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排序方式: 共有64条查询结果,搜索用时 15 毫秒
1.
N Cho Y Nara M Harada T Sugo Y Masuda A Abe K Kusumoto Y Itoh T Ohtaki T Watanabe S Furuya 《Canadian Metallurgical Quarterly》1998,46(11):1724-1737
On the basis of structural information for the cyclic hexapeptide endothelin (ET) receptor antagonist, TAK-044, a series of thieno[2,3-d]pyrimidine-2,4-dione derivatives bearing a carboxyl group and aromatic rings that were important for receptor binding were designed, synthesized, and evaluated for ET receptor binding affinities and inhibitory activities against ET-induced vasoconstriction. Optimization of each substituent in the thieno[2,3-d]pyrimidine ring led to the discovery of a novel and potent nonpeptide ET receptor antagonist, 6-(4-methoxymethoxyphenyl)-5-methylsulfonylaminomethyl-1-(2- methylthiobenzyl)-2,4-dioxo-1,2,3,4-tetrahydrothieno[2,3-d]p yrimidine-3- acetic acid (32 g), which binded to human ETA and ETB receptor subtypes with affinities (IC50) of 7.6 and 100 nM, respectively. Compound 32 g effectively antagonized ET-induced vasoconstriction and the inhibitory effect mediated by the ETB receptor was more potent than that of bosentan, while the inhibitory effect mediated by the ETA receptor was slightly less potent than that of bosentan. 相似文献
2.
Masaaki Takehisa Hiromasa Watanabe Hirondo Kurihara Kouichi Yamaguchi Hayato Nakajima Toshiaki Yagi Terutaka Watanabe Takanobu Sugo Takeshi Suwa Shinsaku Maruyama Atsuro Kodama Takeo Shimada Yoshio Maruyama Masamichi Tohei Takeshi Wada Sueo Machi 《应用聚合物科学杂志》1979,24(8):1831-1844
Radiation-induced polymerization of ethylene using aqueous tert-butyl alcohol as medium was carried out in a large-scale pilot plant with a 50-liter central source-type reactor at a pressure of 105 to 395 kg/cm2, temperature of 30° to 80°C, mean dose rate of 4.5 × 104 to 1.9 × 105 rads/hr, ethylene feed rate of 5.5 to 23.5 kg/hr, and medium feed rate of 21 to 102 l./hr. The space–time yield and molecular weight of the polymer were in the range of 4.7 to 16.8 g/l.-hr and 1.3 × 104 to 8.9 × 104, respectively. The space–time yield and molecular weight increased with mean residence time at 30°C, whereas at 80°C they became almost independent of the time. The space–time yield increased with pressure and dose rate, slightly decreased with temperature, and was maximum at ethylene molar fraction of 0.5. The polymer molecular weight increased with pressure and ethylene molar fraction, and decreased with dose rate and temperature. The total amount of deposited polymer on the reactor wall, source case wall, and scraping blades was usually less than 1 kg, which was negligibly small for the analysis of polymerization. Continuous discharge of the polymer slurry and production of fine-powder polyethylene were successfully carried out. In the central source-type reactor, a dose rate of 1.9 × 105 rads/hr was obtained with a 60Co source of ca. 12 kCi. 相似文献
3.
Effect of running‐in process on friction behaviour of carbon nitride (CNx) coating in N2 gas stream was investigated with a newly introduced two‐step ball‐on‐disk friction test, where the rubbed Si3N4 ball in the pre‐sliding (step 1) was replaced by a new CNx‐coated Si3N4 ball in the subsequent sliding stage under N2 gas (step 2). The two‐step friction test is clarified to be a simple but effective technique for obtaining contact material combination of self‐mated CNx coatings and for achieving stable and low frictions of CNx coatings. Friction coefficients of CNx/CNx in N2 gas stream decrease greatly from 0.07 without pre‐sliding to less than 0.025 in two‐step friction tests. The minimum friction coefficient of 0.004 was obtained by introducing 500 cycles of pre‐sliding in ambient air. These stable and low frictions are attributed to the generation of self‐mated CNx coatings and the formation of a lubricious layer on the disk surface. Copyright © 2014 John Wiley & Sons, Ltd. 相似文献
4.
Shoichi MATSUDA Naomichi SAJI Minoru YAGA Masaaki ISHIKAWA Kenyu OYAKAWA 《热科学学报(英文版)》2010,19(3):228-233
This paper will present the characteristics of flow behavior and thermal field of both free and
impingement jet issued from a circular orifice nozzle at Re=8900.The flow behavior of a single round
jet and impingement jet was observed by smoke flow visualization recorded by a high speed camera
using 5000 frame per second.Heat transfer coefficient on the impingement surface was measured by
means of infrared camera (TVS-8500,Avio) with a two-dimensional array of Indeum-Antimony (In Sb)
sensors varying in the separation distance between the nozzle and the target plate.The heat transfer
coefficient changes in time and spatial.Therefore,the root mean square distribution of the heat
transfer was obtained from the data.As a result,it was confirmed that the longitudinal vortex was
observed outside of the ring vortex,and then the longitudinal vortex was penetrated in the jet
flow.Moreover,the high value of root mean square of the heat transfer coefficient has spread radially
in stripy manner,which is caused as the results of the longitudinal vortexes flowing in the radial
direction on the impingement plate. 相似文献
impingement jet issued from a circular orifice nozzle at Re=8900.The flow behavior of a single round
jet and impingement jet was observed by smoke flow visualization recorded by a high speed camera
using 5000 frame per second.Heat transfer coefficient on the impingement surface was measured by
means of infrared camera (TVS-8500,Avio) with a two-dimensional array of Indeum-Antimony (In Sb)
sensors varying in the separation distance between the nozzle and the target plate.The heat transfer
coefficient changes in time and spatial.Therefore,the root mean square distribution of the heat
transfer was obtained from the data.As a result,it was confirmed that the longitudinal vortex was
observed outside of the ring vortex,and then the longitudinal vortex was penetrated in the jet
flow.Moreover,the high value of root mean square of the heat transfer coefficient has spread radially
in stripy manner,which is caused as the results of the longitudinal vortexes flowing in the radial
direction on the impingement plate. 相似文献
5.
