The use of direct tension tests for the assessment of low temperature properties of bituminous binders

In France, tensile tests on bituminous binders are usually performed on vertical electromechanical loading frames, the test samples being placed in an insulated temperature control chamber and the deformations determined from the displacement of the cross-head. The paper presents the results of an inter-laboratory study of which the objective was to evaluate the suitability of this kind of equipment for the performance of direct tension tests at low temperatures. Most of the test parameters, used for this study complied with the procedure proposed by SHRP as from 1995 (AASHTO TP3). The various operating factors, and more particularly those affecting the determination of true sample elongation (mechanical plays, deformation of the gripping systems, ....), are discussed and a number of correcting procedures are proposed. Nevertheless, the results remained scattered. Considering the “flat” evolution of strain at failure with temperature in the domain of brittle behaviour, this makes it rather difficult to accurately define the temperature for failure at 1% elongation (T_ε=1%). This is also the case when this temperature is located in the zone of transition between brittle and ductile behaviour. The authors suggest that, together with the corresponding tensile strain, this “transition temperature” could be used as an alternative criterion which has the advantage of being linked to a physical behaviour of the material.     

"I non-exist". Paradoxes of death in adolescence

This text presents, from the case study of the analytical treatment of a young girl after a very serious suicide attempt, a theoretical reflection on the question of death during adolescence and its place and function in the psyche. The hypothesis suggested is that resorting to the "idea of death" constitutes an attempt to neutralise the excitement created by the excess of representational activities. A parallel is suggested between the way death and pain are used as a protective shield.     

IR spectroscopy approach for the study of interactions between an oxidized aluminium surface and a poly(propylene-g-acrylic acid) film

In this paper, we report the study of the interactions between a poly(propylene-g-acrylic acid) and an oxidized aluminium surface by IR spectroscopy. A deposit of a pure poly(acrylic acid) on the same surface is used as a model. Under free acid form (COOH) we demonstrate the formation of hydrogen bondings between the acrylic carboxyl groups and OH functions located at the surface of alumina. This is characterized by an IR absorption [v_(c?o)] at 1733 or 1743 cm^?1 when we observe the metal surface either after peeling of a PPg(OH) film initially pressed on it or after a deposit of PAA(OH). Under the carboxylate form (COO^?), we observe two modes of interaction, the one purely ionic between COO^? and Al³⁺ with an absorption located near 1550 cm^?1 and the other of complex form between COO^? and Al³⁺ giving a band near 1610 cm^?1. The water molecules can play a major part, in particular in the first case (COOH) where they destroy hydrogen bondings in favor of the formation of ? COO^? groups, interacting with the metal surface according to ionic or complex modes as above. © 1993 John Wiley & Sons, Inc.     

Study of the effects of structural uncertainties on a fractional system of the first kind – application in vibration isolation with the CRONE suspension

In this paper, we deal with the effects of the uncertainties on a fractional system of the first kind, mainly on the frequency-domain and the time-domain responses. For the structural uncertainties, two main aspects are studied: the nonlinearities of the physical components used to realize the fractional system and the consideration of the previously neglected dynamics of the system. Both uncertainties are introduced for the hydropneumatic CRONE suspension, previously synthesized and realized without taking into consideration these uncertainties. So, the novel approach treated in this work is to find whether the uncertainties, which were previously neglected in the synthesis and the realization phases, alter the behaviour of the system or not. The results show that the fractional order system behaviour is not affected.     

Extension of the Hansen-Bliek Method to Right-Quantified Linear Systems

The problem of finding the smallest box enclosing the united solution set of a linear interval system, also known as the “interval hull” problem, was proven to be NP-hard. However, Hansen, Bliek, and others subsequently, have provided a polynomial-time solution in the case of systems preconditioned by the midpoint inverse matrix. Based upon a similar approach, this paper deals with the interval hull problem in the context of AE-solution sets, where parameters may be given different quantifiers. A polynomial-time algorithm is proposed for computing the hull of AE-solution sets where parameters involved in the matrix are constrained to be existentially quantified. Such AE-solution sets are called right-quantified solution sets. They have recently been shown to be of practical interest.     

