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排序方式: 共有209条查询结果,搜索用时 15 毫秒
1.
以2-吡咯基三氯乙酮为主要原料,经过乙二醇单酯化、羟基氯取代、环合三步反应制得了3,4-二氢吡咯[2,1-c][1,4]噁嗪-1-酮;又经过Friedel—Crafts酰基化和环合反应制得了未见文献报道的7-芳酰基-3,4-二氢吡咯[2,1-c][1,4]噁嗪-1-酮它们及其某些重要中间体的结构分别采用红外光谱、质谱、核磁共振氢谱、核磁共振碳谱以及高分辨率质谱进行了表征. 相似文献
2.
区域水文要素复杂性研究是当今的热点问题,为了研究哈尔滨地区汛期径流量的复杂性特征及变化趋势,将R/S分析法和等概率粗粒化LZC算法引入到区域径流复杂性分析与变化趋势预测中,对地区内10个水文站点的汛期径流序列的复杂性进行诊断并对其变化趋势进行分析。研究结果表明:哈尔滨、通河、阿城、依兰、烟囱山各站未来的汛期径流量呈减少趋势,岔林河、莲花、西北河、延寿、四平山各站未来的汛期径流量呈增长趋势;各站点汛期径流序列的复杂度由高到低依次为:四平山、烟囱山、岔林河、阿城、西北河、依兰、莲花、通河、哈尔滨、延寿;从河流集水面积对其径流长程相关性和复杂性的影响可以看出,站点的河流集水面积越大,其径流量的长程相关性越强,复杂性指数越小。研究成果揭示了本地区汛期径流量的变化趋势以及复杂性演变特征,该特征可为区域径流预测及水资源优化配置提供科学依据。 相似文献
3.
M FAIZAN G MURTAZA S H KHAN A KHAN ASIF MEHMOOD R KHENATA S HUSSAIN 《Bulletin of Materials Science》2016,39(6):1419-1425
We investigated double perovskite compounds of the form Sr 2 XOsO 6 (X = Li, Na, Ca) using the full-potential linearized augmented plane wave (FP-LAPW) method. For the exchange-correlation energy, Wu and Cohen generalized gradient approximation (WC-GGA), Perdew, Burke and Ernzerhof GGA (PBE-GGA), Engel and Vosko GGA (EV-GGA), and GGA plus Hubbard U-parameter (GGA + U) were used. The calculated structural parameters are in good agreement with the existing experimental results. Calculation of different elastic constants and elastic moduli reveals that these compounds are elastically stable and possess ductile nature. The GGA + U approach yields quite accurate results of the bandgap as compared with the simple GGA schemes. The density of states plot shows that Sr-4d, Os-5d and O-2p states predominantly contribute to the conduction and valence bands. Further, our results regarding to the magnetic properties of these compounds reveal their ferromagnetic nature. In addition, these compounds seem to possess half-metallic properties, making them useful candidates for applications in spintronics devices. 相似文献
4.
HADI M MARWANI AMJAD E ALSAFRANI HAMAD A AL-TURAIF ABDULLAH M ASIRI SHER BAHADAR KHAN 《Bulletin of Materials Science》2016,39(4):1011-1019
In this study, an efficiently employed ionic liquid combined with commercially available silica gel (SG–ClPrNTf2) was developed for selective detection of gold(III) by use of inductively coupled plasma–optical emission spectrometry (ICP-OES). The selectivity of SG–ClPrNTf2 was evaluated towards seven metal ions, including Y(III), Mn(II), Zr(IV), Pb(II), Mg(II), Pd(II) and Au(III). Based on pH study and distribution coefficient values, the SG–ClPrNTf2 phase was found to be the most selective towards Au(III) at pH 2 as compared to other metal ions. The adsorption isotherm of Au(III) on the SG–ClPrNTf2 phase followed the Langmuir model with adsorption capacity of 59.48 mg g?1, which was highly in agreement with experimental data of adsorption isotherm study. The kinetics study indicated that Au(III) adsorption kinetics data were well fit with the pseudo-second-order kinetic model on the basis of correlation coefficient fitting (0.996) and adsorption capacity agreement (62.26 mg g?1). Furthermore, SG–ClPrNTf2 phase was effectively performed for the determination of Au(III) in real water samples with satisfactory results. 相似文献
5.