This paper shows the effects of clearance length between a body and a duct wall, and duct height on the heat transfer characteristics and flow behavior at a downstream region of the body when a blunt body was set in a parallel plate duct with some distance separating it from the duct wall as a turbulence promoter. For the ratio of clearance to body height, C/D = 0.05–01, the heat transfer was characterized by the reattachment of shear flow separated from the body. Furthermore, the heat transfer depended on both the reattachment flow and the separation vortex at C/D = 0.15–0.2, and the side vortex induced by Karman vortex at C/D = 0.25–0.275 was also observed. We found the reattachment flow gives a superior effect to enhance heat transfer at a low Reynolds number, but at a larger Reynolds number, the side vortex induced by Karman vortex becomes more effective to heat transfer enhancement. © 2005 Wiley Periodicals, Inc. Heat Trans Asian Res, 34(5): 336–349, 2005; Published online in Wiley InterScience ( www.interscience.wiley.com ). DOI 10.1002/htj.20067 相似文献
6.
7.
8.
S Sugo N Minamino K Kangawa K Miyamoto K Kitamura J Sakata T Eto H Matsuo 《Canadian Metallurgical Quarterly》1994,201(3):1160-1166
This study demonstrates active production of adrenomedullin (AM) in cultured vascular endothelial cells (ECs). To identify the origin of plasma AM and its functional relationship to vascular smooth muscle cells (VSMCs), we checked production of AM in a series of tissues and cell lines and found immunoreactive (ir-) AM in culture media of rat, porcine, human and bovine ECs. Ir-AM was accumulated linearly for up to 48 hours in the culture medium of rat ECs, and the secretion rate of AM was almost comparable to that of endothelin-1. By gel filtration and reverse phase high performance liquid chromatography, ir-AM in the culture medium was shown to have chromatographic behavior indistinguishable from that of synthetic rat AM. By RNA blot analysis of rat tissue, the most highly positive band was detected in cultured ECs, at an intensity 20 to 40 fold higher than that in adrenal gland. Based on these data as well as the presence of AM specific receptor on VSMCs, AM secreted from ECs is deduced to act directly on VSMCs, regulating vascular tone. 相似文献
9.
Masaaki Takehisa Sueo Machi Hiromasa Watanabe Takashi Ueno Seiichi Takahashi Ryoji Tsuchiya Kanji Otaguro Isao Motoda Yoshio Takasaka Kazukiyo Miyanaga Waichiro Kawakami Kouichi Yamaguchi Takanobu Sugo Hayato Nakajima Terutaka Watanabe Chuhei Hinachi 《应用聚合物科学杂志》1979,24(3):853-864
Radiation-induced bulk polymerization of ethylene was carried out with use of a pilot plant with a 10 liter reactor at pressures of 225–400 kg/cm2, temperatures of 30–95°C, ethylene feed rates of 5–28 kg/hr, and dose rate of 3.8 × 105 rad/hr. Characteristics of the process are mild polymerization conditions and capability of producing medium density polyethylene in powder form. The spacetime yield and molecular weight of polymer were in the range of 3.5 to 13.1 g/liter hr and 2.2 × 104 to 14 × 104, respectively. The space-time yield increased with mean residence time and 2.4 powders of pressure, and decreased with temperature. Molecular weight changed similarly with the reaction conditions. These results were consistent with those of the bench plant experiment and the scale effect was small. Polymer deposit to the reactor wall limited a period of continuous operation of the plant. The amount of deposited polymer was increased with the square of reaction time. The rate of polymer deposit was proportional to polymer concentration and to the cube of pressure. The polymer deposit cannot be solved in the bulk process. 相似文献
10.
We studied the one-step purification of endotoxin by hydroxyapatite chromatography using total lipids extracted from Escherichia coli by the Bligh and Dyer method. High endotoxic activity was detected in a fraction eluted from 0.5 mg total lipids using an isopropanol gradient under salt-free buffer conditions. The fraction contained at least 7,000 endotoxin units and was completely free from other phospholipids. Notably, the running time of the chromatographic separation was approximately 4 h, whereas purification by the conventional hot phenol–water procedure requires ≥60 h. The procedure developed here is a simple, scalable, and rapid method for the purification of endotoxin. 相似文献