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1.
2.
A new polymer electrolyte poly(acrylonitrile)-dimethylsulphoxide-salt for electrochemical capacitors
The PAN-DMSO-Et4NBF4 and PAN-DMSO-Et4NTf (Tf is triflate ion) electrolytes were prepared as white, turbid foils with a thickness in the range of 0.1-0.5 mm, using the casting technique. Room temperature conductance of the electrolytes, detected from ac impedance experiments, was at the level of 8 and 14 mS cm−1 for Et4NBF4 and Et4NTf salts, respectively. The electrochemical stability window of approximately 2.6-2.8 V was estimated using a glassy carbon electrode. Temperature dependence of the conductivity is of the Arrhenius-type for both electrolytes, with an activation energy of approximately 34 kJ mol−1. The double-layer capacitors built with these electrolytes, serving both as separators and activated carbon powder (ACP) binders, showed a specific capacity of 50 F g−1 of carbon material. Capacitors were assembled by sandwiching the PAN-DMSO-salt electrolyte between two PAN-salt-DMSO-ACP-AB electrodes and pressing across the system; the resulting devices had a coin-like shape with 8 mm diameter and thickness between 2.0 and 2.5 mm. 相似文献
3.
Chouping Luo Marek Klisinski 《International journal for numerical methods in engineering》2004,61(2):159-188
The present study is a continuation of our previous work with the aim to reduce problems caused by standard higher order elements in contact problems. The difficulties can be attributed to the inherent property of the Galerkin method which gives uneven distributions of nodal forces resulting in oscillating contact pressures. The proposed remedy is use of piece‐wise linear weight functions. The methods to establish stiffness and/or mass matrix for 8‐node quadrilateral element in 2D are presented, i.e. the condensing and direct procedures. The energy and nodal displacement error norms are also checked to establish the convergence ratio. Interpretation of calculated contact pressures is discussed. Two new 2D 8‐node quadrilateral elements, QUAD8C and QUAD8D, are derived and tested in many examples, which show their good performance in contact problems. Copyright © 2004 John Wiley & Sons, Ltd. 相似文献
4.
In this paper an analytical method for determining the permeability of nonwoven filter fabrics is presented. The derived formula shows that the intrinsic permeability, fully characterizing the porous medium, depends on fabric porosity, n, fibre diameter, d, and a shape factor determined experimentally. 相似文献
5.
Marek Markowski Ireneusz Bialobrzewski Janusz Bowszys Stanislaw Suchecki 《Drying Technology》2007,25(9):1527-1536
A neural-deterministic simulation model applied for calculating distributions of temperatures and moisture content in a bed of wheat stored in a steel silo without aeration is presented in the article. The model consists of differential equations of heat and moisture transfer, initial and boundary conditions, and three artificial neural networks used during simulated ambient air conditions. Experiments and computer simulations were carried out in order to determine temperature fields in wheat grain stored in a steel silo for two months. The computer simulations were carried using MATLAB and FEMLAB software. The difference between measured and simulated temperature in grain near the silo wall at a height of 2.5 m from the bottom was less than 3.0°C. On the basis of the analysis performed it was concluded that the temperature distributions obtained with the model were consistent with the measured results obtained for grain stored in a steel silo without aeration. 相似文献
6.
A. Hynaux C. Sayag S. Suppan J. Trawczynski M. Lewandowski A. Szymanska-Kolasa G. Djga-Mariadassou 《Catalysis Today》2007,119(1-4):3-6
Hydrodesulfurization (HDS) is part of the hydrotreating process, which is an ensemble of several reactions (HDN, HDO, HDS, etc.) taking place simultaneously at the industrial scale. Only sulfur is currently submitted to drastic Europeans specifications and conventional commercial catalysts cannot reach the specifications at low cost. This paper presents the behavior of a potential substitute catalyst tested for the deep HDS of a model molecule such as the dibenzothiophene (DBT). The substitute is molybdenum carbide supported on a mesoporous carbon black composite of surface area 240 m2 g−1. A global kinetic study of the deep HDS of DBT (300 ppm S) was performed at 623 K and 5.0 MPa and a global kinetic model was proposed as well as global rate constants were calculated to obtain theoretical plots of concentration versus contact time to compare with the experimental data. The kinetic model and global kinetic orders were confirmed as an acceptable correlation was found between calculated and experimental data. Furthermore, the determination of the global kinetic orders indicated that two types of active sites must be present on the surface in order to explain the observed results. 相似文献
7.
The effect of methanol, acetone, formalin and glucose on the nitrification process in the packed bed reactors has been investigated. For the utilized compounds the inhibition constant Ki was determined according to Dixon's method. The determined values were as follows: methanol Ki = 116.0 mg l?1; acetone Ki = 804.2 mg l?1; formalin Ki = 61.5 mg l?1. The value of Ki for glucose has not been determined because glucose in applied concentration up to 11,325 mg l?1 had no effect on the nitrification course. 相似文献
8.
The flow and fracture behavior of Be-Al alloys were determined in tension with different levels of superimposed pressure.
The Be-Al alloys were prepared by Brush Wellman, Inc. (Cleveland, OH) from prealloyed powders processed to either a hot isostatically
pressed (“hipped”) or cold isostatically pressed and extruded condition. Significant effects of pressure on both the flow
and ductility have been observed at room temperature, with implications on the formability of these materials. The effects
of changes in processing conditions and stress state on the flow and fracture behavior are summarized in addition to both
optical and scanning electron microscopy (SEM) examination of the fracture surfaces. Separate other studies on the alloy constituents
(e.g., Al and Be) are also reported. The results are also compared to previous works on monolithic materials and composites tested
with high pressure. 相似文献
9.
Marek Gondzio 《Software》1987,17(3):215-226
Every microprocessor-based system needs powerful debugging tools. Debugging power strongly depends on a mechanism of control exchange between the debugger and an application program. Several implementation methods of such a mechanism are briefly described and compared in this paper. It is shown that conditional breakpoints facilitate a semantics-oriented approach to program debugging. Some debugging techniques derived from elementary control-exchange mechanisms are proposed. Most of the techniques discussed are implemented in the MD-86 debugger designed for the Intel 8086 microprocessor. The debugger itself is also briefly described. 相似文献
10.
V. D. Okunev Z. A. Samoilenko V. A. Isaev A. Klimov S. J. Lewandowski 《Technical Physics Letters》2002,28(1):44-47
Experimental evidence is presented for the existence of clusters possessing metallic conductivity in epitaxial YBa2Cu3O6+x (x<0.4) films with a tetragonal structure. Despite the overall dielectric state, the optical transmission spectra reveal the regions of absorption due to free charge carriers. The presence of metallic clusters is also confirmed by the X-ray diffraction data. At low temperatures, these metallic clusters are capable of converting into quantum dots responsible for the θ(T) = const regions in the temperature dependence of the electric resistance. The process of cluster formation can be enhanced by high-power laser (KrF) radiation. 相似文献