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1.
J. M. Parpia W. P. Kirk P. S. Kobiela Z. Olejniczak 《Journal of Low Temperature Physics》1985,60(1-2):57-72
The ac susceptibility of lanthanum-diluted cerium magnesium nitrate has been compared to the temperature scales as derived
from the (P, T) relation determined by Halperin and that was measured recently by Greywall. It is found that the susceptibility does
not obey a simple Curie-Weiss law over the temperature range between 1 and 50 mK. The results of these calibrations are also
used to determine the temperatures for the second-order phase transitions into the superfluid phases of3He at several pressures. TheseT
c(P) values are compared to results of earlier experiments that used thermometry based on the susceptibility of platinum as well
as other thermometry techniques. 相似文献
2.
Scale and sludge from Bulalo geothermal field, Philippines, have been characterized by whole rock analysis, radioactivity counting, size analysis, light microscopy, scanning electron microscopy, and X-ray diffraction. Their leachability was assessed by regulatory leaching procedures and by sequential extraction. Both scale and sludge consisted mostly of oxides of Si, Al, and Fe with no radionuclides detected. The scale had 10% S content. Sulfides and silicates were important phases in both samples having size ranges from submicron to 2 mm. Geothermal soils at Bulalo have higher than normal soil levels of As, S, Cu, Cr, Zn, and Pb but regulatory leaching tests indicated that these elements are not released. However, the sequential extraction showed that As, Cu, and Zn were leachable under extreme conditions. 相似文献
3.
The crystallization behaviour of three amorphous alloys, Co50Ni25Si15B10, Ni50Co25Si15B10 and Ni50Co25P15B10, was studied by means of differential thermal analysis in conjunction with scanning transmission electron microscopy. Isochronal annealing showed a strong dependence of crystallization on scan rate over the range of 1.99 to 20.70 K min–1. At high Co/Ni ratios, a sequential two-stage crystallization process involving primary MS-I phase followed by MS-II phase precipitation was observed. At low Co/Ni ratios MS-I and MS-II crystallization were concurrent and inseparable. Replacement of the metalloid Si with P as the glass-former dramatically reduced the activation energy for crystallization as well as the crystallization temperature. A mechanistic understanding of these findings was pursued in light of TEM/STEM microanalysis 相似文献
4.
The formation of zinc ferrite (ZnFe2O4) during the roasting of iron-bearing zinc concentrates requires substantial additional processing to recover the zinc from
this compound by leaching and to eliminate the iron from the leachate. The phase changes that occur in the particles of a
typical industrial zinc sulfide concentrate during roasting in a fluidized bed at 1223 K were investigated by the use of light
microscopy, electron microprobe analysis, and SEM with EDS. The processes which the iron undergoes during its eventual transformation
into ferrite have been clarified by examination of the phases and the morphology of partially roasted marmatitic sphalerite
particles (Zn, Fe)S, and by reference to the known phase equilibria involved in the Zn-Fe-S-0 system. The oxidation of ironbearing
sphalerite occurs in three stages. The first involves the selective diffusion of most of the iron to the particle surface
resulting in the formation of an iron oxide shell enclosing a largely unreacted zinc sulfide kernel. In the second stage,
this kernel is oxidized to form a solid solution of zinc oxide and iron oxide. The iron is initially present in the ferrous
state but, with the disappearance of the sulfide kernel, is oxidized to ferric iron. In the final stage, this dissolved iron
oxide and the iron oxide shell react with the surrounding zinc oxide to form the refractory spinel zinc ferrite. 相似文献
5.
Kirk C. Valanis 《Canadian Metallurgical Quarterly》2003,129(9):1039-1047
In this paper we derive Newton’s 2nd Law of Motion from the constitutive equation of elasticity of a space-time continuum in four dimensions. This we do by introducing a four-dimensional material continuum with a Minkowskian metric, in analogy with Einstein’s general theory of relativity. The four-continuum is deformable in both space and time. The physics of the deformation is embedded in a variational principle, which is a form-invariant extension of its classical mechanical counterpart in three dimensions, but with the acceleration term absent. General dynamic equations of elasticity in four dimensions are thereby derived. When the constraint of temporal inextensibility (universal time) is introduced, these equations yield readily the dynamic equations of elasticity in three dimensions. The presence of the inertia term in these equations, is a direct consequence of the temporal curvature induced by the deformation of the four-continuum. Newton’s law of motion for rigid bodies follows when the additional constraint of spatial inextensibility is introduced. 相似文献
6.
