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排序方式: 共有37条查询结果,搜索用时 15 毫秒
1.
Chateau Marie-Elise Galet Laurence Soudais Yannick Fages Jacques 《Journal of surfactants and detergents》2004,7(4):355-362
A new test was developed to assess the efficiency of no-wiping hard-surface cleaning. The test allows cleaner comparisons
according to their ability to remove greasy soils. The chosen approach minimizes the mechanical forces applied while cleaning
so that the interactions between a detergent solution and the soil to be removed can be characterized. For this, immersion
cleaning was chosen, with coated stainless steel as substrate and pigmented oils as the model soil. Several parameters were
studied in defined ranges using the Experimental Design method and systematic comparisons. The test shows high reliability
on degreasing assessments and is there-fore especially suited to optimization of nonionic surfactant mixes. The originality
of the test lies in the possibility of keeping a visual trace of the cleaned substrate appearance by imprinting it on a piece
of paper. The validation of the test leads to corroboration of several practical observations. Temperature and agitation play
a major role in cleaning efficiency. Detergent solution concentration is a more relevant parameter than pH. Sodium carbonate
is shown to have a higher buffering effect than pentahydrated sodium metasilicate. The test is easy to set up, highly sensitive,
and can be adapted to solve the problems encountered by formulators of detergent cleaners, such as screening the best ethoxylated
fatty alcohol mix for better degreasing properties. 相似文献
2.
Jordan A. Doumanov Christina Zeitz Paloma Dominguez Gimenez Isabelle Audo Abhay Krishna Giovanna Alfano Maria Luz Bellido Diaz Veselina Moskova-Doumanova Marie-Elise Lancelot José-Alain Sahel Emeline F. Nandrot Shomi S. Bhattacharya 《International journal of molecular sciences》2013,14(7):15121-15140
3.
D.-L. Nguyen S. Umbarkar M. K. Dongare C. Lancelot J.-S. Girardon C. Dujardin P. Granger 《Topics in Catalysis》2013,56(1-8):157-164
Supported gold catalysts on γ-Al2O3 have been investigated in the catalytic reduction of NO x in simulated Diesel exhaust gas conditions. Different parameters have been examined essentially the mode of gold incorporation via classical deposition–precipitation and anionic exchange methods and the nature of the pre-activation thermal treatment. The resistance to thermal ageing under reactive conditions at 500 °C was found completely different with a significant rate enhancement on anionic-exchange samples. Further comparisons also show that the nature of the pre-activation thermal treatment influences the extent of surface reconstructions during thermal ageing with a detrimental effect of reductive pre-treatment on the catalytic performances. 相似文献
4.
C Saturnino P Saturnino A Capasso G De Martino L Sorrentino JC Lancelot M Robba 《Canadian Metallurgical Quarterly》1998,53(6):354-360
OBJECTIVE: The measurements of transient evoked otoacoustic emissions and distortion-product otoacoustic emissions are being used increasingly, both as an objective hearing test clinically, and as a research tool to investigate the micromechanical aspects of cochlear function. We hypothesized that localized damage in the apical or middle cochlear turns may have an influence on the micromechanics and the function of adjacent, apparently normal cochlea. For that purpose, we used an animal model of localized apical and middle-turn cochlear lesions. METHOD: Extent of damage was assessed by scanning electron microscopy and the function of the damaged cochlea by change in the otoacoustic emission (OAE) levels. RESULTS: We found that localized damage to the apical or middle turn may be accompanied by an increase in OAE measured from adjacent apparently normal cochlea. CONCLUSION: Explanations to this phenomenon are suggested, and possible clinical associations such as to Meniere's disease and to sudden hearing loss are reviewed. 相似文献
5.
G Lancelot 《Canadian Metallurgical Quarterly》1977,59(7):587-596
Absorption studies of hydrogen bonding association between nucleic acid bases and amino acid side chains show that association constants can be determined from difference absorption spectra in cyclohexane and chloroform. Association constants for the binding of 9-ethyladenine, 1-cyclohexyluracil and 1-cyclohexylcytosine to side chains of serine, threonine, aspartic acid, lysine, cystéine, methionine and tyrosine are reported. Results obtained in chloroform and cyclohexane are compared. 相似文献
6.
Bailly C Viossat B Labouze X Morgant G Saturnino C Lancelot JC Robba M Dung NH 《Metal-Based Drugs》1998,5(5):279-285
The design, synthesis, crystal structure and interaction with DNA of the N,N'-(butane-1,4-diyl)bis(guanidinium) tetrachloroplatinate(ll) are described. Crystal data: a = 8.152(1), b = 8.889(4), c = 10.700(3) A , alpha = 81.59(3), beta = 87.99(5), gamma = 78.48(6) degrees , V = 752(1) A(3), Z = 2 , space group P-1. The structure was refined to R = 0.039 and Rw = 0.046 from 1853 reflections (I > 3sigma(I)). This compound, named PtC(4)Gua, does not exhibit a center of symmetry and the center linker chain C(2) - C(3) - C(4) - C(5) is in gauche conformation. The cation is bisprotonated with the H(+) attached to the imine group of each terminal guanidinium function. The presence of the platinum moiety reinforces the binding of the butane(bis)guanidinium structure with double stranded DNA as judged from thermal denaturation studies and DNA unwinding experiments. 相似文献
7.
