Iron-silicide was produced with a mechanical alloying process and consolidated through vacuum hot pressing. The as-milled powders were of metastable state and fully transformed into the ß-FeSi2 phase through subsequent isothermal annealing. The as-consolidated iron silicides consisted of an untransformed mixture of α-Fe2Si5 and ?-FeSi phases and a partially transformed β-FeSi2 phase was found in the low density compact. Isothermal annealing was carried out to induce transformation into a thermoelectric semiconducting β-FeSi2 phase. The transformation behavior of the β-FeSi2 was investigated utilizing DTA, SEM, and XRD analyses. Isothermal annealing at 830°C in vacuum led to a thermoelectric semiconducting β-FeSi2 phase transformation, but some residual metallic α and ?-phases were unavoidable even after 96 hours of annealing. The iron silicide microstructures were investigated using SEM and TEM. The mechanical and thermoelectric properties of the β-FeSi2 materials before and after isothermal annealing are characterized in this study. 相似文献
Recently, physical layer security commonly known as Radio Frequency (RF) fingerprinting has been proposed to provide an additional layer of security for wireless devices. A unique RF fingerprint can be used to establish the identity of a specific wireless device in order to prevent masquerading/impersonation attacks. In the literature, the performance of RF fingerprinting techniques is typically assessed using high-end (expensive) receiver hardware. However, in most practical situations receivers will not be high-end and will suffer from device specific impairments which affect the RF fingerprinting process. This paper evaluates the accuracy of RF fingerprinting employing low-end receivers. The vulnerability to an impersonation attack is assessed for a modulation-based RF fingerprinting system employing low-end commodity hardware (by legitimate and malicious users alike). Our results suggest that receiver impairment effectively decreases the success rate of impersonation attack on RF fingerprinting. In addition, the success rate of impersonation attack is receiver dependent. 相似文献
Coal devolatilization studies to maximize the yield of condensable products by operating at elevated temperatures and heating rates have been published. The objectives of this study were to investigate the influences of relatively mild operating conditions (e.g. relatively low temperature and pressure) on product quality, by comparing devolatilized products obtained at various temperatures and heating rates. Fixed bed, fluid bed, and entrained flow reactor units were used to obtain pyrolysis products. In addition, literature data on tar yields in various reactor units at a range of temperatures and residence times were surveyed and compared with experimental data. The liquids were characterized by a number of techniques, including field ionization mass spectroscopy (f.i.m.s.), sequential elution solvent chromatography (s.e.s.c.) and elemental analysis. The results demonstrate that the quality and yield of liquids obtained at a rapid heating rate are functions of peak pyrolysis temperature. It was shown that at a rapid heating rate, the yields of heavier polyfunctional groups (i.e. hydrocarbons with greater mean molecular weight) are greater than those obtained in the fixed bed slow heating rate reactor. The liquids generated at a slow heating rate are of lower molecular weight, viscosity, and sulphur content, and of higher H/C atomic ratios compared with the liquids obtained in a rapid heating rate unit. The effect of increasing the maximum pyrolysis temperature (at a constant slow heating rate) was to increase the yield of light gases (mainly H) at the expense of char hydrogen content and char reactivity. The tar yield is not markedly influenced when the peak devolatilization temperature is increased at a relatively slow heating rate. However, the quality (as defined by the H/C (atomic) ratio) of the liquids, and the reactivity (in air) of char, was reduced when the peak pyrolysis temperature was increased. At a rapid heating rate, the primary products, which have many structural characteristics of the parent coal, are devolatilized. The quality of the liquids obtained at a rapid heating rate is, therefore, determined by the devolatilized primary coal fragments evolved at the devolatilization temperature. In a slow heating rate fixed bed unit, however, the primary coal fragments undergo additional cracking reactions which involve stabilization of free radicals by donatable hydrogen. This leads to the formation of low molecular weight hydrocarbons of relatively higher quality. In-situ (both intraparticle or extraparticle) stabilization of reactive coal fragments by donatable hydrogen may lead to a significant improvement in the overall quality of the pyrolysis liquids in a fixed bed system in which time-temperature history is conducive for such reactions. 相似文献
Multimedia Tools and Applications - Nowadays, web users frequently explore multimedia contents to satisfy their information needs. The exploration approaches usually provide linear interaction... 相似文献
