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排序方式: 共有750条查询结果,搜索用时 31 毫秒
1.
Thermally conductive polymers offer new possibilities for the heat dissipation in electric and electronic components, for example, by a three‐dimensional shaping of the heat sinks. To face safety regulations, improved fire performance of those components is required. In contrast to unfilled polymers, those materials exhibit an entirely different thermal behavior. To investigate the flammability, a phosphorus flame retardant was incorporated into thermally conductive composites of polyamide 6 and hexagonal boron nitride. The flame retardant decreased the thermal conductivity only slightly. However, the burning behavior changed significantly, due to a different heat propagation, which was investigated using a thermographic camera. An optimum content of hexagonal boron nitride for a sufficient thermal conductivity and fire performance was found between 20 and 30 vol%. The improvement of the fire performance was due to a faster heat release out of the pyrolysis zone and an earlier decomposition of the flame retardant. For higher contents of hexagonal boron nitride, the heat was spread faster within the part, promoting an earlier ignition and increasing the decomposition rate of the flame retardant. 相似文献
2.
Vladimir Rozenshtein Alexander Berg Haim Levanon Uwe Krueger Dietmar Stehlik Yuri Kandrashkin Art Van Der Est 《Israel journal of chemistry》2003,43(3-4):373-381
Light-induced spin-polarized transient EPR spectra are reported for several water-soluble copper porphyrins. The spectra are assigned to the doublet ground state, with emissive spin polarization resulting from photoexcitation and subsequent electronic relaxation. In contrast to other systems for which polarization of a doublet ground state has been observed, the exchange interactions in the copper porphyrins are strong and the geometry is fixed. It is proposed that intersystem crossing from the photoexcited trip-doublet to the trip-quartet state can lead to net polarization of the spin system and that this polarization is maintained during electronic decay, possibly via charge-transfer and exciplex states. The intensity of the observed spin polarization is essentially independent of the molecular orientation in the external field, but is strongly dependent on the nature of the charged peripheral groups. Possible reasons for this behavior are discussed. 相似文献
3.
Dietmar Schulze 《化学,工程师,技术》1995,67(1):60-68
Flowability of Bulk Solids – Definition and Measuring Principles . The flowability of bulk solids has to be known for many practical applications. The present paper describes how the flowability is defined and on which physical properties it depends. Experimental determination of the flowability using a shear test is demonstrated. Conditions influencing measuremed results are described. Finally an overview of various methods used for characterization of the flowability of bulk solids is given. 相似文献
4.
Cell suspensions of Escherichia coli as a model for bacterial populations in wastewaters were treated with ozone as a disinfectant in a continuously operated pilot plant with a plug flow reactor. Suspensions with an initial number of CFU (colony forming units) of 108 mL?1 were ozonized with ozone concentrations up to 12 mg/L. Metabolic activities and membrane functions break down with increasing ozone concentrations. The fluorochromization using 3′,6′-diacetylfluorescein (FDA) proved to be a suitable method for the detection of an alteration in permeability of the cell membranes and an inactivation of metabolic activity. By fluorescence microscopic and photometric investigations it could be clearly demonstrated that, in the case of disinfection with ozone, inactivation of the cells includes first of all a damage of the cell membranes. In contrast to the determination of the number of CFU, fluorochromization allows the detection of alteration in metabolic activities. 相似文献
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7.
In connection with the analysis and the development of failure concepts in fracture mechanics for quasistatic loaded components and elastic-plastic behaviour of the material, tests are also carried out with welded and/or complex shaped specimens or structures. Thereby the difficulty arises of generating reproducible flaws in the form of fatigue precracks in definite positions in the components, respectively in the welded joint. It is reported exemplarily about experiments on different CT25 and CCT specimens and on a pressure vessel which contained a fatigue pre-crack, a 0.2 mm saw cut or notches with notch root radius ≤ ≥ 0.1 mm as flaws. The comparison of the results with regard to J-integral at initiation of stable crack, Ji, and JR curves shows that under certain conditions the 0.2 mm saw cut (notch root radius ≤ ≤ 0.02 mm) is a useful alternative, if reproducible generation of a fatigue pre-crack will not be successful or too expensive. The tests were carried out on StE 460 and on a welded joint of this steel at 25 ± 2°C. 相似文献
8.
Dietmar Köther 《Journal of Infrared, Millimeter and Terahertz Waves》1987,8(11):1365-1389
In the following paper some different kinds of microwave guides will be inspected under main aspect of higher order modes. The knowledge of these modes is important for field matching problems at discontinuities and for suppressing propagation of higher order modes by geometrical variations. In some cases it is sufficient to know their principal behaviour. They will be calculated in paper by the often used orthogonal expansion. This method allows to determine all kinds of waves: propagating, damping and complex waves. The following guides are inspected:
- rectangular waveguides,
- circular waveguides,
- L-shaped waveguides,
- double ridged rectangular waveguides,
- unilateral finlines with one slot,
- unilateral finlines with two slots,
- shielded microstrip lines,
- circular image guides,
- rectangular waveguides with dielectric slab,
- H-guides.
9.
In the current study, the development of the silicate structure of synthetic calcium silicate hydrates with different calcium contents was followed by in-situ infrared (IR) spectroscopy and correlated to the in-situ phase development evaluated by X-ray diffraction (XRD). A baseline correction method initially developed for X-ray diffractograms was successfully adapted for the complex background of the fingerprint region in in-situ IR, which significantly contributed to signal quality and reproducibility. The development of separate silicate infrared bands could be monitored over 24 h of reaction. These bands could be assigned to oligomeric and dimeric species based on their time and stoichiometry-dependent development. It was clearly shown that the main peak of the dimeric silicate species was overlooked in the literature. The correlation of time-dependent events to in-situ XRD revealed that changes in the unit cell of calcium silicate hydrate are related to silicate polymerization. The results were compared to 29Si-MAS-NMR, which highlighted the benefits of in-situ IR spectroscopy. 相似文献
10.