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1.
The telomerization of dimethylaminoethyl methacrylate (DMAEMA) with mercaptoethanol initiated by 2,2′-azobisisobutyronitrile was first investigated at 70 °C and the influence of the type of solvent was studied. The results showed that well-defined telomers of DMAEMA could not be synthetized via telomerization of DMAEMA in water or water/acetonitrile mixture since the telomerization reaction is in competition with the nucleophilic addition of thiol onto the monomer. Transfer constants for mercaptoethanol in benzene and acetonitrile were determined by Mayo's and O'Brien's methods. The transfer constant obtained in acetonitrile (0,6) was higher than that obtained in benzene. This difference can be explained by the fact that the thiol was consumed by two reactions: nucleophilic addition and telomerization. The influence of solvents on the polymerization kinetics was enlightened. These results were applied to the synthesis of macromonomers of DMAEMA with isocyanatoethyl methacrylate (IEM). These macromonomers were copolymerized with styrene. 相似文献
2.
Topology identification of complex networks is an important problem. Existing research shows that the synchronization of network nodes is an obstacle in the identification of network topology. Identification of the structure of the network presents an interesting challenge during the synchronization of complex networks. We developed a new method using the sinusoidal disturbance to identify the topology when the complex network achieves synchronization. Compared with the disturbance of all the nodes, the disturbance of the key nodes alone can achieve a very good effect. Finally, numerical simulation data are provided to validate our hypothesis. 相似文献
3.
Cyrille Artho 《International Journal on Software Tools for Technology Transfer (STTT)》2011,13(3):223-246
Automated debugging attempts to locate the reason for a failure. Delta debugging minimizes the difference between two inputs,
where one input is processed correctly while the other input causes a failure, using a series of test runs to determine the
outcome of applied changes. Delta debugging is applicable to inputs or to the program itself, as long as a correct version
of the program exists. However, complex errors are often masked by other program defects, making it impossible to obtain a
correct version of the program through delta debugging in such cases. Iterative delta debugging extends delta debugging and
removes a series of defects step by step, until the originally unresolved defect is isolated. The method is automated and
managed to localize a bug in some real-life examples. 相似文献
4.
Zaid M. Odibat Cyrille Bertelle M.A. Aziz-Alaoui Gérard H.E. Duchamp 《Computers & Mathematics with Applications》2010,59(4):1462-1472
The differential transform method (DTM) is an analytical and numerical method for solving a wide variety of differential equations and usually gets the solution in a series form. In this paper, we propose a reliable new algorithm of DTM, namely multi-step DTM, which will increase the interval of convergence for the series solution. The multi-step DTM is treated as an algorithm in a sequence of intervals for finding accurate approximate solutions for systems of differential equations. This new algorithm is applied to Lotka–Volterra, Chen and Lorenz systems. Then, a comparative study between the new algorithm, multi-step DTM, classical DTM and the classical Runge–Kutta method is presented. The results demonstrate reliability and efficiency of the algorithm developed. 相似文献
5.
Damien Trentesaux Cyrille Pach Abdelghani Bekrar Yves Sallez Thierry Berger Thérèse Bonte Paulo Leitão José Barbosa 《Control Engineering Practice》2013,21(9):1204-1225
Benchmarking is comparing the output of different systems for a given set of input data in order to improve the system’s performance. Faced with the lack of realistic and operational benchmarks that can be used for testing optimization methods and control systems in flexible systems, this paper proposes a benchmark system based on a real production cell. A three-step method is presented: data preparation, experimentation, and reporting. This benchmark allows the evaluation of static optimization performances using traditional operation research tools and the evaluation of control system's robustness faced with unexpected events. 相似文献
6.
Vision-Based SLAM: Stereo and Monocular Approaches 总被引:1,自引:0,他引:1
Thomas Lemaire Cyrille Berger Il-Kyun Jung Simon Lacroix 《International Journal of Computer Vision》2007,74(3):343-364
Building a spatially consistent model is a key functionality to endow a mobile robot with autonomy. Without an initial map
or an absolute localization means, it requires to concurrently solve the localization and mapping problems. For this purpose,
vision is a powerful sensor, because it provides data from which stable features can be extracted and matched as the robot
moves. But it does not directly provide 3D information, which is a difficulty for estimating the geometry of the environment.
This article presents two approaches to the SLAM problem using vision: one with stereovision, and one with monocular images.