Montmorillinite clays, modified with either Zn(II) or Fe(III) chlorides have been used to catalyze the Friedel-Crafts alkylation of thiophene. High yields (ca. 80%) of 2- and 3-benzylthiophene mixtures were obtained using either catalyst in chlorobenzene or nitrobenzene solvent at 80°C. The ratio of 2–3-products was found to be controlled by their relative stability. Reactions were most rapid in nitrobenzene solution (<5 min) and resulted in formation of the 2-isomer as the only mono-substituted product. This is believed to be the first example in which an alkylation of thiophene has been limited to one regio-isomer. 相似文献
7.
Heat-shock induction of heat-shock protein genes is due to a specific promoter element (the heat-shock element, HSE). This study used lacZ under HSE control (HSE-lacZ) to characterize HSE activity in Saccharomyces cerevisiae cells of different physiological states and differing genetic backgrounds. In batch fermentations HSE-lacZ induction by heat shock was maximal in exponential growth, and showed marked decline with the approach to stationary phase. Expression in the absence of heat shock was unaffected by growth phase, indicating that the growth-dependent expression of many yeast heat-shock genes uses promoter elements in addition to the HSE. Heat-induced expression was strongly influenced by the temperature at which cultures were grown. While basal, uninduced expression was constant during growth at different temperatures to 30 degrees C, induction by transfer to 39 degrees C was reduced by increases in growth temperature as low as 18-24 degrees C. Maximal HSE-lacZ induction (30- to 50-fold) was in cultures grown at low temperatures (18-24 degrees C), then heat shocked at 39 degrees C. Ethanol was a poor inducer. Mutations having little effect on HSE-lacZ expression included a respiratory petite; ubi4 (which inactivates the poly-ubiquitin gene); also ubc4 and ubc5 (which each inactivate one of the ubiquitin ligases involved in degradation of aberrant protein). pep4-3 increased both basal and induced beta-galactosidase about two-fold, probably because of slower turnover of this enzyme in pep4-3 strains. 相似文献
8.
9.
JH Noseworthy P O'Brien BJ Erickson D Lee D Sneve GC Ebers GP Rice A Auty WJ Hader A Kirk P Duquette J Carter G Francis L Metz E Shuster 《Canadian Metallurgical Quarterly》1998,51(5):1342-1352
OBJECTIVE: To determine whether sulfasalazine is better than placebo in slowing disability progression in MS. METHODS: In this randomized, double-blind, placebo-controlled phase III trial, 199 patients with active relapsing-remitting (n = 151) or progressive (n = 48) MS were evaluated at 3-month intervals for a minimum of 3 years (94% completed 3 years of follow-up; mean follow-up, 3.7 years). MRI studies were performed at 6-month intervals on a subset of 89 patients. RESULTS: Sulfasalazine failed to slow or prevent disability progression as measured by the primary outcome (confirmed worsening of the Expanded Disability Status Scale [EDSS] score by at least 1.0 point on two consecutive 3-month visits). Sulfasalazine influenced favorably a number of secondary outcomes during the first 18 months of the trial (e.g., annualized relapse rate, proportion of relapse-free patients; progressive subgroup only: rate of EDSS progression at 1 and 2 years, median time to EDSS progression) but these positive findings were not sustained into the second half of the trial. CONCLUSIONS: Sulfasalazine does not prevent EDSS score progression in the subset of MS patients studied by this protocol. Treatments may improve relapse-related outcomes in MS, at least temporarily, without providing sustained slowing of EDSS progression. Phase III MS trials should be of sufficient length to determine a meaningful impact on disease course. 相似文献
10.