined. The total contents of these volatile components of the two samples possess 92.9% and 97.75% of the gross of the relevant essential oils, respectively; the contents of the rutin, quercetin and kaempferol in the barks and leaves of Eucommia ulmoides Oliver are 0.016 9, 0.003 6, 0.002 1 and 0.064 4, 0.030 2, 0.010 0 mg/g, respectively, and the determination recoveries are 95.2%–106.2%. The comparative analysis shows that for the barks and leaves of Eucommia ulmoides Oliver, there are significant differences in their components of the relevant essential oils and flavones. Foundation item: Project(20235020) supported by the National Natural Science Foundation of China  相似文献   
7.
通过静态吸附试验,研究了大孔交联聚(对乙烯基苄基脲)树脂(简称PMVBU树脂)对L-苯丙氨酸的吸附热力学及动力学特性。结果表明,在研究的浓度范围内,树脂对L-苯丙氨酸吸附平衡数据符合Langmuir和Freundlich等温吸附方程,相关系数R都在0.99左右,根据热力学函数关系计算了等量吸附焓、Gibbs吸附自由能和吸附熵,表明树脂对L-苯丙氨酸的吸附均为自发、放热、熵减的物理吸附过程。吸附符合二级动力学模型,颗粒内扩散过程是影响吸附速率的主要控制步骤。  相似文献   
8.
有色金属冶炼废水处理新工艺与实践   总被引:2,自引:0,他引:2  
介绍了一种有色金属冶炼工业废水处理新工艺及其在工业生产中的应用,分析了该工艺的经济效益和环境效益。  相似文献   
9.
在碱性条件下,氯甲基化聚苯乙烯与丁二酰亚胺反应合成了聚(对乙烯基苄基丁二酰亚胺)树脂(简称为丁二酰亚胺树脂),采用元素分析、红外光谱对合成树脂的组成进行了表征.并考察了该树脂在酯水解反应中的催化活性.结果表明,在合成反应12 h后,树脂增重最多,其中氮含量为4.08%,残余氯含量为2.51%.IR谱图中1 640 cm-1处出现较强酰胺羰基峰.在催化酯水解反应中,酸收率均大于85%,且催化稳定性好.  相似文献   
10.
周菊峰  谢红  彭爱姣  张辉 《食品科学》2010,31(22):407-410
目的:在微乳液介质中,用分光光度法测定面制食品中铝的含量。方法:样品经智能消解仪消解,在聚乙烯醇、正丁醇、正庚烷和水构成的微乳液中,以乙酸- 乙酸钠为缓冲体系,用铬天青S 作显色剂,其吸光度与铝含量在一定质量浓度范围内呈正比。结果:铝含量在0~6.0μg/25mL 之间线性关系良好,相关系数r=0.9971,回收率在95%~108% 之间。结论:该方法简便、灵敏、稳定,适用于面制食品中铝的测定。  相似文献   
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