Both approaches rely on a robust interest point matching algorithm that works in very diverse environments. The stereovision
based approach is a classic SLAM implementation, whereas the monocular approach introduces a new way to initialize landmarks.
Both approaches are analyzed and compared with extensive experimental results, with a rover and a blimp. 相似文献
7.
Michelle Pinault Cyrille Guimaraes Jean‐Franois Dumas Stphane Servais Stephan Chevalier Pierre Besson Caroline Goupille 《European Journal of Lipid Science and Technology》2020,122(2)
The aim of this study is to identify high performance thin layer chromatography (HPTLC) conditions allowing the separation and quantification of mammalian cellular phospholipids (PLs) (sphingomyelin, phosphatidylcholine, phosphatidylserine, phosphatidylinositol, phosphatidylethanolamine, and especially phosphatidic acid, cardiolipin, and monolysocardiolipin, these latter two being specifically located in mitochondria membranes). In order to make this method faster and easier, a 1D HPTLC method is chosen, testing several eluents as well as several staining methods. A pre‐conditioning of HPTLC plates with boric acid and a copper staining reagent followed by carbonization are selected for the quality of PL separation and homogeneity of staining. The selected conditions are discussed and the method validation is performed according to the International Conference on Harmonization guidelines. Linearity is effective between 1 and 8 µg and limit of quantification is between 0.5 and 2.3 µg depending on PL classes. Precision measurements show coefficients of variation <6%, and when amounts are close to the detection limit, <12%. Lipid extracts of tumor cell lines or isolated mitochondria are used to assess PL profiles. This shows that the HPTLC method can be used routinely to follow level variations of PLs. Practical Applications: The changes in PL composition play a crucial role in tumor processes and regulate cellular functions modulating cellular signaling or mitochondrial metabolism. The simple and cost‐effective 1D HPTLC method that is developed is applied to lipid extracts of whole tumor cells or hepatocyte‐isolated mitochondria. It is sensitive as well as precise to detect variations of phosphatidic acid or cardiolipin levels linked to physio‐pathological conditions. It can also be used to investigate the composition changes of other membrane PLs. Moreover, with a simultaneous analysis of 14 samples/standards on the same plate (six plates per day), this method is adapted for large series of samples. 相似文献
8.
Teresa A. Vidal-CallejaAuthor Vitae Cyrille BergerAuthor Vitae Joan SolàAuthor Vitae Simon LacroixAuthor Vitae 《Robotics and Autonomous Systems》2011,59(9):654-674
This paper addresses the cooperative localization and visual mapping problem with multiple heterogeneous robots. The approach is designed to deal with the challenging large semi-structured outdoors environments in which aerial/ground ensembles are to evolve. We propose the use of heterogeneous visual landmarks, points and line segments, to achieve effective cooperation in such environments. A large-scale SLAM algorithm is generalized to handle multiple robots, in which a global graph maintains the relative relationships between a series of local sub-maps built by the different robots. The key issue when dealing with multiple robots is to find the link between them, and to integrate these relations to maintain the overall geometric consistency; the events that introduce these links on the global graph are described in detail. Monocular cameras are considered as the primary extereoceptive sensor. In order to achieve the undelayed initialization required by the bearing-only observations, the well-known inverse-depth parametrization is adopted to estimate 3D points. Similarly, to estimate 3D line segments, we present a novel parametrization based on anchored Plücker coordinates, to which extensible endpoints are added. Extensive simulations show the proposed developments, and the overall approach is illustrated using real-data taken with a helicopter and a ground rover. 相似文献
9.
We address in this paper the issue of computing diffuse global illumination solutions for animation sequences. The principal difficulties lie in the computational complexity of global illumination, emphasized by the movement of objects and the large number of frames to compute, as well as the potential for creating temporal discontinuities in the illumination, a particularly noticeable artifact. We demonstrate how space‐time hierarchical radiosity, i.e. the application to the time dimension of a hierarchical decomposition algorithm, can be effectively used to obtain smooth animations: first by proposing the integration of spatial clustering in a space‐time hierarchy; second, by using a higher‐order wavelet basis adapted for the temporal dimension. The resulting algorithm is capable of creating time‐dependent radiosity solutions efficiently. 相似文献
10.
asr affected concrete in real structures is usually subject to loads which affect the macroscopic expansion of the material. An experimental study was undertaken using sensors embedded in reactive and non-reactive samples loaded on modified creep frames. Numerical analysis was used to link micro-structural damage under the load to expansion. We show that load influences the micro-crack propagation, which changes the shape of the expansion curve. 相似文献