液相还原法制备纳米银粉的研究

在液相联氨还原法工艺基础上，对液相还原法制备纳米银粉的还原反应条件（体系温度、分散剂、反应物浓度）进行了研究，得到了优化的反应条件；反应体系温度70℃，反应物浓度[Ag[NH3]2^ ]=0.02mol/l和特定的分散剂2^#。且冬季同平均粒径约为50nm、大小均匀、灰白色的球状银粉。     

Fractionation of transgenic corn for recovery of recombinant enzymes

Two germ-separation methods, dry-milling and density separation by flotation, were evaluated for recovering recombinant β-glucuronidase (rGUS) that accumulated primarily in the germ of transgenic corn. The dry-milling process consisted of (i) seed tempering, (ii) degerming with a horizontal-drum degermer/dehuller, (iii) particle size fractionation with standard sieves, (iv) germ and endosperm separation by roller milling and sifting, and (v) removal of hulls by aspiration. Sieves nos. 5, 6, and 7 retained the majority of germ, and subfractions from these sieves were pooled as a germ-rich fraction. Mass balances showed that the germ-rich fraction, which constituted 17% of the total dry-milled corn weight, contained 49% of rGUS activity and 64% of the total recoverable oil. Germ fractionation by flotation was tested as a proof-of-concept method aimed at separating corn fractions based on their difference in specific gravity (sp gr). The process consisted of impact-grinding of corn kernels followed by density separation using 1.15 or 1.3 specific gravity sodium nitrate solution. The oil-containing germ fraction floated, whereas the heavier endosperm fraction sedimented. The flotation method was simpler and resulted in higher enzyme recovery, that is, the germ-rich fraction was 20% (w/w) of the initial corn weight, and accounted for 80% of rGUS activity and 77% of total oil. The sodium nitrate solution did not have an adverse effect on the enzyme activity.     

Coherent Phonon-Induced Modulation of Charge Transfer in 2D Hybrid Perovskites

Electron–phonon interactions play an essential role in charge transport and transfer processes in semiconductors. For most structures, tailoring electron–phonon interactions for specific functionality remains elusive. Here, it is shown that, in hybrid perovskites, coherent phonon modes can be used to manipulate charge transfer. In the 2D double perovskite, (AE2T)₂AgBiI₈ (AE2T: 5,5“-diylbis(amino-ethyl)-(2,2”-(2)thiophene)), the valence band maximum derived from the [Ag_0.5Bi_0.5I₄]^2– framework lies in close proximity to the AE2T-derived HOMO level, thereby forming a type-II heterostructure. During transient absorption spectroscopy, pulsed excitation creates sustained coherent phonon modes, which periodically modulate the associated electronic levels. Thus, the energy offset at the organic–inorganic interface also oscillates periodically, providing a unique opportunity for modulation of interfacial charge transfer. Density-functional theory corroborates the mechanism and identifies specific phonon modes as likely drivers of the coherent charge transfer. These observations are a striking example of how electron–phonon interactions can be used to manipulate fundamentally important charge and energy transfer processes in hybrid perovskites.     

基于Ad hoc网络的联合有效用户识别与信道安全编译码方法

Ad hoc网络是一种无中心的自组织网络,由于用户能量受限当信噪比较低时有效用户识别的可靠性和信道安全性下降.该文针对这个问题提出一种联合有效用户识别与信道安全编译码方法.将发送用户的正交地址码与接收用户的伪随机地址码异或产生基于发送用户与接收用户的有效用户识别码.为提高信道安全性以信道安全码作为密钥加密有效用户识别码得到正交随机安全序列.为实现扩频并提高传输效率将发送数据以6 bit信息作为一个符号进行分组,将每个符号与一个正交随机安全序列对应.接收用户采用基于子空间的方法处理接收信号,通过建立判决模型识别有效用户.实验结果表明该方法与已有方法相比,当有效用户识别的漏警概率为10–3时信噪比增益改善1.6 dB.     

Noise analysis of robot manipulator using neural networks

Due to a lot of robot manipulators application in industry, low noise degree is very important criteria for robot manipulator's joints. In this paper, joint noise problem of a robot manipulator with five joints is investigated both theoretically and experimentally. The investigation is consisted of two steps. First step is to analyze the noise of joints using a hardware and software. The hardware is a part of noise sensors. The second step; according to experimental results, some neural networks are employed for finding robust neural noise analyzer. Five types of neural networks are used to compare each other. From the results, it is noted that the proposed RBFNN gives the best results for analyzing joint noise of the robot manipulator.     

Approximate periodic solutions for the Helmholtz-Duffing equation

Approximate periodic solutions for the Helmholtz-Duffing oscillator are obtained in this paper. He’s Energy Balance Method (HEBM) and He’s Frequency Amplitude Formulation (HFAF) are adopted as the solution methods. Oscillation natural frequencies are analytically analyzed. Error analysis is carried out and accuracy of the solution methods is evaluated.     

Investigation of different load changes in wind farm by using FACTS devices

In this study, voltage, active power and reactive power variation of load bus were examined by Flexible AC Transmission Systems devices (FACTS) in grid-connected wind farm. In the system, FACTS devices, Static Synchronous Compensators (STATCOM), Static VAr Compensators (SVC), Static Synchronous Series Compensators (SSSC) and Thyristor Controlled Series Compensators (TCSC), were used. Also, dual feed induction generator (DFIG) was used as generator in the wind farm. This simulation study was done via Matlab/Simulink environment. According to different values of active and reactive loads at different times being attached to the system, shapes of load bus voltage, active power and reactive power variation were given, also the results were presented in tables. In the conclusion of this study, by means of FACTS devices that is used in the wind farm, instability was healed within a short time.