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石蜡聚苯乙烯微球的制备 总被引:1,自引:0,他引:1
通过悬浮聚合技术合成了石蜡聚苯乙烯微球,研究了合成过程中引发剂浓度及交联剂用量对微球粒径及其分布的影响。 相似文献
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To construct superoxide dismutase (SOD) mimetics, three Cu(Ⅱ) coordination polymers (CPs), [Cu3(L1)4(OH)2(H2O)2]n (CP 1), [Cu(L2)(OH)]n (CP 2) and [Cu(L2)(CH3O)]n (CP 3), in which n is a positive integer, are synthesized by solvothermal method using nicotinate N-oxide (HL1) or isonicotinate N-oxide (HL2) as organic ligands and Cu(OAc)2·H2O as metal salt. Their structures and properties are characterized by single crystal X-ray diffraction, X-ray powder diffraction, infrared spectroscopy, elemental analysis, thermogravimetric analysis and ultraviolet spectroscopy. CPs 1~3 are synthesized under similar solvothermal conditions, but show a multi-dimensional configurations from one-dimensional, two-dimensional to three-dimensional, respectively, exploring the possible mechanisms of the relative position of functional groups in ligand, the coordination mode of ligand and the solvent system on the structural diversity of CPs. Thermogravimetric analysis shows that CPs 1~3 can be stabilized up to 202, 228, and 250 ℃, respectively, which display good thermal stability, and the higher the dimension of CPs 1~3, the better the thermal stability. Nitrotetrazolium blue chloride (NBT) photoreduction test shows that the semi-inhibitory concentration values (IC50) of CPs 1~3 are 0.21, 0.26 and 0.62 μmol/L, respectively, which display certain SOD activity, and the lower the dimension of CPs 1~3, the better the SOD activity. The lower IC50 of CP 1 and CP 2 indicating that they can be used as potential SOD mimetics. 相似文献
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针对微颗粒空间装配的问题,以外径为十几微米的微颗粒与外径为几百微米的柱腔装配为研究对象,开展微颗粒空间跨尺度装配方法研究。首先,针对微颗粒受到基底表面作用力影响不易被拾取与释放的问题,分析了微颗粒的受力情况,设计了真空吸附式微夹持器用于微颗粒的拾取与释放;然后,针对由于微颗粒与柱腔的尺寸跨度大,很难实现装配过程中二者空间位置实时监测的问题,设计了具有多维视觉监测功能的微装配机器人并且建立了多维视觉监测模型,实现微颗粒与柱腔装配过程的在线监测;最后,提出了基于多维视觉监测模型的微颗粒与柱腔空间半自动装配方法。实验结果证明了所提方法的有效性,并且实现了将外径为20μm的微颗粒放入外径为200μm的柱腔内的目标。该方法适用于微机电系统制造中微颗粒的三维空间装配。 相似文献
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