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Rapid synthesis of silver nanowires(Ag NWs) with high quality and a broad processing window is challenging because of the low selectivity of the formation of multiply twinned particles at the nucleation stage for subsequent Ag NWs growth.Herein we report a systematic study of the water-involved heterogeneous nucleation of Ag NWs with high rate(less than 20 min) in a simple and scalable preparation method.Using glycerol as a reducing agent and a solvent with a high boiling point,the reaction is rapidly heated to 210 ℃ in air to synthesize Ag NWs with a very high yield in gram level.It is noted that the addition of a small dose of water plays a key role for obtaining highly pure Ag NWs in high yield,and the optimal water/glycerol ratio is0.25%.After investigating a series of forming factors including reaction temperature and dose of catalysts,the formation kinetics and mechanism of the Ag NWs are proposed.Compared to other preparation methods,our strategy is simple and reproducible.These Ag NWs show a strong Raman enhancement effect for organic molecules on their surface. 相似文献
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Physically based simulation of human hair is a well studied and well known problem. But the “pure” physically based representation of hair (and other animation elements) is not the only concern of the animators, who want to “control” the creation and animation phases of the content. This paper describes a sketch-based tool, with which a user can both create hair models with different styling parameters and produce animations of these created hair models using physically and key frame-based techniques. The model creation and animation production tasks are all performed with direct manipulation techniques in real-time. 相似文献
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在真空系统中的氘压低于0.1 MPa条件下研究了金属镱的吸氘性能,并对不同原子比的氘化物的物相进行了分析.在常压、300 ℃下,金属镱吸氘不明显;400 ℃时,金属镱经较长时间活化后吸附一定量的氘;500 ℃时,镱升华.400 ℃时的吸氘实验结果表明:从活化至开始吸氘直至吸附平衡需很长时间;氘/镱原子比的高低与吸氘时间有关,饱和吸氘时的原子比最大为2.00;金属镱为面心立方(fcc)结构,a0=0.549 2 nm.具有不同原子比的氘化镱的X射线衍射(XRD)分析结果显示:氘化镱有2种结构,即面心立方结构(a0=0.524 nm)和正交结构(a0=0.588 nm、b0=0.358 nm、c0=0.678 nm);金属镱吸氘后,立方结构氘化镱晶格常数及晶胞体积均发生收缩现象,收缩率分别约为4%和11%.正交结构氘化镱晶胞体积收缩约14%. 相似文献
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Morosi S. Marabissi D. Enrico Del Re Fantacci R. Del Santo N. 《Power Delivery, IEEE Transactions on》2006,21(4):1892-1897
This paper deals with a variable rate discrete multitone modulation system for broadband power-line communications, based on the bit-loading algorithm proposed by Leke and Cioffi. In the proposed system a suitable least mean square channel estimator is considered, which is based on the insertion of a training sequence (TS). The proposed approach will be compared with the ideal channel estimates, showing its effectiveness. Moreover, different TS lengths will be compared. The system performance, expressed in terms of bit rate and bit-error rate, is derived by simulation with and without estimation errors. The propagation environment has been assumed as a frequency-selective multipath fading channel with additive colored Gaussian noise, according to the in-building networks model. 相似文献
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This paper proposes a low complexity joint space-time multiuser detection algorithm for asynchronous DS/CDMA antenna array systems. The proposed multiuser detector is composed of an adaptive antenna array, used as a linear beamformer, and a sliding window decorrelator. A QPSK modulation scheme is used in order to increase bandwidth efficiency. Numerical results are given in terms of Bit Error Rate (BER) under the assumption of a frequency-selective Rayleigh slow fading channel. In particular, the proposed receiver is shown to be near-far resistant, even in worst fading cases, and to exploit completely array introduction while maintaining acceptable computational complexity. The proposed architecture avoids linear filter realization of the decorrelator, which is impractical in the case of a large number of users, and operates with relatively short data frames instead of the complete information sequence. Finally, this receiver is very flexible to changes in timing configuration. 相似文献