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聚丙烯酰胺/氧化石墨纳米复合材料的研究 总被引:4,自引:0,他引:4
氧化石墨具有良好的层状结构,其层间具有丰富的官能团,能与有机聚合物形成插层纳米复合材料进而改善材料的性能.采用层离吸收-原位聚合法制备了聚丙烯酰胺/氧化石墨纳米复合材料,并采用XRD、HREM及DSC等对其结构和性能进行了表征。结果表明,聚丙烯酰胺与氧化石墨两者之间存在着较强的相互作用,材料的玻璃化转变温度得到提高,层离吸收-原位聚合法是获得聚丙烯酰胺/氧化石墨层纳米复合材料的有效途径,聚丙烯酰胺在氧化石墨中存在着多种排列方式,不同层间距(1.6nm和2.8nm)的聚丙烯酰胺/氧化石墨纳米复合结构同时存在。 相似文献
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1 INTRODUCTIONOrganic intercalatedlayeredsolidshavebeenstudiedbyscientistsindifferentfieldsformanyyearsbecauseoftheirnew physicalandchemicalpropertiessuchaselectricalproperties[1] ,mechanicalproper ties ,thermalbehavior[2 ] ,surfaceandinterfacialproperties[3] .Graphiteoxide (GO)hasbeenstudiedformany years ,itsstructuralmodel[4 6 ] ,formationprocessandkinetics[7,8] havebeenstudiedindetail.IthasbeenreportedthatGOpossessesC OHande poxidefunctionalgroups[9] whichmakegraphiteox ideeasilyabs… 相似文献
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According to control theories, mine fires can be considered as an unsteady process after the normal ventilation system is disturbed. Applied the principal of physical chemistry and thermal fluid mechanics, the parameters models of the unsteady state system have been given, such as fuel combustion rate, heat of combustion, concentration, temperature, heat losses, heat resistance, work of expansion and heat pressure difference. The results of the calculation agree approximately with the results of the test. By the computer simulation, it is shown that the main factor of producing the throttling effect is the fire rate, second is the heat resistance and the heat pressure difference. The rate of heat flow that passes through the airway wall is the maximum on the surface, and decrease with time. The heat transfer progresses only within the range of 0..5 m away from theairway wall during combus-tion for 2 hours. It‘s variable for the mass flux rate and the percentage concentration of the gas along the airway of the downstream. When the delayed time is very small, the varidtion can be neglected. Viscosity resistance is the main part of the heat resistance, second is the expansion resistance that is less than tens Pascal when Mach number is very small. Work of expansion is principally tumed into heat losses, only a very small part is consumed by the work of the heat resistance and the inertia acceleration. 相似文献
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1 INTRODUCTIONMinefireisoneofthecriticaldisastersinunder groundcoalmining[1] .Oncefireaccidentshappen ,theycausealargelossoflivers ,destroygenerouscoalresourcesandequipment.Iftheyarenothandledproperlyandtimely ,theymaybeinducemoreseriousconsequencessuchasga… 相似文献
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体绘制技术常用于3维体数据场的可视化,其虽然可以生成高质量的投影图像,但通常不能绘制由体数据与点、线、面图形组成的混合场景。在现有的混合场景可视化方法中,有些只能绘制由体数据与面图形组成的复杂混合场景,而不能处理存在点和线的混合场景;有的则成像速度慢、成像质量差。为了能够正确地绘制复杂混合场景,采用SIMD和软件加速等技术,提出了一种速度快、成像质量高的基于光线投射算法的混合场景可视化方法,并分析了该算法所具有的3种绘制次序,以便满足不同应用的要求。该算法既可用于不同场景的绘制,又可用于平行和透视投影中。实验结果表明,该算法能够正确地绘制体数据与点、线、面图形组成的混合场景,且成像速度快,图像质量高。 相似文献
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