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2.
Sibel Akgün Gülsüm Ekici Nilüfer Mutlu Necati Beşirli Baki Hazer 《Journal of Polymer Research》2007,14(3):215-221
Modification of chitosan by grafting of vinyl butyrate was carried out in homogeneous phase using potassium persulfate as
redox initator and 1.5% acetic acid as solvent. The percent grafting and grafting efficiency were analysed and the high grafting
efficiency up to 94% was observed. The effects of reaction variables such as monomer concentration, initiator concentration,
temperature and reaction time were investigated. It was observed that the solubility of chitosan was markedly reduced after
grafting with vinyl butyrate. The grafted product is insoluble in common organic solvents as well in dilute organic and inorganic
acids. Characterization of the graft copolymers were carried out by using Fourier Transform Infrared Spectroscopy (FTIR),
Differential Scanning Calorimetry (DSC) and Scanning Electron Microscopy (SEM) technics. Characteristic signal of carbonyl
group was observed at 1,731 cm−1 which belongs to the poly vinyl butyrate segments in the graft copolymer. The melting transition of the chitosan main chain
in the copolymer shifted to 124°C from its original value 101°C. In addition to these, we have also studied topology of the
graft copolymer and the SEM micrograph showed continuous homogenous matrix which means there is no phase separation. 相似文献
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Martina Bečvářová 《NTM》2004,12(1):40-48
The paper describes the Czech project in the history of mathematics which was initiated at the Faculty of Mathematics and
Physics of Charles University in Prague at the end of the eighties of the 20th century. Its main aim is to map the development
of mathematical research in the Czech lands in the second half of the nineteenth and the first half of the twentieth century.
The main result of this project is the production of monographs. These chart out the life and work of some prominent Czech
personalities-mathematicians who have had substantial influence on the development of Czech mathematics. The aim of the project,
the structure of the monographs and the general method are discussed in the paper. 相似文献
5.
莱钢异型坯连铸机控制系统的研究与应用 总被引:1,自引:1,他引:1
介绍了莱钢异型坯连铸机的控制系统,并对一级、二级控制系统以及硬件、软件进行了较详细的论述。 相似文献
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8.
I. Bešlić L. Vranješ Markić J. Casulleras J. Boronat 《Journal of Low Temperature Physics》2013,171(3-4):436-442
The ground-state properties of spin-polarized deuterium with only one occupied nuclear spin state (D↓1) at zero temperature are studied by means of the variational Monte Carlo (VMC) method. Influence of the backflow correlations on the ground-state energy of this Fermi system under investigation is also explored. The calculations have been performed using several interatomic potentials and the quantum phase of the D↓1 system is discussed. Our results are compared with other previously reported variational results. 相似文献
9.
In the paper the main goals and progress of the surveillance specimen programme for the RPVs WWER-440/213 in Jaslovské Bohunice V-2 and Mochovce NPPs are presented. At Jaslovské Bohunice V-2, the standard surveillance specimen programme (SSSP) was finished and so-called ‘Extended Surveillance Specimen Programme’ (ESSP) was prepared on the base of its critical analysis. For first two units of the Mochovce NPP completely new programmes of irradiation embrittlement monitoring called ‘Modern Surveillance Specimen Programme’ is prepared. It is based on the experience with SSSP and ESSP as well as the recommendations of IAEA experts. This programme will serve for Mochovce NPP during all planned service life. The experience of ESSP application on the 3rd and 4th units in Jaslovské Bohunice V-2 NPP are presented in the paper too. 相似文献
10.
对5种国产复杂三维槽型刀片的断屑性能进行了试验研究,并对三维槽型结构要素的断屑机理及断屑特点进行了分析。 相似文献