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1.
Joseph Breheny Cian Kingston Robert Doran Joao Anes Marta Martins Samus Fanning Patrick J. Guiry 《International journal of molecular sciences》2021,22(12)
Herein, we report antibacterial and antifungal evaluation of a series of previously prepared (+)-tanikolide analogues. One analogue, (4S,6S)-4-methyltanikolide, displayed promising anti-methicillin-resistant Staphylococcus aureus activity with a MIC of 12.5 µg/mL. Based on the antimicrobial properties of the structurally related (−)-malyngolide, two further analogues (4S,6S)-4-methylmalyngolide and (4R,6S)-4-methylmalyngolide bearing a shortened n-nonyl alkyl side chain were prepared in the present study using a ZrCl4-catalysed deprotection/cyclisation as the key step in their asymmetric synthesis. When these were tested for activity against anti-methicillin-resistant Staphylococcus aureus, the MIC increased to 50 µg/mL. 相似文献
2.
Raúl E. Cian Silvina R. Drago Rolando J. González 《International Journal of Food Science & Technology》2012,47(7):1348-1353
The effect of pH on colour and iron content (Fe) of peptide fractions obtained from bovine haemoglobin concentrate (BHC) hydrolysates was studied. Four hydrolysates were obtained using three enzymes: Protex‐6‐L (P), Fungal–Protease–Concetrate (FC) and Flavourzyme (F). BHC and its hydrolysates (P, FC, P + F, FC + F) were fractioned at pH 4.5, 7.0 and 9.5. Solubility and Fe from different fractions were measured. Correlations between CIELAB colour parameters and Fe from different fractions were analysed. The colour from different fractions varied from red to yellow (a* and b* positives). Lightness values (L*) ranged from twenty‐four to seventy. FC4.5 and FC + F4.5 fractions were the clearest and yellow (higher L*, b*, h), while BHC9.5 and P + F9.5 fractions had the lowest values of L*, b* and h. There was an inverse linear relationship between b* and L* parameters and Fe from fractions. This relationship could be associated with the pH of extraction. As pH increases Fe significantly increases and lower b* and L* values were obtained. 相似文献
3.
Taylor CM McCabe EM 《Journal of the Optical Society of America. A, Optics, image science, and vision》2002,19(7):1406-1416
Laser sources offer a possible solution to the problem of low light throughput in direct-view microscopes (DVMs). However, coherent source DVMs have been shown to suffer from problems such as increased sidelobes in the depth response because of coherent cross talk between neighboring apertures. We explore theoretically how source coherence affects the depth responses of DVMs by employing various aperture spacings and number of apertures. We show that, contrary to expectation, closely spaced apertures can result in decreased full width at half-maximum of the depth response curve. We explain this as an effect of destructive interference when cross talk between neighboring apertures occurs. Using apertures arranged in a square grid as an example, we move on to show that the use of aperture arrays that consist of regularly arranged apertures can accentuate the problematic sidelobes of the depth response. We show that arranging pinholes in a rectangular grid rather than a square grid can improve the optical sectioning strength significantly. Finally, by examination of the depth responses corresponding to the infinite-pinhole-array limit, we make some general statements about source coherence and the characteristics of arrays that are likely to perform well. 相似文献
4.
根据三峡工程永久船闸边坡块体分布,利用块体理论并结合支护情况探讨了三峡工程永久船闸边坡的稳定性,这对相关问题的研究将提供有益的借鉴作用。 相似文献
5.
We experimentally studied the three-dimensional imaging of the microspheres by using confocal and conventional scanning polarization microscopes. Because of the field amplitude averaging effect of the confocal system, the polarization of the detected signals is mainly parallel to the initial polarization. As a result, the signal intensity from the microspheres in the confocal polarization microscope with a crossed analyzer was found to be weaker than that in the conventional system. Based on a vector approach that takes the polarization into account and on the image formations of the two systems, theoretical expressions are given that agree well with the experimental results. 相似文献
6.
Najeb M. Abdul-Jabbar David L. Poerschke Cian Gabbett Carlos G. Levi 《Journal of the European Ceramic Society》2018,38(9):3286-3296
Phase equilibria in ZrO2-YO1.5-SiO2 (ZYS) and ZrO2-GdO1.5-SiO2 (ZGS) were experimentally assessed at 1400?°C and 1600?°C as they can offer insight on reactions between thermal barrier coatings (TBCs) based on ZrO2-YO1.5/GdO1.5 and molten silicate deposits in gas turbine engines. Features shared in both systems include the absence of ternary compounds and no ternary solubility in the binary phases. In ZYS however, a quaternary invariant reaction was observed that eliminates the zircon-disilicate equilibrium at higher temperatures. The results suggest no appreciable difference in the reactions between silica and thermal barrier oxides based on ZrO2-YO1.5 or ZrO2-GdO1.5, or environmental barrier coatings based on the corresponding Y/Gd silicates. The phase diagrams derived from these experiments are part of a broader effort to develop thermodynamic databases that can help guide the design of next-generation TBCs. 相似文献
7.
Raúl E. Cian Micaela Albarracín Antonela G. Garzón Silvina R. Drago 《International Journal of Food Science & Technology》2022,57(8):4832-4839
Sorghum flour was heat treated for producing an instant dispersion ingredient. The precooked sorghum flour was added with ACE-I and DPP-IV inhibitory sorghum peptides (3.0 g peptide 100 g−1). The product was reconstituted in water, and peptide bioaccessibility was evaluated by equilibrium dialysis method after simulated gastrointestinal digestion. Total peptide dialysability of precooked sorghum flour added with sorghum peptides was higher than those obtained for precooked sorghum flour (315.9 ± 14.8 vs. 45.2 ± 5.6 µmol, respectively) (P < 0.05). The ACE-I and DPP-IV-IC50 values of the bioaccessible peptides from the bioactive product were lower than those obtained for precooked sorghum flour ingredient (1.04 ± 0.12 vs. 1.82 ± 0.09 and 0.86 ± 0.02 vs. 2.12 ± 0.08 mg protein mL−1, for ACE-I and DPP-IV, respectively) indicating a higher activity. Precooked sorghum flour was a good vehicle since it did not affect the bioaccessibility of ACE-I and DPP-IV inhibitory peptides provided by sorghum protein hydrolysate. 相似文献
8.
9.
研究了三峡工程高程120m施工栈桥钢筋混凝土T形梁的荷载试验方法、试验成果,并对试验成果进行了评价分析,其研究结果对类似工程结构具有借鉴作用。 相似文献
10.
Cian O’LoinsighMarc Oudjene Elisabeth ShottonAntonio Pizzi Paul Fanning 《Composite Structures》2012,94(2):313-321
This paper presents experimental and numerical investigations on multi-layered timber beams using welded-through wood dowels in place of traditional poly(vinyl acetate) (PVAc)-adhesives (or metallic nails). Four-layer beams were constructed with varying numbers of dowels, in each, and then loaded using four-points bending tests to evaluate the mechanical performance of these beams. The practical difficulties encountered in constructing deeper multi-layer beams are discussed and possible solutions which have been employed for the purpose of this work, and proved successful are presented. In order to investigate thoroughly the full potential of multi-layered beams with a very limited number of experimental studies, a 3D FE model has been presented, validated against experimental results and then used to study some influential parameters. The results showed that a reasonable bending stiffness of multi-layered beams is achievable with a good combination of material and geometric parameters. 相似文献