The effect of radiopacifiers agents on pH,calcium release,radiopacity, and antimicrobial properties of different calcium hydroxide dressings

The aim of this study was to evaluate the antimicrobial activity, pH level, calcium ion release, and radiopacity of calcium hydroxide pastes associated with three radiopacifying agents (iodoform, zinc oxide, and barium sulfate). For the pH and calcium release tests, 45 acrylic teeth were utilized and immersed in ultrapure water. After 24 h, 72 h, and 7 days the solution was analyzed by using a pH meter and an atomic absorption spectrophotometer. Polyethylene tubes filled with the pastes were used to perform the radiopacity test. For the antimicrobial test, 25 dentin specimens were infected intraorally in order to induce the biofilm colonization and treated with the pastes for 7 days. The Live/Dead technique and a confocal microscope were used to obtain the ratio of live cells. Parametric and nonparametric statistical tests were performed to show differences among the groups (P < 0.05). The pH analysis at 7 days showed significant differences (P < 0.05) among the groups. No differences among the pastes were found in the calcium release test on the 7th day (P > 0.05). The calcium hydroxide/iodoform samples had the highest radiopacity and antimicrobial activity against the biofilm‐infected dentin in comparison to the other pastes (P < 0.05). Calcium hydroxide mixed with 17% iodoform and 35% propylene glycol into a paste had the highest pH, calcium ion release, radiopacity, and the greatest antimicrobial action versus similar samples mixed with BaSO4 or ZnO. Microsc. Res. Tech. 78:620–625, 2015. © 2015 Wiley Periodicals, Inc.     

Brazing of UNS S32101 and UNS S32304 lean duplex stainless steels and UNS S32750 super duplex with AWS A5.3 BNi-7 (Ni–Cr–P) filler metal

Summary

Weld metals solidified in the ferritic-austenitic solidification mode (FA mode) have dual phases of ferrite and austenite in their as-solidified condition, where ferrite exhibits different morphologies depending on the chemical composition and welding conditions. This paper describes an investigation of the effect of the solidification and transformation sequence on the formation of final ferrite morphologies. Austenite is formed through either a eutectic reaction or peritectic reaction at the dendrite boundaries after the primary formation of ferrite. During the eutectic formation of austenite, the <100>_δ direction of the primary ferrite and the <100>_γ direction of the eutectic austenite are parallel to each other and lie along the growth direction of the primary dendrites. However, any specific lattice plane relationship between the two phases is not identified. During cooling after solidification, the austenite extends into the primary ferrite via solid-state transformation, and the final morphology of the ferrite is vermicular without any coherent orientation relationship between the primary ferrite and eutectic austenite. During peritectic formation of austenite, the Kurdjumov-Sachs orientation relationship is established between the primary ferrite and peritectic austenite, and the <100>_γ direction of the peritectic austenite is not parallel to the growth direction of the primary dendrites. During cooling after solidification, the primary ferrite transforms into austenite, and the final morphology of the ferrite is lathy, since the primary ferrite and peritectic austenite have a favourable coherent orientation.     

Improving inter-block backtracking with interval Newton

Inter-block backtracking (IBB) computes all the solutions of sparse systems of nonlinear equations over the reals. This algorithm, introduced by Bliek et al. (1998) handles a system of equations previously decomposed into a set of (small) k ×k sub-systems, called blocks. Partial solutions are computed in the different blocks in a certain order and combined together to obtain the set of global solutions. When solutions inside blocks are computed with interval-based techniques, IBB can be viewed as a new interval-based algorithm for solving decomposed systems of nonlinear equations. Previous implementations used Ilog Solver and its IlcInterval library as a black box, which implied several strong limitations. New versions come from the integration of IBB with the interval-based library Ibex. IBB is now reliable (no solution is lost) while still gaining at least one order of magnitude w.r.t. solving the entire system. On a sample of benchmarks, we have compared several variants of IBB that differ in the way the contraction/filtering is performed inside blocks and is shared between blocks. We have observed that the use of interval Newton inside blocks has the most positive impact on the robustness and performance of IBB. This modifies the influence of other features, such as intelligent backtracking. Also, an incremental variant of inter-block filtering makes this feature more often fruitful.