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1.
Eu3 ions were incorporated in sol and gel by a sol-gel processing using 3-glycidoxypropyltrimethoxysilane(CH2OCHCH2O(CH2)3Si(OCH3)3, GPTMS) and ethyl silicate (TEOS) as precursors. The basic chemical-physical properties such as DTA curve, FF-IR spectra and specific surface area were recorded. The characteristics of their optical spectra were measured and investigated. The results indicate that the emission intensity of Eu3 ion in ormocer is much higher and the global line width is wider than those in SiO2 gel. The relationship between the composition and structure of gels and the fluorescence intensity and width were discussed. The obtained ormocer shows good mechanical strength, which can be cut and polished in machine without broken. 相似文献
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通过优选合适的化学原料,用坩埚下降法生长出了无宏观缺陷的Zn:Fe:LiNbO3(Zn:Fe:LN)单晶。生长的工艺参数是:用微凸生长界面生长,生长速度为1~3mm/h,温度梯度为20~30℃/cm。用X射线衍射及DTA对晶体进行了分析;测定了晶体的吸收光谱。结果表明:所有Zn:Fe:LN晶体中的Fe^2 浓度沿生长方向增加;掺杂3%ZnO(摩尔分数)的Zn:Fe:LN单晶中的Fe^2 浓度沿生长方向的变化量比掺杂6%ZnO的大。从坩埚下降法的温场特点、晶体的热处理过程、环境气氛,以及ZnO组分对Fe离子的排斥作用解释了产生Fe^2 离子浓度变化的原因。 相似文献
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用高温熔融法制备了Dy3+/Tb3+掺杂的高钆镥氟氧化物闪烁玻璃样品,测试分析了其吸收光谱、激发与发射光谱及衰减曲线等。研究了Dy3+和Tb3+离子浓度增加对Tb3+离子发光的影响以及Dy3+离子的浓度猝灭效应;通过IH理论模型分析了Dy3+和Tb3+离子的能量传递方式和能量传递效率。结果表明Dy3+离子对Tb3+离子发光具有敏化作用,随着Dy3+离子浓度增加敏化作用增强,但是当Dy3+离子的浓度达到2%(摩尔分数)以上时,随着Dy3+离子浓度的增加,Tb3+离子的发光强度降低;Dy3+和Tb3+离子的能量传递方式为无辐射能量传递方式,且能量传递效率可以达到60%以上。 相似文献
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The (60 - x)Bi2O3 - xGeO2-30B2O3-10ZnO (x = 5, 10, 20, 30 molar percent) glasses doped with Er^3+ and Er^3+/Yb^3+ were fabricated using the melting method. The thermal stability of the glasses was studied with their DTA curves. The results show that the difference between the glass transition temperature and the crystallization onset temperature increases with the increase of GeO2 content, indicating that the thermal stability of the glass has become better. The absorption spectra were recorded and the stimulated emission cross sections were calculated using the McCumber theory. The Ω2, O4, and Ω6 parameters,the transition probability, the radiative lifetime, and the fluorescence branch ratio of Er^3+ for optical transition were calculated from their absorption spectra in terms of reduced matrix U^(t)(λ = 2, 4, 6) character for optical transitions. The infrared emission of Er^3+ was measured upon excitation with 970 nm light and the full width at half-maximum (FWHM) was estimated from the emission spectra. The pumping efficiency and the intensity of the emission at the 1.54 μm band of Er^3+ were enhanced considerably by co-doping Yb^3+ . 相似文献
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The lithiumniobate single crystal (LiNbO3,LN)is one of the most i mportant materials because of itsexcellent properties such as piezoelectricity , photo-electricity, photorefractivity , and a nonlinear opticaleffect .It has been widely used for functional applica-tions such as , in the surface acoustic wave device(SAW) ,the piezoelectric transducer (PET) ,the op-tic parameter oscillator ( OPO) , the high-resolutionholographic storage and so on[1]. The Er3 +dopedLiNbO3crystals have also … 相似文献
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以K2O为助熔剂,在较大的温度梯度(90~100℃/cm)条件下进行引种和晶体生长,应用坩埚下降法技术成功地生长出了初始Mn2 掺杂浓度为0.5%(摩尔分数)的近化学计量比的铌酸锂晶体.用X射线衍射表征了获得的晶体,并计算了晶体的结构参数.与同成分的铌酸锂晶体相比,样品的晶格常数略变小,紫外吸收边向短波方向发生了移动.测定了晶体的吸收与发射光谱,观测到吸收中心在571nm(6A1g(6S)→4T1g(4G))的吸收宽带以及发光中心约620nm(4T1g(4G)→6A1g(6S))的红色荧光带.从晶体上部与下部的颜色以及吸收强度的变化,可初步推测出沿着晶体生长方向Mn2 离子浓度逐渐增加,Mn2 离子在晶体中有效的分凝系数<1. 相似文献
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Lithium lutetium fluoride (LiLuF4) single crystals doped with different Dy3+ ion concentrations were grown by Bridgman method. The Judd-Ofelt (J-O) strength parameters (Ω2, Ω4, Ω6) of Dy3+ in LiLuF4 crystal are calculated according to the measured absorption spectra and the J-O theory, by which the asymmetry of the Dy3+:LiLuF4 single crystal and the possibility of attaining stimulated emission from 4F9/2 level are analyzed. The capability of the Dy3+:LiLuF4 crystal in generating white light by simultaneous blue and yellow emissions under excitation with ultra- violet light is produced. The effects of excitation wavelength and doping concentration on chromaticity coordinates and photoluminescence intensity are also investigated. Favorable CIE coordinates, x=0.319 3 and y=0.349 3, can be obtained for Dy3+ ion in 2.701% molar doping concentration under excitation of 350 nm. 相似文献