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1.
The effect of controlled heterogeneous nucleation by platinum on the crystallization of a ZrF4-BaF2-LaF3-AlF3-NaF (ZBLAN) glass was studied. Various levels of platinum were incorporated into this glass by a combination of PtCl2-doping and melting-atmosphere variation. The effect of doping levels and melting conditions on the incorporation of platinum and the subsequent nucleation of crystals was studied by optical microscopy, scanning electron microscopy, differential scanning calorimetry (DSC), and X-ray diffraction. Increased platinum in the glass resulted in an increased number of nucleation sites for the growth of β-ZrF4-BaF2 crystals. Analysis of isothermal and ramp-rate DSC measurements indicated that the crystallization of this glass changed from surface controlled to bulk controlled with an increased number of nuclei. This was confirmed by optical microscopy. In addition, Avrami analysis of the isothermal crystallization data gave an accurate approximation of the number of nuclei in the glass.  相似文献   
2.
This paper demonstrates the use of TissueQuant - an image analysis tool for quantification of color intensities which was developed for use in medical research where the stained biological specimen such as tissue or antigen needs to be quantified. TissueQuant provides facilities for user interaction to choose and quantify the color of interest and its shades. Gaussian weighting functions are used to provide a color score which quantifies how close the shade is to the user specified reference color. We describe two studies in medical research which use TissueQuant for quantification. The first study evaluated the effect of petroleum-ether extract of Cissus quadrangularis (CQ) on osteoporotic rats. It was found that the analysis results correlated well with the manual evaluation, p < 0.001. The second study evaluated the nerve morphometry and it was found that the adipose and non adipose tissue content was maximum in radial nerve among the five nerves studied.  相似文献   
3.
Gobinath  V. K.  Rajasekar  R.  Santhosh  S.  Moganapriya  C.  Sri  A. Manju  Jaganathan  S. K. 《SILICON》2022,14(15):9773-9788
Silicon - Antireflection coatings (ARCs) have become one of the key techniques for mass production of Si solar cells. They are generally performed by vacuum processes such as thermal evaporation,...  相似文献   
4.
An experimental study has been carried out on a continuously operated pilot fractional distillation column equipped with an external heat pump. The distillation column was a 15 cm internal diameter glass unit containing eleven single bubble cap plates. A methanol-water mixture was fed to the column. After operating the heat pumps with R114 as the working fluid, further experiments have been conducted with R11 as the working fluid. Plots of pressure against enthalpy, condensation pressure and latent heat of vaporization against condensation temperature and theoretical Rankine coefficient of performance against gross temperature lift and condensation temperature are presented for both R114 and R11. R11 has correspondingly higher theoretical Rankine coefficients of performance than R114. The experiments show that the actual coefficients are also higher for R11 than for R114. A maximum actual coefficient of performance of 5.3 was obtained using R11 as the working fluid with a gross temperature lift of 38.4°C. The experimental data for R11 were found to be reproducible during operation over a number of weeks. This showed that the relative thermal instability of R11 compared to R114 had not apparently affected the performance of the system.  相似文献   
5.
Determining permeability of fibrous media is of great importance to many industries. While there are several 2-D and 3-D analytical models developed for predicting the permeability of fibrous disordered media, there are not many numerical works that compare the predictions of these models with that of real media. In this work, we present a series of numerical simulations performed on the microstructure of a real fibrous media. An efficient procedure is presented for reconstructing 3-D images from the 2-D images of the real fibrous media and processing them for the purpose of performing fluid flow simulation. Digital volumetric imaging (DVI) of a typical hydroentangled fibrous fabric is obtained, as an example, and its permeability is computed. These results are compared with those obtained from the analytical equations given in the literature. In particular, it was found that permeability of a typical hydroentangled material can be closely predicted by the layered anisotropic models.  相似文献   
6.
A theoretical analysis of mass transfer effects in ethyl cellulose manufacture has been reported. This is the first model to describe a complex fluid–solid reaction in the presence of two immiscible liquids. The model derived here can be used to evaluate the dependency of the overall rate on different parameters incorporating the multiphase mass transfer effects.  相似文献   
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In the present study, pre-treated paper mill sludge (PMS) was evaluated extensively as a substrate for production of acetone-butanol-ethanol using Clostridium sporogenes NCIM 2337. The PMS was subjected to three types of pre-treatment methods namely alkali, mechanical, and thermal treatment and was analyzed by SEM. The pre-treatment of PMS by alkali was observed to be more effective over the other pre-treatment methods. The alkali pre-treated sludge was then made to undergo fermentation, which showed the conventional process of acidogenesis followed by solventogenesis. The acetone, butanol, and ethanol concentration for 15% alkali pre-treated PMS was estimated to be maximum.  相似文献   
10.
The rapid development of internet of things (IoT) is to be the next generation of the IoT devices are a simple target for attackers due to the lack of security. Attackers can easily hack the IoT devices that can be used to form botnets, which can be used to launch distributed denial of service (DDoS) attack against networks. Botnets are the most dangerous threat to the security systems. Software-defined networking (SDN) is one of the developing filed, which introduce the capacity of dynamic program to the network. Use the flexibility and multidimensional characteristics of SDN used to prevent DDoS attacks. The DDoS attack is the major attack to the network, which makes the entire network down, so that normal users might not avail the services from the server. In this article, we proposed the DDoS attack detection model based on SDN environment by combining support vector machine classification algorithm is used to collect flow table values in sampling time periods. From the flow table values, the five-tuple characteristic values extracted and based on it the DDoS attack can be detected. Based on the experimental results, we found the average accuracy rate is 96.23% with a normal amount of traffic flow. Proposed research offers a better DDoS detection rate on SDN.  相似文献   
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