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1.
Vincent Cantarel David Lambertin Arnaud Poulesquen Fabrice Leroux Guillaume Renaudin Fabien Frizon 《Ceramics International》2018,44(9):10558-10568
This work investigates emulsion templating to synthesize hexadecane oil/geopolymer composites. In a system with hexadecane as the internal (dispersed) phase and an alkali activated continuous phase without added surfactant, adding aluminosilicate clay particles does not increase resistance against creaming or coalescence, while adding a surfactant (L35 or CTAB) stabilizes the solid-liquid interface. Infrared studies and rheological studies of the associated geopolymerization determined that the presence of the organic phase or surfactant has no significant effect on the geopolymerization kinetics, as determined by the change in time of the Si-O-T IR stretching frequency and the rheological moduli involved during the process. The stabilization of the organic template is reminiscent of Pickering emulsion even though we employ a much greater amount of inorganic material for geopolymer formation. Although the addition of surfactant has a significant effect on the behavior of the paste, the percolation of the network remains unmodified, highlighting the fact that the phenomenon is not dependent on viscosity. Finally, rheological measurements were used to obtain the mass fractal dimension of the as-made gel network, which is able to differentiate the interfacial effect between surfactant molecules with a slightly denser interphase when a cationic surfactant is used. 相似文献
2.
Observer-based estimators (OBE) were used for estimation of state variables and kinetic parameters in an anaerobic digestion (AD) process. A simplified first-order model with time-varying kinetic parameters was used to design an OBE for kinetic parameter estimation. This approach was validated on a laboratory-scale anaerobic reactor equipped with a multiwavelength fluorometer for on-line measurements of COD and VFA concentrations in the reactor effluent. The proposed estimators provide continuous adjustment of kinetic parameters and can be used for predictions of state variables between samples acquisition and during sensor failure. 相似文献
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In this work we present the discrete models for dynamic fracture of structures built of brittle materials. The models construction is based on Voronoi cell representation of the heterogeneous structure, with the beam lattice network used to model the cohesive and compressive forces between the neighboring cells. Each lattice component is a geometrically exact shear deformable beam which can describe large rigid body motion and the most salient fracture mechanisms. The latter can be represented through the corresponding form of the beam constitutive equations, which are derived either at microscale with random distribution of material properties or at a mesoscale with average deterministic values. The proposed models are also placed within the framework of dynamics, where special attention is paid to constructing the lattice network mass matrix as well as the corresponding time-stepping schemes. Numerical simulations of compression and bending tests is given to illustrate the models performance. 相似文献
5.
Arnaud C. Feron P. Boustimi M. Grosso P. Bosc D. Guignard P. 《Electronics letters》2003,39(17):1249-1250
Numerical results on polymer surrounded by an air micro-ring coupled to waveguides are presented. The FDTD method predicts a filter width of 1.4 nm and an extraction efficiency of almost 80% for a gap of 0.15 /spl mu/m. 相似文献
6.
The design of an adaptive nonlinear controller for the control of a fluidized bed reactor is derived by using exact linearization techniques. Reset action and parameter adaptation are used to make more robust the precise compensation of nonlinear terms, which is called for in the linearization technique. A nonlinear antiwindup mechanism is introduced to handle reset windup problem and to provide fast response without large overshoot. Simulation results show that the proposed adaptive controller guarantees good setpoint tracking. The developed estimation algorithm allows accurate estimation of the parameters for which the regressor component is not zero. 相似文献
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F. Riffard H. Buscail E. Caudron R. Cueff C. Issartel S. Perrier 《Corrosion Science》2003,45(12):2867-2880
The present results reveal the interest of sol–gel coating technique to improve 304 steel high temperature oxidation resistance. An yttrium sol–gel coating appears to enhance the oxidation resistance during isothermal oxidation test, to decrease widely the oxide weight gain and to reduce the initial transient oxidation stage generally observed in the case of blank steels. Moreover, the experimental results confirm that yttrium sol–gel coating also plays a significant role on the cyclic oxidation behaviour of the 304 steel. In fact, the yttrium addition promotes remarkably the prolongation of the period during which the oxide scale still remains adherent to the substrate. 相似文献
10.
This is the last part of a four-part survey of optimization models and solution algorithms for winter road maintenance planning. The two first parts of the survey address system design problems for winter road maintenance. The third part concentrates mainly on vehicle routing problems for spreading operations. The aim of this paper is to provide a comprehensive survey of optimization models and solution methodologies for the routing of vehicles for plowing and snow disposal operations. We also review models for the fleet sizing and fleet replacement problems. 相似文献