纳米银的置换反应制备及其表征

通过对纳米银的制备和结构表征,研究贵金属纳米材料的制备方法和纳米结构。采用硝酸银和锌反应置换银纳米粒子,与传统化学还原法相比,工艺简单,无需添加保护剂和活性剂。采用光学显微镜、XRD、SEM、TEM、SAED等手段,表征纳米材料的尺寸、形貌、组成和晶体结构。结果表明,反应所得的产物为银枝晶结构,面心立方晶体。每个银枝晶都由主干、二次分枝、三次分枝组成,具有自相似性。     

An in Vitro Investigation of Acid Etching Treatment Prior to Post and Core Cementation and Teeth Fracture Resistance

In order to investigate how to enhance the teeth fracture resistance after the post and core treatment, an in vitro study was conducted to measure the fracture resistance of endodontically treated teeth restored with cast post and core with two kinds of surface treatment technology and acid etching preparation on the dentinal surface. Sixty-four recently extracted human single-rooted first premolars were endodontically treated and sectioned approximately 1.5 mm above the cementoenamel junction to remove the coronal portion. Each specimen received a cast post, core build-up and a metal alloy crown restoration. All teeth were randomly divided into the smooth surface post, core repair group, the sand blasting surface post, and core repair group, each group was divided into 10 s, 30 s, 60 s acid corrosion treatment group and control group. In acid test groups, an acid etching solution was applied for 10, 30 and 60 seconds, respectively, to the root canal wall surface. Each specimen was embedded in acrylic resin block and tested in an electronic universal testing machine. Fracture loads results showed that canal acid etching could increase teeth fracture resistance strength both in smooth groups and sandblasting group, and achieved the best effect when acid etching for 30 s. Sand spray treatment on the surface of the cast metal post can improve the flexural strength of the teeth after postcrown restoration. Acid etching on the root canal wall surfaces and sand spray treatment on the surface of the cast metal post can improve the flexural strength of the root after post-crown restoration. Therefore, these two methods could be used to strengthen the tooth fracture resistance, and maintain the long-term therapeutic effect of cast post and core restoration.     

开关磁阻电机磁固耦合建模与分析

针对开关磁阻电机振动和噪声问题,本文应用麦克斯韦应力法,考虑铁磁材料的磁饱和和边缘磁通效应,对气隙磁密和电磁力进行分析计算,建立了定子系统的磁固耦合非线性模型。并用有限元软件ANSYS对其进行分析验证。结果表明:该模型与二维有限元结果基本趋于吻合,在误差允许的范围内,且符合电机实际动行特点,验证了模型的有效性。