Fabrication of barium titanate ceramics via digital light processing 3D printing by using high refractive index monomer

A digital light processing (DLP) technology has been developed for 3D printing lead-free barium titanate (BTO) piezoelectric ceramics. By comparing the curing and rheological properties of slurries with different photosensitive monomer, a high refractive index monomer acryloyl morpholine (ACMO) was chosen, and a design and preparation method of BTO slurry with high solid content, low viscosity and high curing ability was proposed. By further selecting the printing parameters, the single-layer exposure time was reduced and the forming efficiency has been greatly improved. Sintered specimens were obtained after a nitrogen-air double-step debinding and furnace sintering process, and the BTO ceramics fabricated with 80 wt% slurry shows the highest relative density (95.32 %) and piezoelectric constant (168.1 pC/N). Furthermore, complex-structured BTO ceramics were prepared, impregnated by epoxy resin and finally assembly made into hydrophones, which has significance for the future design and manufacture of piezoelectric ceramic-based composites that used in functional devices.     

Facile synthesis of Li 2 ZrO 3 -modified LiNi 0.5 Mn 0.5 O 2 cathode material from a mechanical milling route for lithium-ion batteries

Li2ZrO3-modified LiNi0.5Mn0.5O2 materials with improved electrochemical performance were directly synthesized by a simple mechanical milling route with ZrO2, Li2CO3 and Ni0.5Mn0.5(OH)2 precursors...     

Advanced Surface of Fibrous Activated Carbon Immobilized with FeO/TiO2 for Photocatalytic Evolution of Hydrogen under Visible Light

FeO-doped TiO₂ nanoparticle photocatalysts were immobilized onto the surface of fibrous activated carbon (ACF) via a sol-gel process. As an adsorbent and photocatalyst, FeO-TiO₂ on immobilized ACFs (FeO-TiO₂/ACF) greatly improved the photocatalysis rate of hydrogen production as compared with pure TiO₂ and ACF-TiO₂ under UV irradiation and visible light. The addition of ACFs surface significantly reduced the photogenerated pairs of electrons-hole recombination, thereby promoting the photocatalysis action of doped photo-metal oxides of FeO-TiO₂. Co-doping of FeO onto the lattice of the TiO₂ approach can improve the absorption activity of visible light through photo-metal oxide of TiO₂ and further enhance hydrogen production under visible light. The photocatalytic fabrics (FeO-TiO₂/ACF) were effortlessly split out from the experimental solution for re-utilization and exhibited high stability even after five complete regeneration cycles.     

Abrasive wear of dental composite resins

Abrasive wear is a major problem in the application of dental composite resins. In this study the friction and wear behaviours of two types of dental composites: one containing relatively coarse filler particles and some microfillers (Estilux) and another containing only microfiller particles (Durafill), have been investigated by using a scratch testing machine. Experimental results show that the coefficients of friction in both composites are essentially constant for applied loads up to 20 N. The wear resistance of Durafill is better than Estilux. Under the same testing conditions, the size, shape and distribution of the filler particles are more important variables than applied load and sliding speed in controlling the wear mechanism. It is shown that for Estilux, plastic ploughing by the diamond indenter is the predominant mechanism. For Durafill, however, the formation and propagation of tensile cracks on the worn surface is the main wear mechanism. The effects of two different indenters, diamond and enamel, on the basic wear mechanisms are also discussed.     

In situ SEM studies on the effects of particulate reinforcement on fatigue crack growth mechanism of aluminium-based metal-matrix composite

The effects of particulate reinforcement on the fatigue behaviour and fatigue mechanisms of two 6061 aluminium-based metal-matrix composites (MMCs) in three different heattreatment conditions were studied in situ with a scanning electron microscope and compared to the unreinforced alloy in the as-received condition. It was observed that the fatigue properties of the MMCs were influenced by the ceramic particles in two ways: firstly the particles increased the fatigue stress intensity threshold mainly by crack-deflection and crack-closure mechanisms, and secondly, the particles raised the fatigue crack growth rates in the Paris region by providing an easy crack path. The effect of ageing was small on the fatigue stress intensity threshold of MMCs, but for the peak-aged MMCs the fatigue crack growth rates in the Paris region were faster. The mechanism of fatigue crack growth was largely associated with the matrix/particle interface and the linkage with subcracks initiated ahead of the main crack at high applied stress intensity factors.     

32位实时操作系统FCCRTOS的设计与实现

介绍了自行设计的，不依赖其他软件支持而存在，可直接运行在Ｉｎｔｅｌ８０３７６、８０３８６、８０４８６和８０５８６处理器的计算机上，便于移植的一个完全独立的实时操作系统—ＦＣＣＲＴＯＳ。其特点为：３２位寻址、内存保护模式的段式管理、多任务并发处理、实时事件线程管理、支持多总线通信协议、模块化设计及目标程序完全ＲＯＭ化等。     

单模光纤中模耦合微扰功率谱与偏振关系的研究

提出用测量光纤偏振耦合率来确定模耦合系数，从而得到耦合微扰功率谱与双折射关系。它给出了光纤拉制中微扰作用 的信息，是研制偏振光纤的一种有效方法。     

Micromechanical characterisation of fibre/matrix interfaces

Theoretical analyses for the single fibre pull-out and push-out models under monotonic loading are given which are based on a shear-lag analysis in a fracture mechanics approach considering non-constant friction at the debonded interface as a result of fibre Poisson contraction (or expansion). The solutions allow the determination of typical fibre/matrix interfacial properties such as the interfacial fracture toughness, G_ic, the coefficient of friction, μ, and the residual clamping stress, q₀. Under cyclic loading the interfacial properties are expected to degrade as a result of repetitive abrasion, and a power law function is assumed between μ and the number of elapsed cycles, N. However, G_ic is assumed to be unaffected and a fracture mechanics based debond criterion is derived for the relationship between the external applied stress, the debond length and the reduced friction coefficient for both fibre pull-out and fibre push-out. In addition, the relative displacements between the free fibre end and the matrix top are obtained for cyclic fatigue when the fibre is loaded and unloaded. A relationship obtained for the protrusion (or intrusion) length in fibre pull-out (or push-out) experiments allows the severity of the interface frictional degradation to be evaluated and characterised. Similarities and differences in the frictional degradation behaviour between fibre pull-out and push-out are also identified.