Dr. Dmitrii V. Kalinin Dr. Sunit K. Jana Maxim Pfafenrot Dr. Alokta Chakrabarti Dr. Jelena Melesina Dr. Tajith B. Shaik Dr. Julien Lancelot Dr. Raymond J. Pierce Prof. Dr. Wolfgang Sippl Dr. Christophe Romier Prof. Dr. Manfred Jung Prof. Dr. Ralph Holl 《ChemMedChem》2020,15(7):559-559
Schistosomiasis is a neglected tropical disease caused by parasitic flatworms of the genus Schistosoma, which affects over 200 million people worldwide and leads to at least 300,000 deaths every year. In this study, initial screening revealed the triazole-based hydroxamate 2 b (N-hydroxy-1-phenyl-1H-1,2,3-triazole-4-carboxamide) exhibiting potent inhibitory activity toward the novel antiparasitic target Schistosoma mansoni histone deacetylase 8 (smHDAC8) and promising selectivity over the major human HDACs. Subsequent crystallographic studies of the 2 b /smHDAC8 complex revealed key interactions between the inhibitor and the enzyme's active site, thus explaining the unique selectivity profile of the inhibitor. Further chemical modifications of 2 b led to the discovery of 4-fluorophenoxy derivative 21 (1-[5-chloro-2-(4-fluorophenoxy)phenyl]-N-hydroxy-1H-1,2,3-triazole-4-carboxamide), a nanomolar smHDAC8 inhibitor (IC50=0.5 μM), exceeding the smHDAC8 inhibitory activity of 2 b and SAHA (vorinostat), while exhibiting an improved selectivity profile over the investigated human HDACs. Collectively, this study reveals specific interactions between smHDAC8 and the synthesized triazole-based inhibitors and demonstrates that these small molecules represent promising lead structures, which could be further developed in the search for novel drugs for the treatment of schistosomiasis. 相似文献
8.
Morgant G Viossat B Roch-Arveiller M Prognon P Giroud JP Lancelot JC Robba M Huy DN 《Metal-Based Drugs》1998,5(3):127-137
The synthesis and crystal structures of bis(S-methylisothiouronium) (MSTUH)(+), N,N'-bis((3- guanidinopropyl)piperazinium (PipeC3GuaH4)(4+) and hexamidinium (HexaH2)(2+) tetrachloro platinate(ll) salts ( called hereafter PtMSTU, PtPipeC3Gua and PtHexa respectively ) were investigated. These compounds contain the "amidine" function ( - C(=NH)NH(2) ) in which the H atoms supplied by the acid have become attached to the imino group of each terminal amidino function. Moreover, in PtPipeC3Gua, the nitrogen atoms of the chair-piperazine moiety are also protonated. The influence of tetrachloroplatinate(ll) counteranion ( versus sulfate, nitrate and diisethionate ) in the in vivo nitrite inhibition by the (MSTUH)(+), (PipeC3GuaH4)(4+) and (HexaH2)(2+) cations was investigated. The three tetrachloroplatinate(ll) salts, unexpectedly, do not inhibit significantly the in vivo nitrite production in comparison with the other salts (sulfate, nitrate and diisethionate and their corresponding previous countercations) which exhibit NO synthase inhibition, especially bis(S-methylisothiouronium) sulfate, a selective and potent inducible NO synthase (iNOS) inhibitor commonly used as standard. 相似文献
9.
The study evaluates the tumor distribution of the rapid clearance blood pool agent (RCBPA) gadomelitol, in a breast tumor model. Different techniques were used : (1) tissue gadolinium concentrations measured by inductively coupled plasma atomic emission spectroscopy (ICP-AES), (2) whole body quantitative autoradiography using radiolabeled [153Gd] gadomelitol and (3) dynamic contrast-enhanced MRI with compartmental analysis. An accumulation of gadomelitol in tumors compared to muscle was observed 30 min and 3 h post injection (p.i.). Thirty minutes p.i., the gadomelitol tumor distribution evaluated by autoradiography showed a marked difference between the rim and the center, whereas both areas showed comparable concentrations after 3 h. Using dynamic contrast-enhanced MRI, three phases could be observed during the 1 hour observation period: (1) rapid tumor uptake within the first few minutes post-injection (2) a progressive increase in tumor signal enhancement over 10 min and (3) a steady-state phase. Average +/− SD (n=5) transendothelial permeability KPS and the fractional blood volume fBV were 12.2±1.6 μl/min−1/g and 5.4±0.2% respectively. Due to its slow extravasation and high tumor residence time, gadomelitol may potentially be useful to improve characterization between benign versus malignant tumors using dynamic MRI. 相似文献
10.
Laurent Lancelot Isam Shahrour Marwan Al Mahmoud 《Canadian Metallurgical Quarterly》2006,132(12):1396-1399
Analysis of geotechnical problems concerned by low confinement such as design of shallow foundations and analysis of slope stability and soil liquefaction requires modeling of the soil behavior at low stresses. This note includes a laboratory study of the behavior of Hostun RF sand at low cell pressure (20–50?kPa). Isotropic and triaxial compression drained tests were performed. Drained tests show that both failure and dilatancy angles at low stresses are stress dependent. The contractive/dilative phase transition is observed for loose sand, which may result from the overconsolidated nature of this sand for low values of cell pressure. 相似文献