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The efficiency of the process of refining technical boron nitride was assessed based on calculations of the chemical equilibrium in the B-N-O-C-Cl-H system. Three refining mixtures, CCl4 + H2, CCl4 + NH3 and CHCl3 + NH3, were considered. The analysis indicates that the use of ammonia-containing mixtures is more convenient, a lower residual oxygen content, lower contamination of the product by carbon and a better overall boron balance emerging. The calculations of the equilibrium composition of the solid phase enabled suitable technological conditions of the refining process (temperature and starting composition of the gaseous phase) to be established. The calculated results are compared with experimental data, and some observed differences are discussed. 相似文献
4.
T. Lalinsky J. Kuzmík D. Gregušová Ž. Mozolová J. Breza M. Feciško P. Seidl 《Journal of Materials Science: Materials in Electronics》1992,3(3):157-161
The formation of WN
x
/GaAs Schottky contacts using selective ion implantation of nitrogen into the sputtered tungsten film has been demonstrated. The contacts were characterized by Auger electron spectroscopy and current-voltage measurements. The composition of WN
x
films and the thermal stability of WN
x
/GaAs contacts were investigated. Good thermal stability of WN
x
/GaAs contacts compared with a W/GaAs contact was observed after capless rapid thermal annealing at 450, 800 and 950°C for 10 s. 相似文献
5.
Sibel Akgün Gülsüm Ekici Nilüfer Mutlu Necati Beşirli Baki Hazer 《Journal of Polymer Research》2007,14(3):215-221
Modification of chitosan by grafting of vinyl butyrate was carried out in homogeneous phase using potassium persulfate as
redox initator and 1.5% acetic acid as solvent. The percent grafting and grafting efficiency were analysed and the high grafting
efficiency up to 94% was observed. The effects of reaction variables such as monomer concentration, initiator concentration,
temperature and reaction time were investigated. It was observed that the solubility of chitosan was markedly reduced after
grafting with vinyl butyrate. The grafted product is insoluble in common organic solvents as well in dilute organic and inorganic
acids. Characterization of the graft copolymers were carried out by using Fourier Transform Infrared Spectroscopy (FTIR),
Differential Scanning Calorimetry (DSC) and Scanning Electron Microscopy (SEM) technics. Characteristic signal of carbonyl
group was observed at 1,731 cm−1 which belongs to the poly vinyl butyrate segments in the graft copolymer. The melting transition of the chitosan main chain
in the copolymer shifted to 124°C from its original value 101°C. In addition to these, we have also studied topology of the
graft copolymer and the SEM micrograph showed continuous homogenous matrix which means there is no phase separation. 相似文献
6.
Juskanič Dominik Mištinová Jana Poláková Hollý Samuel Sekerešová Monika Koleják Kamil Pátrovič Lukáš 《Magma (New York, N.Y.)》2022,35(1):45-52
Magnetic Resonance Materials in Physics, Biology and Medicine - Oncometabolite D-2-hydroxyglutarate (2HG) is pooled in isocitrate dehydrogenase (IDH)-mutant glioma cells. Detecting 2HG by MR... 相似文献
7.
A. Brahimi S. Alleg Z. Yamkane H. Lassri J. J. Suňol E. K. Hlil 《Journal of Superconductivity and Novel Magnetism》2017,30(11):3045-3054
The structure, morphology, and magnetic properties of the mechanically alloyed iron manganese phosphides (Fe1?x Mn x )2P with 0.15 ≤ x ≤ 0.75 (Mn/Fe ratio = 0.17, 0.33, 0.66, and 3) have been studied by means of X-ray diffraction, scanning electron microscopy coupled with energy-dispersive X-ray spectrometry, and BS1 and BS2 magnetometry. The powder form (Fe1?x Mn x )2P compounds exhibit multiphase structures that contain Fe(Mn)-type solid solution and Fe2P-type, Mn2P-type, Fe3P-type, and MnP/FeP-type phosphides. The magnetization versus temperature reveals the existence of multiple magnetic phase transitions. The saturation magnetization, coercivity, and squarness M r/M s ratio values are discussed as a function of both the Mn content and the temperature. From the approach to saturation magnetization studies, several fundamental magnetic parameters were extracted. The local magnetic anisotropy constant K 1 was determined. 相似文献
8.
We consider a system of Maxwell’s and Landau-Lifshitz-Gilbert equations describing magnetization dynamics in micromagnetism. The problem is discretized by a convergent, unconditionally stable finite element method. A multigrid preconditioned Uzawa type method for the solution of the algebraic system resulting from the discretized Maxwell’s equations is constructed. The efficiency of the method is demonstrated on numerical experiments and the results are compared to those obtained by simplified models. 相似文献
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We consider a problem of dynamic stochastic portfolio optimization modelled by a fully non-linear Hamilton–Jacobi–Bellman (HJB) equation. Using the Riccati transformation, the HJB equation is transformed to a simpler quasi-linear partial differential equation. An auxiliary quadratic programming problem is obtained, which involves a vector of expected asset returns and a covariance matrix of the returns as input parameters. Since this problem can be sensitive to the input data, we modify the problem from fixed input parameters to worst-case optimization over convex or discrete uncertainty sets both for asset mean returns and their covariance matrix. Qualitative as well as quantitative properties of the value function are analysed along with providing illustrative numerical examples. We show application to robust portfolio optimization for the German DAX30 Index. 相似文献