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排序方式: 共有117条查询结果,搜索用时 10 毫秒
1.
Amrita Kundu Claire Davis Martin Strangwood 《Metallurgical and Materials Transactions A》2011,42(9):2794-2806
The present investigation examines the applicability of the Dutta–Sellars equations in predicting the recrystallized grain
sizes following deformation for a 0.046 wt pct Nb-bearing, commercially produced steel with a segregated solute content (from
continuous casting). The investigation considered initial unimodal and bimodal grain size distributions before deformation
that were generated by reheating the steel to 1498 K and 1423 K (1225 °C and 1150 °C), respectively. It was found that the
reheated grain size distribution (separated into grain size classes) could be related to the solute-rich (smaller grain size
classes) and solute-depleted (larger grain size classes) regions. The use of these relationships and a simple halving of the
grain size within the distribution on recrystallization (used previously for homogenized samples of this steel) were found
to be appropriate in the grain size class-based use of the Dutta–Sellars equations with respect to mode and maximum grain
sizes after hot deformation and holding. This approach successfully predicted (confirmed by experiment) the grain size distribution
after deformation in the presence of Nb segregation from continuous casting. 相似文献
2.
The nonpeptide δ-opioid agonist BW373U86 (3 to 300 μg/kg) was tested in rabbits for effects on heart rate, cardiac orienting and Pavlovian conditioned responses to tones, and unconditioned cardiac and somatomotor responses to signaled and unsignaled shocks. BW373U86 did not alter shock-evoked somatomotor reflexes and had few effects on the development or retention of Pavlovian conditioned heart rate discrimination. However, BW373U86 appeared to modulate cardiac conditioning indirectly, by facilitating sympathetic reflexes evoked by the signaled stressor, and the dose effect was ∪-shaped within the dose range tested. The pronounced tachycardiac effect of BW373U86 was completely blocked, or rapidly reversed, by the selective δ-opiate antagonist naltrindole. BW373U86 was more potent in increasing signaled than unsignaled shock-evoked tachycardia, suggesting release of an endogenous substance (e.g., a δ-opioid) because of the Pavlovian conditioning contingency. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
3.
A material consisting of multi-walled carbon nanotubes (MWCNTs) and larger titania (TiO(2)) nanotube arrays has been produced and found to be efficient for reversible hydrogen (H(2)) storage. The TiO(2) nanotube arrays (diameter ~60?nm and length ~2-3?μm) are grown on a Ti substrate, and?MWCNTs a few μm in length and ~30-60?nm in diameter are grown inside these TiO(2) nanotubes using chemical vapor deposition with cobalt as a catalyst. The resulting material has been used in H(2) storage experiments based on a volumetric method using the pressure, composition, and temperature relationship of the storage media. This material can store up to 2.5?wt% of H(2) at 77?K under 25?bar with more than 90% reversibility. 相似文献
4.
In this work we demonstrate a large electric field‐induced bipolar strain ~0.40% in Li, Ta and Sb modified BNT–KNN ((1?x) Bi0.5Na0.5TiO3–xK0.47Na0.47Li0.06 Nb0.74Sb0.06Ta0.2O3) system. The morphotropic phase boundary (MPB) of the system between rhombohedral and tetragonal phases lies in the range 0.02 ≤ x ≤ 0.06, beyond which all compositions (up to x < 0.15) were found to be tetragonal. A clear trade‐off between the large strain values and achievable d33, kp for a particular composition was noted. It is shown that while for x = 0.03, d33 169 pC/N, kp 49% and strain ~0.13% were obtained, for x = 0.08 with 0.40% strain, d33 and kp values decreased drastically. 相似文献
5.
The simultaneous addition of styrene maleic anhydride copolymer and multiwall carbon nanotubes during melt‐mixing on the morphology of binary blends of polyamide6 and acrylonitrile butadiene styrene copolymer 下载免费PDF全文
B.F. Jogi Arup R. Bhattacharyya Amrita V. Poyekar Petra Pötschke George P. Simon Satish Kumar 《Polymer Engineering and Science》2015,55(2):457-465
The effect of simultaneous addition of multiwall carbon nanotubes (MWNTs) and a reactive compatibilizer (styrene maleic anhydride copolymer, SMA) during melt‐mixing on the phase morphology of 80/20 (wt/wt) PA6/ABS blend has been investigated. Morphological analysis through scanning and transmission electron microscopic analysis revealed finer morphology of the blends in presence of SMA + MWNTs. Fourier transform infrared spectroscopic analysis indicated the formation of imide bonds during melt‐mixing. Non‐isothermal crystallization studies exhibited the presence of a majority faction of MWNTs in the PA6 phase of 80/20 (wt/wt) PA6/ABS blend in presence of SMA + MWNTs. Rheological analysis, dynamic mechanical thermal analysis, and thermogravimetric analysis have demonstrated the compatibilization action of simultaneous addition of a reactive compatibilizer (SMA copolymer) and MWNTs in PA6/ABS blends. An attempt has been made to investigate the role of simultaneous addition of SMA copolymer and MWNTs on the morphology of 80/20 (wt/wt) PA6/ABS blend through various characterization techniques. POLYM. ENG. SCI., 55:457–465, 2015. © 2014 Society of Plastics Engineers 相似文献
6.