Data from spacecrafts suggest that space plasma has an abundance of suprathermal particles which are controlled by the spectral index κ when modeled on kappa particle velocity distribution. In this paper, considering homogeneous plasma, the effect of integer values of κ on the damping rate of an obliquely propagating magnetosonic(MS) wave is studied. The frequency of the MS wave is assumed to be less than ion cyclotron frequency, i.e.,iw(28)w. Under this assumption, the dispersion relation is investigated both numerically and analytically, and it is found that the real frequency of the wave is not a sensitive function of κ, but the imaginary part of the frequency is. It is also shown that for those values of κ where a large number of resonant particles participate in wave–particle interaction, the wave is heavily damped, as expected. The possible application of the results to the solar wind is discussed. 相似文献
6.
7.
M. RIAZ KHAN 《国际生产研究杂志》2013,51(3):443-452
This paper introduces a model for efficient utilization of warehouse personnel in an inventory selection process. A simple mathematical model, based on a time study that can be applied to establishing standards for efficiency measurement of labour in a warehouse setting is presented. The problem of determining a standard to compute performance in an environment with variable workload is solved by using an adjustable standard for each particular assignment. Specifically the proposed model is designed to estimate the time required to complete a picking cycle. Three time components are considered; the lead time, travel time, and non-efficient time. The results of an empirical study are used to set the values of system parameters. The use of a computer system that can generate order lists is essential for an effective application of this methodology. Useful information can be obtained that can aid managers in formulating and implementing incentive plans and for controlling the labour cost which represents a major proportion of the total cost in warehouse operation. 相似文献
8.
Industrialization has led to a number of environmental problems, such as release of toxic metals and other toxic organic and inorganic compounds to the environment. Among all, the rapid expansion of leather related industries in Pakistan have resulted in considerable environmental problems and effluents from processing of both domestic and imported hides and skins have increased pollution to alarming levels. Some tannery effluents of Peshawar area investigated in the present study showed high concentrations of Cr(Ⅵ) (2.7-12.6 mg/L), Cu(Ⅱ) (2.6-11.4 mg/L) and phenol (0.1-4.2 mg/L). These contaminants are very toxic and must be removed from effluents before releasing into water bodies. A new technique of gamma irradiation has been investigated to decrease the load of COD and concentrations of Cr(Ⅵ), Cu(Ⅱ) and phenol associated with tannery effluents to the permitted values. It was observed that concentration of Cr(Ⅵ) in the effluents can be brought to the permitted level by applying radiation dose of 3 kGy. A radiation dose of 2.5 kGy was required to remove more than 95% of Cu(Ⅱ) and 100 % degradation of phenol in tannery effluents could be achieved by only one kGy of radiation dose. 相似文献
9.
A new configuration for operational amplifier based instrumentation amplifier is presented. The analytical expressions are obtained and the performance of the proposed circuit is examined in relation to the conventional circuit. Simulation and experimental results are presented which establish the superiority of the proposed instrumentation amplifier topology over the conventional circuit. The effect of second pole of op amps on the circuit stability has also been investigated. Numerical results are given in support of theoretical conclusions. 相似文献
10.
ANWAR A. KHAN 《International Journal of Electronics》2013,100(2):421-431
A new integrable BIFET composite unit comprising two BJTs, one JFET and one passive resistor is described and as a unit shown to exhibit FET-like characteristics with much improvement in thermal stability and transfer curve linearity over a wide range of input bipolar voltage and temperature variations. The forward transfer admittance of the unit may easily be adjusted over a wide range. Amplifier circuits using the proposed unit are also described. 相似文献