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1.
We examined the influence of polyaniline (PAn)'s unit sequence and doping with low molecular weight dopants or polymer dopants on permeation property. It was found that CO2 permeability was increased by the formation of a quinonediimine unit in PAn with the oxidation. CO2 sorption amount of PAn was decreased by oxidation. The increase of CO2 permeability with oxidation, therefore, resulted from the increase of diffusivity, which was attributable to morphological variation by the increase of a quinonediimine unit. The permselectivity of PAn films was found to be remarkably improved by doping. In particular, the selectivity value of the PAn film doped with polyvinyl sulphonic acid as a polymer dopant went up to over 2,000. This remarkable increase of selectivity was found to result in the increase of selectivity, depending on diffusivity. It was also found that the permselectivity of the PAn film doped by polymer dopants was surpassed, as compared with that doped by low molecular dopants. © 1995 John Wiley & Sons, Inc. 相似文献
2.
Minoru Tsuda Setsuko Oikawa Akira Yokota Mitsuo Yabuta Wataru Kanai Ken-Ichi Kashiwagi Isamu Hijikata Hisashi Nakane 《Polymer Engineering and Science》1983,23(18):993-999
A dry developable negative working resist composition comprised of poly(methyl isopropenyl ketone) (PMIPK) and 4-methyl-2,6-di(4′-azido-benzylidene) cyclohexanone-1 was examined. The main photochemical product formed in the resist pattern was found to be a secondary amine which crosslinks PMIPK. Post-annealing forms a hydrogen-bonded product which shows a powerful electronic excitation energy quenching effect. The quencher is more powerful than the aromatic compound arising from the azide by post-annealing only. The residual resist thickness of the negative pattern is about 80 percent of the initial thickness of the coating in spite of all the azide compound remaining in the resist coating. The obtained dry developed resist pattern has a high dry etch resistance. Etchings of Si and SiO2 were performed by plasma and reactive ion etching, respectively. 相似文献
3.
Hoshiaki Iijima Osamu Taguchi Ken-Ichi Hirano 《Metallurgical and Materials Transactions A》1977,8(6):991-995
Interdiffusion coefficient
in cobalt-manganese alloys has been determined by Matano's method in the temperature range between 1133 and 1423 K on (pure
Co)-(Co-30.28 at. pct Mn alloy) and (pure Co)-(Co-51.76 at. pct Mn alloy) couples. This, ∼D, has been found to increase with the increase of manganese content. However, the activation energy (∼Q) and frequency factor (
0) show a maximum at about 10 at. pct Mn. The concentration dependence of
and
has been discussed taking into account the thermodynamic properties of the alloy. The difference in
between the ferro- and paramagnetic phases in Co-5 at. pct Mn alloy has been found to be 24 kJ/mol, which is larger, than
that for the diffusion of Mn54 in this alloy. Further it has been found that the Kirkendall marker moves toward manganese-rich side, showing that manganese
atoms diffuse faster than cobalt atoms. From the marker shift, the intrinsic diffusion coefficients,D
Co andD
Mn, at 33 at. pct Mn have been determined as follows:D
Co=0.22×10−4 exp(−263 kJ mol−1/RT) m2/s, andD
Mn=0.98×10−4 exp(−229 kJ mol−1/RT) m2/s. 相似文献
4.
6-(2-Cyanoethylamino)-6-deoxycellulose (Cell-CEA) as a novel cellulose derivative was prepared from 6-bromo-6-deoxycellulose. The influence of the reaction conditions on the degree of substitution was studied in detail. The dielectric characteristics of a Cell-CEA sample having degree of substitution of 0.86, together with those of microcrystalline and regenerated celluloses, have been investigated in the temperature range from −60 to 120°C, and frequency range 30 Hz to 100kHz. One relaxation process, designated as β, was recognised, which was attributed to side-group motions, probably −CH2X (X = OH or NHCH2CH2CN). The higher activation energy of this process and the shift to higher temperature in Cell-CEA, compared with microcrystalline and regenerated celluloses, reflects the enhanced steric constraints involved in the motion of the bulkier, −CH2NHCH2CH2CN, side groups. The results obtained are discussed in terms of the dielectric parameters ϵ″max′ β and Δϵ. 相似文献
5.
Shoya Ueno Yuki Nakamura Ken-Ichi Sugioka Masaki Kubo Takao Tsukada Masahito Uchikoshi Hiroyuki Fukuyama 《International Journal of Thermophysics》2017,38(2):16
The normal spectral emissivity of molten Cu–Co alloy with different compositions was measured in the wavelength range of 780 nm to 920 nm and in the temperature range of 1430 K to 1770 K including the undercooled condition by an electromagnetic levitator superimposed with a static magnetic field. The emissivity was determined as the ratio of the radiance from a levitated molten Cu–Co droplet measured by a spectrometer to the radiance from a blackbody calculated by Planck’s law at a given temperature, where a static magnetic field of 2.5 T to 4.5 T was applied to the levitated droplet to suppress the surface oscillation and translational motion of the sample. We found little temperature dependence of the normal spectral emissivity of molten Cu–Co alloy. Concerning the composition dependence, the emissivity decreased markedly above 80 at%Cu and reached that of pure Cu, although its dependence was low between 20 at%Cu and 80 at%Cu. In addition, this composition dependence of the emissivity of molten Cu–Co alloy can be explained well by the Drude free-electron model. 相似文献
6.
7.
Porous membrane tubes filled with an absorbing solution that change colors upon selective reactions with specific gases provide high sensitivity inexpensive gas sensors. These can be routinely used for ambient monitoring in a fully automated manner. We consider both stopped and continuous flow operations and show the superiority of the stopped flow mode theoretically and experimentally. Light throughput through various membrane tubes is presented, and superior performance of such tubes over Teflon AF is shown. Sensors for NO2 and for O3 were based on Griess-Saltzman and indigotrisulfonate chemistries, respectively. A computer-controlled two-LED absorbance measurement system (one wavelength monitors the signal, the other references the system) that also governs automated reagent refilling was implemented. Sub-parts-per-billion-volume detection limits are attainable within a few minutes for both gases. Comparative data with a commercial UV-photometry-based ozone monitor showed excellent agreement with the response pattern of the present instrument. Low cost, ready applicability to the measurement of different gases by merely changing the light source and chemistry, and high sensitivity makes this instrument attractive for both pedagogic and practical purposes. 相似文献
8.
Mizuno Makoto Imai Satoshi Tsukada Minoru Hida Eiki Naka Ken-Ichi 《IEEE transactions on bio-medical engineering》1985,(1):56-60
A microcomputer system was developed to measure visual spatiotemporal receptive fields. The system performs three functions: 1) generation of a binary spatiotemporal white-noise stimulus, 2) acquisition of spike discharges from retinal ganglion cells, and 3) extraction of the linear part of the spatiotemporal receptive flelds by cross correlating the input against the output. We have applied this system to the measurement of the spatiotemporal receptive fields of cat and catfish retinal ganglion cells. 相似文献
9.
10.
Yokoyama Kiyoko Ishii Naohiro Naka Ken-Ichi 《IEEE transactions on bio-medical engineering》1986,(3):308-314
A software system was produced to digitize neuronal images and to extract a set of simple parameters from the digitized images. The system was designed to classify a large number of neurons based on simple and automatically extracted features. The system was used to characterize catfish retinal ganglion cells. Several examples of parameter extraction and classification are presented. 相似文献