Ateek Shah Yashwant Kumar S. Rohan Amrita B. Hazra 《Chembiochem : a European journal of chemical biology》2023,24(11):e202300055
Flavin adenine dinucleotide (FAD) is an essential redox cofactor in cellular metabolism. The organic synthesis of FAD typically involves coupling flavin mononucleotide (FMN) with adenosine monophosphate, however, existing synthesis routes present limitations such as multiple steps, low yields, and/or difficult-to-obtain starting materials. In this study, we report the synthesis of FAD nucleobase analogues with guanine/cytosine/uracil in place of adenine and deoxyadenosine in place of adenosine using chemical and enzymatic approaches with readily available starting materials, achieved in 1–3 steps with moderate yields (10–57 %). We find that the enzymatic route using Methanocaldococcus jannaschii FMN adenylyltransferase (MjFMNAT) is versatile and can produce these FAD analogues in high yields. Further, we demonstrate that Escherichia coli glutathione reductase is capable of binding and using these analogues as cofactors. Finally, we show that FAD nucleobase analogues can be synthesized inside a cell from cellular substrates FMN and nucleoside triphosphates by the heterologous expression of MjFMNAT. This lays the foundation for their use in studying the molecular role of FAD in cellular metabolism and as biorthogonal reagents in biotechnology and synthetic biology. 相似文献
7.
Potential of Sr4Al14O25: Eu2+,Dy3+ inorganic oxide-based nanophosphor in Latent fingermark detection
Vishal Sharma Amrita Das Vinay Kumar O. M. Ntwaeaborwa H. C. Swart 《Journal of Materials Science》2014,49(5):2225-2234
In this paper, the potential of the Sr4Al14O25: Eu2+,Dy3+ fluorescent nanophosphor is explored to visualize the latent fingermarks. The nanophosphor has been synthesized using self-propagating high temperature synthesis and shows intense luminescence and strong long after glow properties. These nano particles have been characterized for their particle size, crystalline phase, and photoluminescent properties. The calculated PL CIE co-ordinates (0.138, 0.359) correspond to the blue–green shade. Different porous, non-porous, as well as slightly non-smooth surfaces are taken and successfully tested for latent fingerprints development with the prepared Sr4Al14O25: Eu2+,Dy3+ fluorescent nanophosphor powder. Present nano powder is advantageous to use on luminescent or multicolored surfaces as it gives greater contrast and also eliminates the problem of background interferences with the friction ridges due to its strong long after glow property. The results are very good when latent fingerprints were developed on the currency notes with optical variable ink and highly fluorescent pattern areas. 相似文献
8.
Pedro Villalba Manoj K. Ram Humberto Gomez Amrita Kumar Venkat Bhethanabotla Ashok Kumar 《Materials science & engineering. C, Materials for biological applications》2011,31(5):1115-1120
The importance of nanodiamond in biological and technological applications has been recognized recently, and applied in drug delivery, biochip, sensors and biosensors. Under this investigation, nanodiamond (ND) and nitrogen doped nanodiamond (NND) were deposited on n-type silicon films, and later functionalized with enzyme Glucose oxidase (GOX). The GOX functionalized doped and undoped ND films were characterized using combination of several techniques; i.e. FTIR spectroscopy, Raman spectroscopy, atomic force microscopy (AFM) and electrochemical techniques. ND/GOX and NND/GOX thin films on n-type silicon have been found to provide sensitive glucose sensor. GOX has been chosen as a model enzyme system to functionalize with ND at molecular level to understand the glucose biosensor. 相似文献
9.
Amrita Haldar Soniya D. YambemKang-Shyang Liao Nigel J. Alley Eoghan P. DillonAndrew R. Barron Seamus A. Curran 《Thin solid films》2011,519(18):6169-6173
Indium Tin Oxide (ITO) is the most commonly used anode as a transparent electrode and more recently as an anode for organic photovoltaics (OPVs). However, there are significant drawbacks in using ITO which include high material costs, mechanical instability including brittleness and poor electrical properties which limit its use in low-cost flexible devices. We present initial results of poly(3-hexylthiophene): phenyl-C61-butyric acid methyl ester OPVs showing that an efficiency of 1.9% (short-circuit current 7.01 mA/cm2, open-circuit voltage 0.55 V, fill factor 0.49) can be attained using an ultra thin film of gold coated glass as the device anode. The initial I-V characteristics demonstrate that using high work function metals when the thin film is kept ultra thin can be used as a replacement to ITO due to their greater stability and better morphological control. 相似文献
10.
Singha Amrita K.; McCance-Katz Elinore F.; Heck Stephanie A.; Kosten Thomas R.; Oliveto Alison 《Canadian Metallurgical Quarterly》1999,7(4):391
Twenty-six cocaine-abusing volunteers were trained to discriminate cocaine (80 mg/70 kg, p.o.) from placebo. On the basis of a discrimination acquisition criterion (i.e., >80% drug-appropriate responding for 4 consecutive sessions within 8–10 sessions), 18 participants were classified as discriminators (Ds) and 8 as nondiscriminators (NDs). Relative to Ds, NDs reported a greater amount of cocaine use per time. During the training phase, NDs showed significantly lower ratings than Ds on a stimulant ratings scale, regardless of the training drug condition. During the test-of-acquisition phase, cocaine-induced increases in scores on ratings of drug strength, anxious-nervous and cocaine high, as well as on a euphoria ratings scale, were significantly greater in Ds than NDs, relative to placebo. These results suggest that drug use history, general arousal level, and drug sensitivity may be important variables influencing the acquisition of cocaine versus placebo discrimination in cocaine abusers. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献