Multimedia Tools and Applications - The advancement in communication and computation technologies has paved a way for connecting large number of heterogeneous devices to offer specified services.... 相似文献
Speech emotion recognition (SER) systems identify emotions from the human voice in the areas of smart healthcare, driving a vehicle, call centers, automatic translation systems, and human-machine interaction. In the classical SER process, discriminative acoustic feature extraction is the most important and challenging step because discriminative features influence the classifier performance and decrease the computational time. Nonetheless, current handcrafted acoustic features suffer from limited capability and accuracy in constructing a SER system for real-time implementation. Therefore, to overcome the limitations of handcrafted features, in recent years, variety of deep learning techniques have been proposed and employed for automatic feature extraction in the field of emotion prediction from speech signals. However, to the best of our knowledge, there is no in-depth review study is available that critically appraises and summarizes the existing deep learning techniques with their strengths and weaknesses for SER. Hence, this study aims to present a comprehensive review of deep learning techniques, uniqueness, benefits and their limitations for SER. Moreover, this review study also presents speech processing techniques, performance measures and publicly available emotional speech databases. Furthermore, this review also discusses the significance of the findings of the primary studies. Finally, it also presents open research issues and challenges that need significant research efforts and enhancements in the field of SER systems.
As the number of objectives increases, the performance of the Pareto dominance-based Evolutionary Multi-objective Optimization (EMO) algorithms such as NSGA-II, SPEA2 severely deteriorates due to the drastic increase in the Pareto-incomparable solutions. We propose a sorting method which classifies these incomparable solutions into several ordered classes by using the decision maker's (DM) preference information. This is accomplished by designing an interactive evolutionary algorithm and constructing convex cones. This method allows the DMs to drive the search process toward a preferred region of the Pareto optimal front. The performance of the proposed algorithm is assessed for two, three, and four-objective knapsack problems. The results demonstrate the algorithm's ability to converge to the most preferred point. The evaluation and comparison of the results indicate that the proposed approach gives better solutions than that of NSGA-II. In addition, the approach is more efficient compared to NSGA-II in terms of the number of generations required to reach the preferred point. 相似文献
In this work, Bis-(3-triethoxysilylpropyl) tetrasulphane was employed for surface modification of silica, ferrite and kenaf fiber filled natural rubber composites using aqueous solvent deposition, dry blending and integral blend methods. The efficiency of each method and the preferred modification method for improving the mechanical performance of natural rubber composites was assessed. The appearance of the Fourier transform infrared spectroscopy peak around 1088 cm−1 for all types of fillers provided evidence that silane interaction had occurred between the fillers and rubber and the formation of siloxane linkages were quantitatively determined by the crosslink density measurement. The surface treatment by dry method for silica and ferrite fillers showed significant improvement of tensile performance at approximately 67% and 34% compared to those with untreated fillers. For kenaf fiber-filled rubber composites, the surface treatment by aqueous solvent deposition showed the highest tensile improvement of 59% compared to the dry blending and integral blend method. 相似文献
Mn doped p-type iron disilicide powders have been produced by a mechanical alloying process. As-milled powders were of metastable
state and mostly transformed to β-FeSi2 phase by subsequent isothermal annealing. As-milled powders were consolidated by various processes such as sintering of the
cold compact in vacuum, vacuum hot pressing (VHP), and spray drying/atmospheric plasma thermal spraying. Phase transitions
during the processes were investigated using XRD, EDS, and SEM. As-consolidated specimens consisted of a mixture of α-Fe2Si5 and ε-FeSi phases, which were gradually transformed into a thermoelectric semiconducting α-FeSi2 phase by subsequent isothermal annealing in the vicinity of 845°C in vacuum. However, some residual α and ε phases remained
even after prolonged annealing. Thermoelectric properties were measured as a function of temperature and correlated with phase
transformation. They showed optimum values in the vacuum hot pressed specimen due to a higher fraction of β phase and/or higher
density. 相似文献