结构优化分子筛的制备及其催化裂化性能Ⅱ.结构优化分子筛的催化裂化性能

利用结构优化改性前后的分子筛作为活性组元制备出一系列催化剂,并通过重油微反及ACE-Model R+固定流化床评价其催化裂化性能,并进行了比较.结果表明,采用气相超稳制备的分子筛再经稀土离子优化改性后,用其制成的催化剂的催化裂化反应的转化率显著提高,重油裂化能力明显增强,汽油中烯烃的含量大幅度降低.     

再入飞行器最佳外形探讨

本文介绍再入飞行器可能的最佳外形的研究情况。选择再入飞行器最佳形状的准则是:气动稳定性、端头和截锥体边界层转捩的发生和传播、非对称端头形状变化引起的配平、最小的再入散布以及助推器的尺寸和重量限制。数值计算结果表明,根据上述准则,与球形端头相比,扁圆形端头(例如平面端头或5×1椭球形端头)具有较好的潜在性能。对于后体,只考虑了双锥外形,并且经研究确定最佳的双锥外形有如下特点:θ_1≈2θ_2和R_b≈2R_i,其中θ_1,θ_2分别为前后锥的半锥角,R_i是双锥连接处的当地半径,R_b是再入飞行器的底部半径。在这些约束条件下,有可能在截锥体边界层转捩性能不降低的条件下,改善再入飞行器的气动热力学性能,例如x_(c·p),随M_∞和α的变化小;烧蚀端头对下游的影响降到最小。本文也对文中提出的再入飞行器最佳外形的缺点进行了讨论。     

Preparation and Properties of Rare Earth Modified Carbon Black/Natural Rubber Composites

The oxides Eu, Ho, Er and Dy were used to prepare the hydroxides of rare earth modified carbon black. Then natural rubber latex （NRL） was added into the reactor. The system reacted at 85 ℃ with stirring for 1 h to prepare powdered HAF-Ln（OH）3/NR composites. The effects of the kind and content of Ln on the particle size distribution of P [ NR/HAF-Ln （OH）3 ] and mechanical properties of its vulcanizate were studied respectively. It is found that rare earth can help to get the powder of the composite, the product particle with a diameter less than 0.9mm will be get when the composites containing the compound of Ho, Er and Dy with dosage of 1.0, 1.0, O. 5 percent, respectively. The adding of Ln can improve the tensile strength and tear strength of the vulcanizate effectively, what＇s more, Er and Dy can decrease the permanent set of vulcanizate significantly. The SEM studies shows that P[ NR/HAF-Dy （OH）3 ] vulcanizate shows superior mechanical properties that depend primarily on the absence of free carbon black, the fine dispersion of carbon black in the rubber matrix and better polymer-filler interaction.     

Upgrade of Physical Design for Removable Segmented Gamma Scanner

为提高加速器控制领域的智能化水平，吸收近年来IT领域中控制技术的最新发展成果，设计实现了低能强流离子束网络控制系统，可提供20mA、能量为5-100keV的两条离子束线，并进行脉冲束流和气体靶试验。实现了手动、自动建立系统真空，数字量输入输出、模拟量输入输出、串口通讯等150多个量的常规测控以及不同电位状态下多个量的报警互锁保护等功能。     

The Bisphosphonate Clodronate Modifying Hydroxyapatite Bioceramics for Bone Scaffold

To investigate the efficiency of clodronate modifying HA bioceramics,and to evaluate the effect of clodronate modifying HA bioceramics on the cells in vitro,clodronate modified the porous HA bioceramics for bone scaffold by chelation .The outermost layer of the specimens was analyzd by XPS and FI-IR ,The depth profile was investigated by the argon-ion sputtering method.The cell culture test was conducted using MC3T3-E1 osteoblastic cells,The cells were inoculated and cultured on the scaffolds.Morphological observation of the cells,MTT test and ALP activity test evaluated the cell attachment ,proliferation and activity on the scaffolds.The cell culture test in cell quantity and morphology indicated active proliferation of the cells on the scaffolds.The ALP activity of the cells cultured for 3d and 7d on clodronate-HA bioceramics was slightly higher than that on HA bioceramics ,but the difference was not signifcant,This result indicated that clodronate-HA bioeramics had favorable cytocompatibility to be used as bone scaffold with potential ability to improve asteogensis.     

Abstract Implementation of Algebraic Specifications in a Temporal Logic Language

A formal technique for incorporating two specification paradigms is presented,in which an algebraic specification is implemented by a set of abstract procedures specified in pre and post-condition style.The link between the two level specifications is provided via a translation from terms of algebraic specifications into temporal logic formulae representing abstract programs.In terms of translation,a criterion for an abstract implementation satisfying its specification is given,which allows one to check the consistency between the two levels of specifications.The abstract implementations can be refined into executable code by refining each abstract procedure in it.It is proved that the satisfication relation between a specification and its implementations is preserved by such refinement steps.     

Observation of atomic steps on CaCO3 crystal surface

By using scanning polarization force microscopy,the deliquescence process and the atomic steps on the cleavage surface of CaCO3 in air were studied in situ.Under an exposure to medium umidity(-57%),the sloiw step movement has been observed.     

Theoretical Discussion of Couple-Mode Using Chirped Fiber Grating for Dispersion Compensation

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Measurement system for wind turbine acoustic noise assessment based on IEC standard and Qin＇s model

A novel measurement system specially used in noise emission assessment and verification of wind turbine generator systems is presented that complies with specifications given in IEC 61400-11 to ensure the process consistency and accuracy. Theory elements of the calculation formula used for the sound power level of wind turbine have been discussed for the first time, and detailed calculation procedure of tonality and audibility integrating narrowband analysis and psychoacoustics is described. With a microphone and two PXI cards inserted into a PC, this system is designed in Qin＇s model using VMIDS development system. Benefiting from the virtual instrument architecture, it＇s the first time that all assessment process have been integrated into an organic whole, which gives full advantages of its efficiency, price, and facility. Mass experiments show that its assessment results accord with the ones given by MEASNET member.     

Input-output finite-time stability of time-varying linear singular systems

This paper studies the input-output finite-time stabilization problem for time-varying linear singular systems. The output and the input refer to the controlled output and the disturbance input,respectively.Two classes of disturbance inputs are considered,which belong to L-two and L-infinity.Sufficient conditions are firstly provided which guarantee the input-output finite-time stability.Based on this,state feedback controllers are designed such that the resultant closed-loop systems are input-output finite-time stable.The conditions are presented in terms of differential linear matrix inequalities.Finally,an example is presented to show the validity of the proposed results.